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Vanillin ring closure
....Am I missing something? What does confidence have to do with this? I am well aware of the fact t ...		 2-2-2020 at 18:22
by: njl
Vanillin ring closure
I'd like to preface this by saying my question definitely relates to cookery so it should be moved a ...		 2-2-2020 at 17:35
by: njl
Extension of the Eschweiler-Clarke alkylation
Thanks. Why exactly can't longer acids be oxidized?

Edit: I don't suppose the addition of someth ...		 2-2-2020 at 11:52
by: njl
Extension of the Eschweiler-Clarke alkylation
Why can't the EC alkylation be performed with longer main-chain acids? The procedure calls for Formi ...		 2-2-2020 at 11:03
by: njl
Acetic anhydride preparation
[rquote=630331&tid=9&author=Tsjerk][rquote=630330&tid=9&author=DavidJR]Ozone + acety ...		 31-1-2020 at 10:36
by: njl
Acetic anhydride preparation
2 Ideas:

Ozonolysis of acetylene

"Decomposition" of acetate salt

I know Wikipedia isn't ne ...		 31-1-2020 at 07:20
by: njl
Ispropyl Nitrite synth now requires heating?
Can you outline the thermal decomposition to nitrite? I've seen several threads on here with conflic ...		 13-1-2020 at 14:57
by: njl
Sulfuric Acid from Sulfate Salts and Oxalic acid?
I'm happy to see someone in the same boat as me! As a beginner it was also hard for me to get my han ...		 3-1-2020 at 08:10
by: njl
O-Cresol from Salicylic acid

[quote]
o-toluidine -> o-cresol
[/quote]

This is interesting. I found a report on orgsynth ...		 27-12-2019 at 08:17
by: njl
O-Cresol from Salicylic acid
To the point: Can I reduce salicylic acid to cresol or will I just end up with a bunch of phenols?
...		 26-12-2019 at 12:30
by: njl
An odd smell from some acetone
[rquote=627066&tid=154497&author=TheMrbunGee]
Or maybe Your hotplate is the source of smell ...		 29-11-2019 at 09:34
by: njl
An odd smell from some acetone
[rquote=627031&tid=154497&author=TheMrbunGee]Just had to check: are You sure the caffeine sm ...		 28-11-2019 at 18:48
by: njl
An odd smell from some acetone
The acetone is from a fresh jug of klean strip acetone. Just did a little test with some straight fr ...		 28-11-2019 at 10:02
by: njl
An odd smell from some acetone
I'm in the process of recrystallizing some caffeine in warm acetone and it is giving off a very stro ...		 28-11-2019 at 08:18
by: njl
What would the procedure for Benzidine to aniline look like?
Thanks. I wasn't planning on using it in any particular reaction, just wondering if there was a know ...		 26-11-2019 at 15:24
by: njl
What would the procedure for Benzidine to aniline look like?
Is is silly to assume a one step conversion in an acidic solution is possible?

Edit: On a tangen ...		 26-11-2019 at 13:33
by: njl

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