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Oxamide synthesis
I am now thinking that the white precipitate formed in the follow-up experiment is actually oxamide. ... |
27-5-2002 at 18:45
by: madscientist |
Oxamide synthesis
Very interesting...
I poured the contents of the flask from the follow-up experiment into a 500mL ... |
27-5-2002 at 10:29
by: madscientist |
Oxamide synthesis
On the subject of the follow-up experiment: the contents of the flask are now the color of orange so ... |
27-5-2002 at 08:27
by: madscientist |
Acetic anhydride preparation
I placed a few drops of the distilled liquid on a piece of aluminum foil. No visible bubbling, or au ... |
27-5-2002 at 08:26
by: madscientist |
Oxamide synthesis
I just tried to synthesize (CONH2)2 via the following method:
2CH3CH2OH + (COOH)2 --(H2SO4)--> (C ... |
26-5-2002 at 21:49
by: madscientist |
Acetic anhydride preparation
I'm not sure, but I think that it's possible that I prepared acetic anhydride by accident today. I m ... |
26-5-2002 at 21:18
by: madscientist |
Toxic-gas liberating explosives
I have no idea why I asked that question. *smacks forehead*  |
26-5-2002 at 06:56
by: madscientist |
Dinitrodimethyl oxalate
Whoops! I forgot about this! The NO2 group resonates between the nitro and the nitrite structure! Th ... |
26-5-2002 at 06:40
by: madscientist |
Chloroacetic acid...
Whoops! I forgot about this! The NO2 group resonates between the nitro and the nitrite structure! Th ... |
26-5-2002 at 06:31
by: madscientist |
Dinitrodimethyl oxalate
Something that has just occurred to me: (COOCH2NO2)2 could be used to prepare CH2NO2OH! CH2NO2OH sho ... |
25-5-2002 at 20:55
by: madscientist |
Dinitrodimethyl oxalate
Since I unfortunately do not have any methanol on hand, I have begun preparing isopropyl oxalate, wh ... |
25-5-2002 at 19:35
by: madscientist |
Toxic-gas liberating explosives
Exactly how does it decompose (equation please)?  |
25-5-2002 at 14:09
by: madscientist |
Picramic acid synthesis
I have no detailed information on preparing picramic acid. Does anyone have information to share? Th ... |
25-5-2002 at 11:16
by: madscientist |
Dinitrodimethyl oxalate
It's my own idea. If the following doesn't happen, then I believe the nitration
of the methyl gro ... |
25-5-2002 at 10:54
by: madscientist |
Chloroacetic acid...
I'll share most of what my chemical dictionary has to say on the topic of chloroacetic acid (just wh ... |
25-5-2002 at 10:48
by: madscientist |
Dinitrodimethyl oxalate
I believe that dinitrodimethyl oxalate would be a fairly powerful, and fairly sensitive, energetic c ... |
24-5-2002 at 22:19
by: madscientist |
Nitric acid stills
Latest yield: 76%. I was not able to complete the distillation due to time constraints, enforced by ... |
24-5-2002 at 19:32
by: madscientist |
Preparation of cyclic-ketone compounds
I do know that when H2SO4 is added to CH3CHO, the trimer of CH3CHO, (CH3CHO)3, is catalytically form ... |
23-5-2002 at 20:22
by: madscientist |
Ammonium permanganate preparation
Well, the reactions posted in the post directly above have spelt the end of the ammonium permanganat ... |
22-5-2002 at 17:40
by: madscientist |
Carbamide Peroxide
Carbamide peroxide CO(NH2)2*H2O2
Properties: White crystals or crystalline powder; melting point ... |
22-5-2002 at 17:27
by: madscientist |
Toxic-gas liberating explosives
Here are a few energetic compositions that would release toxic gasses, and would be very simple to p ... |
22-5-2002 at 17:18
by: madscientist |
Trinitrotoluene preparation
[quote][b]Mr. Cool[/b]: There is also a method similar to the aspirin method for TNP. I haven't trie ... |
21-5-2002 at 16:41
by: madscientist |
Trinitrotoluene preparation
Could you share information on how to tell if runaway nitration is imminent, such as runaway nitrati ... |
21-5-2002 at 16:39
by: madscientist |
Trinitrotoluene preparation
I no longer have Megalomania's instructions for preparation of TNT on my hardrive (computer crashed) ... |
21-5-2002 at 16:37
by: madscientist |
Organic peroxides
Here's a good opportunity for this:
I'm theorizing that CH2O could be prepared from CH2Cl2 and NaOH ... |
21-5-2002 at 16:30
by: madscientist |
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