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Picric Acid and the Mystery of the Red Goo
Well, a total of 2.2g of binder - the binder being composed of starch and dicalcium phosphate - shou ... |
21-6-2002 at 13:49
by: madscientist |
Picric Acid and the Mystery of the Red Goo
Today I attempted to prepare picric acid. I used non-purified aspirin tablets. Each contained 0.325g ... |
20-6-2002 at 19:23
by: madscientist |
Nitrating with NH4NO3 and HCl
I highly doubt it will work. |
17-6-2002 at 12:47
by: madscientist |
Ammonium permanganate preparation
I would think it would; but not nearly as well as the method I posted previously.  |
15-6-2002 at 10:46
by: madscientist |
Organic chlorinations
Has anyone successfully carried out an organic chlorination? I recently attempted to chlorinate acet ... |
14-6-2002 at 17:09
by: madscientist |
Ammonium permanganate preparation
Here's a way of preparing high-purity NH4MnO4 that has been tested, and works. Simply mix a stoichem ... |
14-6-2002 at 13:11
by: madscientist |
Eliminating NO2 from HNO3
Purging NO2 from HNO3 with oxamide doesn't work. Details have been posted in the nitroxamide thread, ... |
7-6-2002 at 16:06
by: madscientist |
Nitroxamide
I believe I have stumbled upon a superior method of preparing dinitroxamide. I was attempting to use ... |
7-6-2002 at 16:00
by: madscientist |
Tsk, tsk.
Firstly, I'd like to thank Pu239 Stuchtiger for valiantly attempting to give due credit.
Secondly ... |
5-6-2002 at 14:38
by: madscientist |
Carbamide Peroxide
I just realized I forgot to say this: carbamide peroxide is not explosive.
By the way, it should ... |
5-6-2002 at 14:17
by: madscientist |
Acetaldehyde synthesis
I have more to say:
CH3CHO can also be prepared by the dehydrogenation of CH3CH2OH. I think there ... |
4-6-2002 at 12:00
by: madscientist |
oxidation of acetone
I'd just like to clarify on my post: when I spoke of oxidation of acetone being difficult, I was ref ... |
4-6-2002 at 11:52
by: madscientist |
Preparation of perchlorates
It doesn't seem right that MnO2 is formed as a product; I'm not sure though, it's possible. Do you h ... |
4-6-2002 at 11:47
by: madscientist |
Acetaldehyde synthesis
Sorry plasma, that won't work; organic chemistry isn't as straightforward as inorganic. :-/
Nick, ... |
4-6-2002 at 11:39
by: madscientist |
Eliminating NO2 from HNO3
I'm fairly certain these equations occur:
2NO2 + H2O --> HNO3 + HNO2
Nitrous acid is unstable, a ... |
2-6-2002 at 14:48
by: madscientist |
Oxamide nitrate
Hm, seems that oxamide nitrate isn't as sensitive as I predicted! I was smacking little piles of it ... |
2-6-2002 at 14:21
by: madscientist |
Anhydrous ammonia preparation
The reason for using the sulfate is the fact that sodium sulfate is a dessicant. |
2-6-2002 at 14:15
by: madscientist |
Anhydrous ammonia preparation
I have considered various possibilities for preparing anhydrous ammonia. Here are the best ideas:
... |
2-6-2002 at 11:59
by: madscientist |
Preparation of ionic nitrites
I have been looking into various methods outside of the NaNO3/Pb method for preparing sodium nitrite ... |
2-6-2002 at 09:57
by: madscientist |
oxidation of acetone
Oxidation of acetone is very difficult; even agents like KMnO4 will not oxidize it. The reason is be ... |
2-6-2002 at 08:19
by: madscientist |
Nitromethane extraction
When I heard "distillation" from you, I was thinking of you heating nitromethane with a propane burn ... |
29-5-2002 at 15:47
by: madscientist |
Oxamide synthesis
I tried preparing oxamide again today.
I placed 20.3g (COOH)2*2H2O in a flask. I added 34.3g CH3O ... |
28-5-2002 at 18:33
by: madscientist |
Methyl Ethyl Ketone Peroxide
After some thought, I now believe that the solid form of methyl ethyl ketone peroxide is actually (C ... |
28-5-2002 at 12:06
by: madscientist |
Eliminating NO2 from HNO3
I have heard that urea, CO(NH2)2, removes NO2 from HNO3. I have also found out from my own experienc ... |
28-5-2002 at 11:48
by: madscientist |
Oxamide nitrate
Today I prepared a small quantity of oxamide nitrate. I took 2.1g of (CONH2)2, and placed it in 25mL ... |
27-5-2002 at 18:53
by: madscientist |
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