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Toxic-gas liberating explosives
Wouldn't ammonia be one of the products of the detonation of ammonium azide? Ammonia has an exotherm ...
17-11-2002 at 17:17
by: madscientist
A call to all new members
Vulture is right.

This place is about science; it is not about making a fierce fire, or a loud ba ...
17-11-2002 at 15:21
by: madscientist
Nitrogen trioxide
IodineForLunch noticed an entry for NO3 in his CRC handbook. According to the CRC handboo ...
14-11-2002 at 19:13
by: madscientist
Reducing nitriles
Does anyone know if it's feasible to reduce a nitrile to an amine? For example: reducing acetonitril ...
14-11-2002 at 18:06
by: madscientist
haha...
The Al-Chymist clearly was hacked...
13-11-2002 at 21:41
by: madscientist
Phorone
Whoops, I meant to say sodium carbonate.

I forgot to ask: was there fizzling upon addition of the ...
13-11-2002 at 18:11
by: madscientist
Phorone
I think it's clear that the addition of the sodium bicarbonate initiates a more complex chemical cha ...
13-11-2002 at 18:07
by: madscientist
Catechol preparation
Adding HCl to the molecule you shared a diagram of should yield the free acid of that salt: 4,5-Dihy ...
13-11-2002 at 18:01
by: madscientist
Catechol preparation
I have been interested in preparing Benzene-1,2-diol (catechol) for some time. Here's the route of s ...
12-11-2002 at 16:37
by: madscientist
Nitration with electrolysis
"Nitrated with electrolysis" That is far too vague for me to be able to go anywhere with it.
12-11-2002 at 14:33
by: madscientist
Nitration with electrolysis
We might as well be asking how to make stuff with chemicals. Your question needs to be much more spe ...
11-11-2002 at 13:43
by: madscientist
metallic peroxy salts
Mixing Cl2O7 with H2O2 would probably result in an equim ...
10-11-2002 at 12:34
by: madscientist
Organic chlorinations
Here's an idea that just occurred to me.

Why not add a stoichemitric quantity of a dry ammonium s ...
1-11-2002 at 13:10
by: madscientist
Nitrohydrazine synthesis
Nitrohydrazine, NH2NHNO2, would obviously be an extremely powerful explosive c ...
1-11-2002 at 13:07
by: madscientist
Can't make CuO
CuO is black.
31-10-2002 at 14:39
by: madscientist
HMTD problem
Try neutralizing your solution - it's likely that HMTD will precipitate (not certain though, this is ...
31-10-2002 at 14:23
by: madscientist
Can't make CuO
You'll get the blue insoluble Cu(OH)2. Filter it out, and heat it strongly, to get the bl ...
30-10-2002 at 15:55
by: madscientist
simple energetic materials
It would improve the density, but I don't think that it's going to make it any more powerful. Think ...
30-10-2002 at 15:00
by: madscientist
Preparation of cyanides
Nick, could you post your results here as well? :)
29-10-2002 at 15:37
by: madscientist
simple energetic materials
[quote]NO2CH2CBrNO2CH3O2N[/quote]

I think that was supposed to be O2NCH2CBrNO2CH2NO2 (1,2,3-trini ...
29-10-2002 at 15:35
by: madscientist
Dangerous Peroxides
One that would be interesting is the peroxide of dimethyl ether. I calculated that it should yield s ...
29-10-2002 at 04:35
by: madscientist
Potassium ferrate
Electrolyzing a solution of potassium nitrate with iron electrodes will initially yield a solution o ...
28-10-2002 at 14:26
by: madscientist
Synthesis of alkali nitrogen compunds.
Electrolyzing NaCl in CH3OH would be a mess. The liberated chlorine gas would react with ...
27-10-2002 at 20:10
by: madscientist
Triple post :D
This is something that PHILOU Zrealone posted in the trinitromelamine thread:

[quote]NH2-C6H5 + H ...
24-10-2002 at 10:37
by: madscientist
Hexanitrobenzene
It seems that PHILOU Zrealone didn't post that in the trinitrotoluene preparation thread. I know I s ...
24-10-2002 at 10:33
by: madscientist
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