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Glycolic acid + HCl -> Chloroacetic acid
You think sodium glycolate is going to react with hydrochloric acid to give sodium chloroacetate ins ... |
29-12-2023 at 13:33
by: DraconicAcid |
N,N'-dimethyl ethylenediamine
The diamine is only needed as a counterion, so why not make it with a different one? The potassium ... |
28-12-2023 at 12:30
by: DraconicAcid |
Taurine metal salts
My taurine just arrived, so I'll be able to try some of these soon. |
28-12-2023 at 10:07
by: DraconicAcid |
2023 Science Madness Secret Santa – The fun begins!
W00T!!
Santa's delivery finally fought its way through Canada Post!
I got a nice bunch of chem ... |
27-12-2023 at 16:21
by: DraconicAcid |
2023 Science Madness Secret Santa – The fun begins!
Merry xmas, everyone! I'm relaxing with my kids tonight- maybe Santa will deliver something next we ... |
24-12-2023 at 18:23
by: DraconicAcid |
Which chlorine oxidants dissolve gold?
[rquote=689652&tid=159835&author=pneumatician]dissolve potassium nitrate in hcl & you ge ... |
23-12-2023 at 11:53
by: DraconicAcid |
Everyday Chemistry
I've got a paper here (https://tesla.pmf.ni.ac.rs/lgc/articles/40-1992.pdf ) that discusses the synt ... |
21-12-2023 at 14:02
by: DraconicAcid |
Disposing of Tollen's Reagent After Silver Mirror Reaction
I'd add enough reducing agent to precipitate all the silver as the metal, and recover it.
If you ... |
13-12-2023 at 14:14
by: DraconicAcid |
Kojic acid metal complexes
I did find an article about the chelating product of chlorokojic acid with ethylenediamine.
ETA: ... |
12-12-2023 at 22:50
by: DraconicAcid |
Synthesis of Ethyl ß-Naphtholate (Nerolin)
[rquote=689395&tid=23333&author=Texium]Not really. That’s a pretty typical trend for molec ... |
12-12-2023 at 12:24
by: DraconicAcid |
Kojic acid metal complexes
Cool idea. Since manganese tends not to form amine complexes, you could use ammonia as the base, so ... |
12-12-2023 at 08:10
by: DraconicAcid |
2023 Science Madness Secret Santa – The fun begins!
Still waiting patiently, both for SS stuff, and for the stuff I ordered for myself while shopping fo ... |
11-12-2023 at 14:21
by: DraconicAcid |
Synthesis of iron(III)-acetylacetonate
I've made copper(II) dibenzoylmethanide. It's a green powder, almost completely soluble in everythi ... |
9-12-2023 at 15:41
by: DraconicAcid |
Ammonia to Hydrogen (Ruthenium catalysis)
Haber is rolling over in his grave. |
8-12-2023 at 12:34
by: DraconicAcid |
Synthesis of iron(III)-acetylacetonate
We use FeCl3 in a Friedels-Craft reaction, and our lab manual reminds the students not to leave it s ... |
7-12-2023 at 14:15
by: DraconicAcid |
The Short Questions Thread (4)
PS- if you're looking to get crystals, rather than just purifying the compound, I believe double sal ... |
6-12-2023 at 17:00
by: DraconicAcid |
Some uncommon/precious metals
I'm waiting to hear back from someone who said they may have some ruthenium for me. If they don't, ... |
6-12-2023 at 16:25
by: DraconicAcid |
The Short Questions Thread (4)
The brown crud is from oxidation of iron(II) to iron(III), which happily precipitates as various for ... |
6-12-2023 at 14:52
by: DraconicAcid |
Synthesis of iron(III)-acetylacetonate
Very nice!! I always have trouble getting the right solvent for recrystallization of these things.
... |
6-12-2023 at 14:39
by: DraconicAcid |
Heating a round bottom flask
A sand bath isn't as effective as an oil bath, but better than an air bath, and less messy than an o ... |
6-12-2023 at 13:58
by: DraconicAcid |
Blood red substance dropping out of mixed metal ion solution
https://en.wikipedia.org/wiki/Chevreul%27s_salt |
4-12-2023 at 19:16
by: DraconicAcid |
New Europium complex?
Cool. I don't have any alkylpyridinium cations or triethylamine, but I do have tetramethylammonium ... |
4-12-2023 at 12:45
by: DraconicAcid |
New Europium complex?
[rquote=689163&tid=159991&author=unionised]I don't know if it's "new" or not, but it reminde ... |
4-12-2023 at 12:08
by: DraconicAcid |
Synthesis of Ethyl ß-Naphtholate (Nerolin)
I'm not sure it's the KOH wash that's getting rid of the naphthol, but the use of dichloromethane (i ... |
4-12-2023 at 11:59
by: DraconicAcid |
Taurine metal salts
I found this paper about taurinates:
https://journals.iucr.org/e/issues/2011/10/00/bx2374/bx2374 ... |
3-12-2023 at 14:58
by: DraconicAcid |
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