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Organic substitutions
I found those reactions in my inorganic chemistry textbook.
8-8-2002 at 18:37
by: madscientist
N10O5 - A compound of mind-boggling power
Are you sure? I played with a model of it, and the molecule didn't seem to be as strained as acetone ...
8-8-2002 at 18:32
by: madscientist
Preparation of ionic nitrites
The theoretical yield was about 16.2g of NaNO2. I managed to scrape about 11g of NaNO2 off of the bo ...
7-8-2002 at 12:48
by: madscientist
Rust stain remover H3PO4
My H3PO4 is a thick, syrupy liquid. According to my references, H3PO4 that is a thick, syrupy liquid ...
6-8-2002 at 21:40
by: madscientist
Preparation of ionic nitrites
I made some sodium nitrite today. This is the process I used:

2HSO3NH2 + 2CaO + 3NaNO3 ----> 2CaS ...
6-8-2002 at 21:20
by: madscientist
Rust stain remover H3PO4
Does anyone know the concentration of the "rust stain remover" type H3PO4 that is found at hardware ...
6-8-2002 at 11:10
by: madscientist
Preparing alkali amides
I would think that it would be possible to prepare NaN3 from NaNH2 and NaNO2 using CH3COCH3 as a sol ...
5-8-2002 at 15:32
by: madscientist
Preparing alkali amides
Everyone knows about the standard process for preparing sodium amide: passing anhydrous ammonia over ...
4-8-2002 at 16:07
by: madscientist
Picric Acid and the Mystery of the Red Goo
I think that the Red Shit is actually picric acid anhydride. That would explain all of its propertie ...
27-7-2002 at 21:49
by: madscientist
Extracting Sodium from Sodium Chlorate
I don't know much about this, but these are my best guesses for what should be used:

-low voltage ...
25-7-2002 at 08:06
by: madscientist
Photos
I just got access to a highly-trusted friend's digital camera. I have taken some photos. Here's a li ...
24-7-2002 at 19:36
by: madscientist
Extracting Sodium from Sodium Chlorate
Sodium hydroxide is sold at hardware stores - it is sold for cleaning out problematic plumbing. It's ...
9-7-2002 at 18:26
by: madscientist
Extracting Sodium from Sodium Chlorate
The only realistic route to preparing sodium metal is electrolysis of a molten sodium compound in an ...
9-7-2002 at 09:03
by: madscientist
Reducing organic peroxides.
Today I attempted to reduce liquid methyl ethyl ketone peroxide with sodium sulfite, in solution. I ...
8-7-2002 at 21:46
by: madscientist
N10O5 - A compound of mind-boggling power
N10O5 would be an explosive compound of ridiculous power. The structure is two five-membered nitroge ...
8-7-2002 at 21:36
by: madscientist
Organic substitutions
It is possible to carry out organic substitutions with considerable ease when using an electric curr ...
7-7-2002 at 18:33
by: madscientist
Reaction of CH3OH with NH3
Does anyone know for certain what happens? This is my current hypothesis:

CH3OH + NH3 ----> CH3NH ...
7-7-2002 at 18:10
by: madscientist
Nitration
Well, add potassium metal to 100% white nitric acid...
7-7-2002 at 10:15
by: madscientist
Shocking!
[url]http://www.roguesci.org/cgi-bin/ewforum/ultimatebb.cgi?ubb=search_tng;d=results;record=2452462- ...
6-7-2002 at 11:09
by: madscientist
Locating Equipment
This supplier is excellent (I buy everything from them): www.sciplus.com

A good supplier of disti ...
5-7-2002 at 18:13
by: madscientist
Shocking!
Uh, the link doesn't seem to work...
5-7-2002 at 14:55
by: madscientist
Purification of acetone peroxide
I thought it would be an interesting challenge to attempt to prepare reasonably pure trimeric aceton ...
4-7-2002 at 21:06
by: madscientist
Methylamine question
This synthesis sounds feasible:

[QUOTE]
Methylamine Hydrochloride from HMTA, Eleusis' version [w ...
4-7-2002 at 20:47
by: madscientist
Nitrating with NH4NO3 and HCl
Hydrogen fluoride is extremely toxic.
25-6-2002 at 09:34
by: madscientist
Preparation of nitrostarch
I have found that the runaway nitration temperature for nitrating starch in concentrated mixed acid ...
24-6-2002 at 11:01
by: madscientist
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