Sciencemadness Discussion Board
Not logged in [Login ]
Go To Bottom

Search
[Next Page]
Sodium Metal from NaCl Reduction using Lead
what temps do you need to heat the mixes ( of say, NaOH/Pb ) to?
surely it would be difficult to fi ...
25-7-2008 at 14:38
by: Picric-A
Iodine preparation for who needs it
most people who want to use idoine know how to make it,
This video just educates meth cooks how to ...
25-7-2008 at 13:49
by: Picric-A
white phosphorous by accident???? HELP!
as with all phosphides, one used to be able to buy a 25kg back of calcium phosphide for about £5. n ...
25-7-2008 at 09:28
by: Picric-A
Silver Nitrate + Ethanol = Ethyl Nitrate?
lol soz my mistaque.
i sent the company an email and asked them to change it, i have just checked a ...
22-7-2008 at 15:34
by: Picric-A
white phosphorous by accident???? HELP!
cool, thanks.
soz admin about picture... i need to get me a new camera :P
22-7-2008 at 12:26
by: Picric-A
white phosphorous by accident???? HELP!
Today i was making some magnesium posphide the way i normally make calcium phosphide. This envolves ...
22-7-2008 at 08:13
by: Picric-A
Manufacture of sodium azide via hydrazine
yes i have made Hydrazine in the past using NaClO 14%.
here is a site describing th manufacture of ...
22-7-2008 at 03:43
by: Picric-A
Silver Nitrate + Ethanol = Ethyl Nitrate?
oh kk, this must be wrong then :P
http://www.saltlakemetals.com/MSDS_Silver_Oxide.htm
21-7-2008 at 12:18
by: Picric-A
The lead salts preparation thread!
yes then lead the NO2 fumes through water to regain the nitric used in the production of the Pb(NO3) ...
21-7-2008 at 12:14
by: Picric-A
H2SO4 by the Lead Chamber Process - success
are you sure phosphoric acid, HPO3, can dehydrate H2SO4? i thought only phosphorous pentoxide, P2O5, ...
21-7-2008 at 09:58
by: Picric-A
The lead salts preparation thread!
yea, you didnt heat it strong enough so it didnt seperate fully, hence the granular form
cant expla ...
21-7-2008 at 01:30
by: Picric-A
Practical guide for converting red P to white P
nice write up on a very difficult (not to mention dangerous :P) procedure!
your demos and your webs ...
20-7-2008 at 15:01
by: Picric-A
Silver Nitrate + Ethanol = Ethyl Nitrate?
ouch, improvised distillation apparatus whe dealing with explosives, be careful!
maybe a bit off th ...
20-7-2008 at 14:07
by: Picric-A
Found on eBay
lol if you buy it, expect a visit from the police :P
20-7-2008 at 13:59
by: Picric-A
Non-nitrate explosives
nitrogen halides, NI3 NCl3. very easy to make but sensitive as hell :P oh and nitrogen trichloride i ...
20-7-2008 at 13:57
by: Picric-A
Manufacture of sodium azide via hydrazine
After a bit of research i found that sodium azide could be made by reacting Sodium Nitrite with Hydr ...
20-7-2008 at 13:53
by: Picric-A
The lead salts preparation thread!
Was your lead glowing red hot? maybe there wasnt enough oxygen.
I normally make less than 50g at a ...
20-7-2008 at 13:36
by: Picric-A
Very Mild Chlorinating Reagents for Delicate Substrates
where do you get your N,N-simethylamide of isobutyric acid?
U2U me if you dont want to let it out, ...
20-7-2008 at 13:21
by: Picric-A
diethyl ether
as a source of EtOH i buy surgical spirits wich is available readily where i live.
It costs about  ...
20-7-2008 at 13:19
by: Picric-A
The lead salts preparation thread!
woops i think its a bit big :P soz admin!
20-7-2008 at 08:13
by: Picric-A
The lead salts preparation thread!
the picrtue shows the products of roasting lead at around 600 degrees C. I didnt do it for long enou ...
20-7-2008 at 08:10
by: Picric-A
The lead salts preparation thread!
It doesnt take long to convert to PbO however the lead forms a oxide layer wich you have to scape of ...
20-7-2008 at 07:20
by: Picric-A
The lead salts preparation thread!
this is a tiny bit of the topic.
Until now i have made my lead dioxide from a 3 way process.
First ...
20-7-2008 at 03:54
by: Picric-A
Can I store nitric acid safely?
I had a 1L bottle of i think 52% Nitric acid. I thought at this concentration it wouldnt release fum ...
18-7-2008 at 14:18
by: Picric-A
Cleaning crude DCM (from distillation)
burning the DCM MeOh mix (after purification) keeps comming to my head but i dont know how you would ...
18-7-2008 at 14:12
by: Picric-A
[Next Page]

  Go To Top