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Preparation of 3,4,5 trimethoxyphenylpyruvic acid
[rquote=653742&tid=156948&author=njl]Would sodium acrylate react the same way that acrylic a ...
26-1-2021 at 08:08
by: clearly_not_atara
Why is Chemsavers comfortable with shipping chemicals to residential addresses, but sigma/fisher/TCI/etc are not?
[rquote=648366&tid=156488&author=Cou]
Yeah if someone is just ordering some 1-pentanol, the ...
26-1-2021 at 06:39
by: clearly_not_atara
Preparation of 3,4,5 trimethoxyphenylpyruvic acid
Reactions of this form have been reported also with [b]hydantoin[/b], although the hydrolysis produc ...
26-1-2021 at 06:34
by: clearly_not_atara
Why do Mg salts not color the flame ?
https://physics.nist.gov/PhysRefData/Handbook/Tables/magnesiumtable2.htm

tl;dr: the strong lines ...
25-1-2021 at 07:25
by: clearly_not_atara
Nitric Acid and Silver Nitrate
[rquote=645553&tid=27851&author=Herr Haber]
I have 8 or 9 kilograms of plated crap in a box ...
22-1-2021 at 08:27
by: clearly_not_atara
Propionyl chloride with cyanuric chloride and anger
[rquote=653511&tid=156935&author=mr_bovinejony] Why would I bother bubbling hcl gas into thi ...
22-1-2021 at 08:05
by: clearly_not_atara
Propionyl chloride with cyanuric chloride and anger
I'm not sure PCl3 is so great for acid chlorides either. Usually PCl5 IIRC.

For acid chlorides fr ...
21-1-2021 at 20:41
by: clearly_not_atara
The simplest preparation of sulfuric acid?!
In principle, you should have no trouble distilling off all of the methanol. However, if dimethyl et ...
21-1-2021 at 08:57
by: clearly_not_atara
Small scale production of H2SO4 in the amateur lab
Hypothetically speaking:

Suppose you wanted to use what seems to be the consensus option for conc ...
20-1-2021 at 16:15
by: clearly_not_atara
Low(est) boiling point salts?
It depends on what you call a "salt". Is tungsten hexafluoride a salt? How about trimethylammonium a ...
20-1-2021 at 08:30
by: clearly_not_atara
1,3,5-trichlorohexahydrotriazine
[quote]It would probably give triazine with elimination of HCl.
[/quote]
This was the first thing ...
15-1-2021 at 15:15
by: clearly_not_atara
THIS WILL BE ILLEGAL IN FEBURARY 2021 (EU)
[rquote=653145&tid=156904&author=nitro-genes] for a scientist it is "Publish or Perish" and ...
15-1-2021 at 15:01
by: clearly_not_atara
Preparation of furfural from cherry gum and other pentose sources
[quote] Furfural from Cherry Gum “Syrup”[/quote]
Who would have thought you could do something ...
8-1-2021 at 10:27
by: clearly_not_atara
Things to do with Ethyl Formate
I would consider reduction -- Mg should recover Cu metal and triazole separately
8-1-2021 at 09:01
by: clearly_not_atara
Gamma Amino Butanal from GABA
Self-condensation will occur and in fact is nearly inevitable; this isn't a concern because it is re ...
6-1-2021 at 11:12
by: clearly_not_atara
Gamma Amino Butanal from GABA
Aldehydes react faster than esters in nearly all reductions, so you'll get a mixture of products. Th ...
3-1-2021 at 14:48
by: clearly_not_atara
Reductions of Nitro groups with Zn and acid
Interesting that a key here seems to be a fast addition and high temp. It seems more often "difficul ...
3-1-2021 at 14:40
by: clearly_not_atara
Does nuclear fusion really solve problems ?
http://en.wikipedia.org/wiki/Jevons_paradox

Bottom line is that if fusion does make electricity a ...
30-12-2020 at 09:46
by: clearly_not_atara
Iodide/sulphur dioxide adducts, BaI2 x 4 SO2
time for XRD :p
28-12-2020 at 14:09
by: clearly_not_atara
[Meme]Oh so you like amateur chemistry?
Only two words longer:
https://fermatslibrary.com/s/shortest-paper-ever-published-in-a-serious-math ...
20-12-2020 at 09:33
by: clearly_not_atara
Violuric acid salts (fantastic colors and variety)
Amazing work, had no idea this anion even existed, or that it was so colorful.

[rquote=651499& ...
18-12-2020 at 19:05
by: clearly_not_atara
Is it generally safe to openly evaporate heptane or does it pose an explosion hazard?
^don't do that

Heptane flows along the floor because it is a very heavy gas. It can remain somewh ...
18-12-2020 at 15:07
by: clearly_not_atara
Preparation of ethylene diamine from glycol and urea (via imidazolidone type polymer)
Nice!

extension: form mega-hexamine (1,3,6,8-tetraazatricyclo-[4.4.1.1[sup]3,8[/sup]]dodecane (TA ...
16-12-2020 at 10:32
by: clearly_not_atara
Acetic anhydride preparation
A variation on the succinic anhydride method, which was cool, but succinic acid isn't quite as easy ...
15-12-2020 at 15:29
by: clearly_not_atara
Questions about MPV reduction
[b]Opylation[/b]: Reduction with Mg will reduce the iodide.

[b]EverythingAl2O3[/b]: First of all, ...
13-12-2020 at 19:35
by: clearly_not_atara
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