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Diethylamine Hydrochloride Synthesis
I finally got round to distilling the free diethylamine from my hydrochloride. The distillation was ...
17-11-2019 at 05:11
by: Boffis
OTC pyrazole synthesis
@ Nitrogenes, did you ever get any further with your pyrazole project?

I have found an interestin ...
14-11-2019 at 02:16
by: Boffis
Synthesis of Boron subphthalocyanine chloride (with pictures!)
Nice work numos and I love those colours!

A couple of question I have, 1) why is BCl3 used in equ ...
11-11-2019 at 08:36
by: Boffis
Suggestions for experiments with Dimethyl glyoxime
Dehydration and cyclitisation with NaOH solution yields dimethylfurazan. This can be oxidized to the ...
8-11-2019 at 07:53
by: Boffis
Preparation of cinnamalacetone
@UC235, its interesting that in the Ozone lab prep they acidify the reaction medium after completion ...
29-10-2019 at 13:14
by: Boffis
Preparation of cinnamalacetone
Another question! In the link posted by UC235 above the description gives an amount of NaOH to be us ...
28-10-2019 at 08:11
by: Boffis
Synthesis of a Highly Fluorescent Boron subporphyrazine
Hi Nimos, Keep us posted on how you get on I have lots of o-cyanobenzene too!
28-10-2019 at 04:46
by: Boffis
Synthesis of a Highly Fluorescent Boron subporphyrazine
Very nice preparation, pitty I don't have any BCl3 or I would have a go too. I have benzil and diami ...
27-10-2019 at 10:28
by: Boffis
Preparation of cinnamalacetone
UC235 many thanks for that link. This will be very helpful for the disubstituted acetones I am goin ...
26-10-2019 at 04:07
by: Boffis
What real life mineral is the closest to minecraft redstone, except for the colour?
Apart from native copper there are nickeline (NiAs), briethauptite (NiSb) and melonite (NiTe2). The ...
25-10-2019 at 14:52
by: Boffis
Preparation of cinnamalacetone
Has anyone on this board ever prepared cinnamyl acetone? I am trying to prepare this compound in the ...
25-10-2019 at 14:42
by: Boffis
Distilled, De-ionised or Tap water?
Hi RedDwarf, sorry I got confused between you and artemov's posts. Here in the NW of England there i ...
24-10-2019 at 09:40
by: Boffis
Distilled, De-ionised or Tap water?
I see you have water very similar to ours and don't live too far away! I use tap water only to wash ...
24-10-2019 at 03:13
by: Boffis
What journal is this?
Yes thats why I will have to contact the the institution to see if I can persuade them to supply me ...
23-10-2019 at 13:45
by: Boffis
What journal is this?
I don't have a title but it is referenced as containing the preparation of various substituted aryla ...
23-10-2019 at 11:43
by: Boffis
What journal is this?
Many thanks guys. Looks like I will have to contact them to see if I can get a copy.
23-10-2019 at 09:21
by: Boffis
What journal is this?
I am trying to track down this reference:

J. H. Yoe; Va. J. Sci.; v3; p8-10; 1942

but what doe ...
23-10-2019 at 07:10
by: Boffis
Should 99.99% mercury contain slag? [Update from seller]
10% nitric acid attacks mercury rather slowly, the oxide dissolves almost instantly. By the time the ...
21-10-2019 at 09:26
by: Boffis
Ferrous tartarate
Many thanks Waffles. Interestingly I have already used two of the methods and got what appear to be ...
21-10-2019 at 02:13
by: Boffis
Diethylamine Hydrochloride Synthesis
[rquote=624665&tid=24131&author=draculic acid69]You could turn the toluic acid into toluene ...
20-10-2019 at 08:23
by: Boffis
Ferrous tartarate
Has anyone ever tried to prepare ferrous tartarate? I want some as a catalyst for a Fenton type oxid ...
20-10-2019 at 02:09
by: Boffis
Diethylamine Hydrochloride Synthesis
I have now tried to recrystallise the better m-touic acid from the larger scale hydrolysis experimen ...
19-10-2019 at 14:18
by: Boffis
Chemistry of Terephthalic acid
@Fulmen; I am not sure what you are getting at but I don't think that evaporating terphthalic acid s ...
19-10-2019 at 13:43
by: Boffis
silicon carbide from old abrasive paper ("sand" paper)
Can't you just buy the silicon carbide? I use it for polishing rock slabs and its dirt cheap. You ca ...
19-10-2019 at 01:23
by: Boffis
Should 99.99% mercury contain slag? [Update from seller]
Even the purest mercury oxidizes slowly and more importantly absorbs sulphur from the atmosphere. Su ...
19-10-2019 at 01:16
by: Boffis
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