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bromate synthesis
The only process I have any real confidence in is electrolysis of an aqueous solution of a bromide.
... |
2-10-2002 at 13:22
by: madscientist |
Eliminating NO2 from HNO3
H2O2 did remove NO2 from yellow HNO3.
I'm guessing th ... |
28-9-2002 at 08:43
by: madscientist |
Phenol
Benzene can also be prepared from toluene and anhydrous aluminum trichloride. |
27-9-2002 at 04:17
by: madscientist |
peroxide_nitramine?
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26-9-2002 at 20:09
by: madscientist |
Glycerol to Propionic Acid: A Chemical Safari Tour.
[b]Excellent[/b] post!  Thank you very much for sharing the mechanism of that
reaction in such det ... |
26-9-2002 at 09:06
by: madscientist |
Hopelessly gunked up reaction vessels
I recently tried to prepare CS2 from charcoal and sulfur, and for whatever reason I'm not able to co ... |
25-9-2002 at 09:02
by: madscientist |
Acetic anhydride preparation
I think that reaction chloroacetic acid with sodium acetate would yield CH3COOCH2COOH, not acetic an ... |
25-9-2002 at 08:51
by: madscientist |
Diphoronepentaperoxide (DPPP)
I added 50mL of 27.5% H2O2, after letting the phorone solution cool to 25C. The temperature jumped t ... |
23-9-2002 at 20:17
by: madscientist |
Success with phorone preparation!
I mixed 35mL of 31% HCl with 25mL of CH3COCH3, and held the temperature at 0C for two hours. Since n ... |
23-9-2002 at 20:05
by: madscientist |
Phenol
I haven't gotten around to doing a titration to see if this really did work, but here's my idea. Hyd ... |
23-9-2002 at 14:35
by: madscientist |
Sulfur chlorides preparation
Whatever it may be, it does not react violently with water. I added a piece of it to 200mL of water ... |
23-9-2002 at 13:56
by: madscientist |
Sulfur chlorides preparation
It has completely solidified - it didn't seem to take too long for that to happen. The solid is a ve ... |
23-9-2002 at 13:37
by: madscientist |
Sulfur chlorides preparation
I forgot to mention the reaction that I think occurred.
CuCl2 + 3/8S8 ----> ... |
22-9-2002 at 20:05
by: madscientist |
Sulfur chlorides preparation
Today I attempted to prepare sulfur chlorides, more specifically, S2Cl2. Polve ... |
22-9-2002 at 20:02
by: madscientist |
Extracting Sodium from Sodium Chlorate
What I meant by "potassium is too reactive" is that the potassium metal likely is being oxidized on ... |
22-9-2002 at 08:30
by: madscientist |
Extracting Sodium from Sodium Chlorate
The reason your potassium metal attempt failed could also be because potassium metal is significantl ... |
21-9-2002 at 14:02
by: madscientist |
Seriously
That's almost certainly "IamGod". He's been using some Chinese proxy recently. He's some random moro ... |
20-9-2002 at 18:21
by: madscientist |
Nitrosyl Perchlorate
HNO3 is dehydrated to N2O5, an unstable crystalline solid.
When ... |
20-9-2002 at 12:43
by: madscientist |
Nitrosyl Perchlorate
Never mind, the equation IS balanced, for some reason I was seeing 2ONClO4 but thinking 2O2NClO4.... |
19-9-2002 at 16:06
by: madscientist |
Nitrosyl Perchlorate
Uh, your equation isn't balanced. 
I would think that perchloric acid would be dehydrated by su ... |
19-9-2002 at 16:03
by: madscientist |
Nitrosyl Perchlorate
Nitrosyl chloride, NOCl, is formed by reacting HNO3 with HCl. I suppose that the reaction proceeds l ... |
19-9-2002 at 15:30
by: madscientist |
Seriously
No, he's not directing that comment towards you, Psycho. Stick around. He's
referring to people l ... |
19-9-2002 at 15:24
by: madscientist |
Diphoronepentaperoxide (DPPP)
About two-thirds of the way through this thread there is an attempt to synthesize acetone peroxide t ... |
18-9-2002 at 18:25
by: madscientist |
Greetings
Welcome to sciencemadness.
I believe this is how the reaction proceeds.
NaNO2 + HCl ----> N ... |
17-9-2002 at 14:42
by: madscientist |
Diphoronepentaperoxide (DPPP)
Phorone dissolves in alcohol. It's essentially insoluble in water. |
16-9-2002 at 15:55
by: madscientist |
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