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Chemical Isolation of Fluorine
Heat PbF4 to about 100C and it should liberate F2.
31-8-2002 at 09:48
by: madscientist
Ammonium Nitrate and detonation
Don't worry, you're not being annoying. :)

You've got those examples right. Here's a few examples ...
30-8-2002 at 22:05
by: madscientist
Does sulfur monoxide exist?
I just purchased an advanced inorganic chemistry textbook. Here's what it says.

[i]The lower oxid ...
30-8-2002 at 22:01
by: madscientist
Ammonium Nitrate and detonation
I'll write an explanation of the basics of explosives. :)

Low explosives explode by burning very ...
30-8-2002 at 21:28
by: madscientist
Ammonium Nitrate and detonation
Oh sorry, I didn't read your post carefully enough. You aren't going to find an ammonium nitrate mix ...
30-8-2002 at 19:20
by: madscientist
Ammonium Nitrate and detonation
By the way, ANNM is actually supposed to be quite easy to detonate. There are some more sensitizers ...
30-8-2002 at 19:18
by: madscientist
Hypobromite?
[QUOTE] It could be one of two liquids: COBr2 or C(N)2[/QUOTE]

I meant to write CO(N)2.
30-8-2002 at 17:06
by: madscientist
Hypobromite?
The mass is still unchanged.

I think this experiment may answer the question of how hypochlorites ...
30-8-2002 at 16:27
by: madscientist
Hypobromite?
It is now a wet, gunky mix, that contains solids. It seems that the bromination of the urea has form ...
30-8-2002 at 15:09
by: madscientist
Hypobromite?
I went back outside and checked on it. It was solidified, still a deep orange, and dry. I added 1g o ...
30-8-2002 at 14:24
by: madscientist
Hypobromite?
I just got done with an experiment a few minutes ago. Here's what I did and what happened.

I mixe ...
30-8-2002 at 14:04
by: madscientist
Chemical Isolation of Fluorine
Er, you can't oxidize HF to liberate F2. Fluorine is, after all, the most electronegative element. H ...
29-8-2002 at 21:10
by: madscientist
Trinitrotoluene preparation
I just discovered that the temperature where the reaction between toluene and highly concentrated mi ...
27-8-2002 at 16:42
by: madscientist
Trinitrotoluene preparation
How are polynitrotoluenes synthesized?
27-8-2002 at 14:02
by: madscientist
Preparation of elemental phosphorus
Vulture mentioned in another thread that CaC2 would make a good reducing agent in such a reduction a ...
24-8-2002 at 16:50
by: madscientist
Photos
I thought that salicylic acid decarboxylated when strongly heated.

HOC6H4COOH ----> C6H5OH + CO2

I ...
24-8-2002 at 15:14
by: madscientist
Metal nitrates - the easy way
Wouldn't the easiest route to, say, Ca(NO3)2, be reacting Ca(OH)2 directly with NH4NO3?

Ca(OH)2 + 2 ...
22-8-2002 at 16:50
by: madscientist
Does sulfur monoxide exist?
Does sulfur monoxide exist? I haven't seen any mention of it anywhere.
21-8-2002 at 11:09
by: madscientist
NO2 preparation
I'm looking for cheap routes of preparing NO2 gas. Cu + HNO3 is expensive, as is nitrite + acid. So ...
21-8-2002 at 09:49
by: madscientist
Organic peroxides
I have attempted to prepare acetaldehyde peroxide using H2O2, acetaldehyde, and H2SO4. It failed, pr ...
20-8-2002 at 17:38
by: madscientist
Preparation of ionic nitrites
I added a small amount of my product from the sulfamic acid process to a sulfuric acid solution (abo ...
9-8-2002 at 17:44
by: madscientist
N(NN)3N
NCl3 + 3KN3 ----> N(N3)3 + 3KCl

N2H4 + 4Cl2 ----> N2Cl4 + 4HCl
N2Cl4 + N2H4 ----> N4 + 4HCl

N ...
8-8-2002 at 19:06
by: madscientist
A remarkable discovery...
Haha, something is terribly messed up with the board software. But I'm not about to reinstall it - t ...
8-8-2002 at 18:55
by: madscientist
N(NN)3N
This compound would liberate approximately 2.55 times as much energy per gram as ethylene glycol din ...
8-8-2002 at 18:52
by: madscientist
A remarkable discovery...
I think vulture was thinking of tossing CaC2 into a large quantity of H2O.

CaC2 + H2O ----> CaO + ...
8-8-2002 at 18:43
by: madscientist
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