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ortho nitration of p-toluenesulfonic acid(QUESTIONS)
I don't remember the yield but I left the solution of dcm/HNO3/toluene stirring overnight (probably ... |
14-6-2020 at 10:27
by: njl |
Nitrogen Triiodide HELP ME!
What on earth does WTSUFHN mean? |
14-6-2020 at 07:19
by: njl |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
I just tried the dcm nitration and I honestly have never seen something so beautiful. No thermal run ... |
14-6-2020 at 07:16
by: njl |
Most toxic compound OTC?
Salvinorin is potent but as you said there's basically no data that I've seen on its toxicity so it ... |
14-6-2020 at 07:09
by: njl |
barrels of solvent, not many uses... any ideas?
Lucky! like drac suggested you could hydrolyze the ether to ethylene glycol and butanol (both useful ... |
3-6-2020 at 04:45
by: njl |
Most toxic compound OTC?
Many insecticides, radioisotopes, alkaloids, and commodity chemicals. Sodium isocyanate (pool chemic ... |
23-5-2020 at 10:34
by: njl |
Question - C and MnO2 separation
If the mush isn't contaminated with anything too harmful, I would think hitting it with a torch in o ... |
19-5-2020 at 18:45
by: njl |
Piperazine workup
Hi all. After doing some reading on the use of amines as proton sponges, I thought I'd try a typical ... |
17-5-2020 at 10:50
by: njl |
5-MEO-DMT struggle
Ah yes, the funeral store. My favorite place for otc formaldehyde. |
17-5-2020 at 10:39
by: njl |
Alternative Solvents and New Solvents - General Discussion
I agree dcm is great. I bought a liter for pretty cheap but now my only way is to distill from paint ... |
12-5-2020 at 05:32
by: njl |
Alternative Solvents and New Solvents - General Discussion
@fusso I have about 400 ml of dcm left, it's pretty hard for me to get but very precious |
12-5-2020 at 03:09
by: njl |
Alternative Solvents and New Solvents - General Discussion
This is a topic I'm very interested in. Whenever I get to thinking about solvents I feel like I'm at ... |
10-5-2020 at 18:01
by: njl |
Cryo Refrigerated Well ... thingy
Cryogenic cooling. I remember applied science using a real cryo machine in his anhydrous ammonia vid ... |
10-5-2020 at 17:18
by: njl |
Anthranilic acid preparation(questions)
Hey @B.D.E: I don't use retail bleach solutions because they tend to degrade over short periods of t ... |
7-5-2020 at 08:02
by: njl |
Cheap, interesting elements/compounds to buy?
@Draeger please let me know how to accidentally create boranes because that sounds like a useful ski ... |
6-5-2020 at 19:29
by: njl |
Large Scale Iron Oxide Synthesis
I think the quick solution to both problems would be to allow it to completely air-dry, then sift in ... |
28-4-2020 at 08:59
by: njl |
Dibenzalacetone - Organic Synthesis writeup
@vibbzlab I have a bit of piperonal with your name on it if you'd like. Might be useful for opening ... |
28-4-2020 at 08:52
by: njl |
TCCA purification, strange things happen
I'm not too aware of the process, but I don't think any appreciable amount of Chloroacetone was form ... |
28-4-2020 at 08:50
by: njl |
sodium borohydride
u2u me |
4-4-2020 at 10:49
by: njl |
Leuckart reaction with oxalic acid
I agree the Cannizzaro reaction looks better. I don't have any experience with it which is why I did ... |
31-3-2020 at 09:09
by: njl |
Leuckart reaction with oxalic acid
@All thank you for responses.
@Atara depends on where you are/what you have but basically hydroly ... |
31-3-2020 at 07:22
by: njl |
Leuckart reaction with oxalic acid
Would oxalic acid work as a substitution for formic acid as a reducing agent in the leuckart reactio ... |
30-3-2020 at 07:27
by: njl |
Formamide from urea
@Atara thank you for the feedback. I agree that reduction in basic conditions is unlikely to be a vi ... |
27-3-2020 at 17:26
by: njl |
Formamide from urea
[b]Background[/b]: Was bored. Have 5 pounds of urea. Have no formamide.
[b]Theory[/b]: A well kno ... |
27-3-2020 at 13:09
by: njl |
Several interesting reactions
im guessing the dark precipitate from Mn and Ag is superfine manganese or silver oxide (or both) |
25-3-2020 at 07:32
by: njl |
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