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Salicylic acid
I would rather use bicarbonate as a base, phenol does react with carbonates to some extent....
... |
3-8-2008 at 14:46
by: Klute |
Problem with monomethylation of amines.....
I'm currently doing the workup 
Will report results when finished!
BTW, the CTH product gave ... |
2-8-2008 at 14:29
by: Klute |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
It seems LiAlH4 doesn't generally cause debenzylation, so that should be possible.
A note on the ... |
2-8-2008 at 08:41
by: Klute |
Laundry detergent?
I think sodium percarbonate is the most common bleaching agent used. Perborate is fairly common too. ... |
1-8-2008 at 19:13
by: Klute |
What reagent would you like to see an illustrated guide for?
I'm getting fairly intereste din diborane too, but there isn't much to it experimentally speaking, i ... |
1-8-2008 at 16:45
by: Klute |
What reagent would you like to see an illustrated guide for?
[quote] even proper labs might have trouble running a research program with that price. What do peop ... |
1-8-2008 at 09:53
by: Klute |
TEMPO substitute?
Thanks alot
Indeed, the acetals weren't something I focused on, but do look promising. there a ... |
1-8-2008 at 09:34
by: Klute |
Oxidation of phenethylamine to (2-nitroethyl)benzene
That's not possible in a one step reaction, and I highly doubt it's possible.
Addition of formald ... |
31-7-2008 at 15:41
by: Klute |
Acetophenones from benzaldehydes?
Thank you for the details ziqquratu, it would be great to have the the opinion of people regularily ... |
31-7-2008 at 00:32
by: Klute |
Whaddya do with the waste?
I'ev just checke dthe SM library, and I'm surprised to see no book on the subject. Pretty surprising ... |
30-7-2008 at 15:36
by: Klute |
Whaddya do with the waste?
Well, there are few at work, I will get the exact titles, but it's along the lines of this:
"Haza ... |
30-7-2008 at 15:30
by: Klute |
Whaddya do with the waste?
I seperate my waste in different types: the "clean" aqueous goes in a jerrican to be emptied in the ... |
30-7-2008 at 15:15
by: Klute |
What reagent would you like to see an illustrated guide for?
Indeed, a hydrogeantion apparatus would be very usefull! But considering the hazard, i think that th ... |
29-7-2008 at 18:30
by: Klute |
Drying oxalic acid
Thanks for all your replies; I can't beleive I didn't find the orgsyn preparation....
I think i ... |
29-7-2008 at 18:23
by: Klute |
Drying oxalic acid
I woul dlike to dry commercial oxalic acid dihydrate to anhydrous. My first thought was drying it in ... |
29-7-2008 at 15:27
by: Klute |
What reagent would you like to see an illustrated guide for?
A low-pressure hydrogenation apparatus is a good idea, I'm starting to make a fewplans on making on ... |
29-7-2008 at 04:57
by: Klute |
Question: Red phosphorus purification
Out of curiosity, is there any solvent in which red phosphorus is soluble? CS2 maybe? |
28-7-2008 at 07:45
by: Klute |
A few of questions about HCl(aq.)
and if you want to titrate the obtained solution, dilute them to 0.1-0.5 N, with conc. solution you ... |
28-7-2008 at 06:21
by: Klute |
Problem with monomethylation of amines.....
Trying out the freifelder hydrogenation, with >1g of 10% Pd/C at the 100mmol scale, the H2 uptake ... |
28-7-2008 at 06:01
by: Klute |
A few of questions about HCl(aq.)
The yellow impurity is most likely Fe3+ contamination, but of very slight contamination. In a number ... |
28-7-2008 at 05:54
by: Klute |
law in France
This is the most revelant document I have found regarding european law on precursors, but indeed not ... |
27-7-2008 at 05:59
by: Klute |
VERY strange electrolysis results?
Did the white component start appearing immeidatly at the beggining of the electrolysis? Or was ther ... |
27-7-2008 at 05:42
by: Klute |
Ethyl/Isopropyl Bromide preparation
Thanks alot for sharing Smuv, very interesting read. Alkyl halides are very usefull reagents and det ... |
27-7-2008 at 05:36
by: Klute |
Problem with monomethylation of amines.....
I tried the HCHO/Zn reductive methylation on a preparative scale, 100mmol, and it didn't work out we ... |
26-7-2008 at 17:10
by: Klute |
possible conversion of alkyl phoshite to iodide?
Why not use directly HI rather than precious PCl3? There are lots of ways of preparing alkyl iodides ... |
26-7-2008 at 17:05
by: Klute |
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