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pyridine reduction
Cheers madscientist, I didnt realise I had a fan ;)

Anders: Yes I'm sure. Try picking up a book s ...
3-7-2013 at 09:47
by: DJF90
Ostwald process
Catalytic converters for cars are designed to reduce NOx to N2, so your idea won't work as you've de ...
30-6-2013 at 13:34
by: DJF90
I quit
I agree alot with Plante on some of his points. I think there is alot of bone idleness amongst some ...
30-6-2013 at 07:06
by: DJF90
database of rare reactions
I'm glad you got to him first, Heuteufel.

Anders, maybe you should pick up a decent book sometime ...
29-6-2013 at 06:17
by: DJF90
pyridine reduction
Pyridine forms a stable adduct with borane, and is not reduced.
29-6-2013 at 00:12
by: DJF90
Flammable gas from TCCA and bleach!
Could you be making HOCN in some way? It can be made by high temperature decomposition of cyanuric a ...
16-6-2013 at 11:11
by: DJF90
question on scaling up
You havent said what your initial scale or reaction is, but you do say you're scaling to 100 mmol. T ...
10-6-2013 at 10:25
by: DJF90
TLC Reference paper
If the extract is dilute it allows you to apply a reasonable amount of material to the plate without ...
3-6-2013 at 11:44
by: DJF90
Cooling bath at -10*C
[rquote=286599&tid=24490&author=adamsium]A frigorific mixture of ice and ammonium chloride w ...
3-6-2013 at 09:13
by: DJF90
TLC Reference paper
They're using plates with a pre-concentration area. You spot below the baseline, where the pre-conce ...
2-6-2013 at 08:57
by: DJF90
dimethyl mercury synthesis
[rquote=286446&tid=24482&author=Vikascoder]I was searching for some toxic compounds of mercu ...
2-6-2013 at 08:50
by: DJF90
Dimethyl Sulfate, cheapest preparation, OTC !
I've tried the thermal decomposition of methyl hydrogen sulfate, as per sartori. Painkilla (a member ...
2-6-2013 at 06:12
by: DJF90
Succinimides to pyrroles
Distillation with zinc dust is said to work with succinimide itself
15-5-2013 at 23:07
by: DJF90
Building a polarimeter
Cheers for your input watson. I've built a wheatstone bridge before so I should know this, but it wa ...
8-5-2013 at 09:15
by: DJF90
Building a polarimeter
Component G is a microammeter I expect. What bothers me is the values of the two resistors, R1 and R ...
4-5-2013 at 00:38
by: DJF90
entropy51 memorial
I consider Robert a good friend of mine We had exchanged so many U2Us that I had forgotten about hal ...
21-4-2013 at 12:33
by: DJF90
I just made some Rheosmin, what is pure, but has no odor.
I'm befuddled. The carbon spectra looks good. The proton is fairly good too, although not too happy ...
9-4-2013 at 12:37
by: DJF90
I just made some Rheosmin, what is pure, but has no odor.
I too would like to see the spectra. I have no software on my home computer, so if you could post an ...
7-4-2013 at 03:35
by: DJF90
Replacing air with gas in vessel without vacuum?
Of course, but it depends on how much gas you're willing to expend in such a process. A continual st ...
7-4-2013 at 03:26
by: DJF90
Basifying Agents
There are a whole variety of solutions available for work up. Generally theres strong/weak acid/base ...
7-4-2013 at 01:42
by: DJF90
Lab Prep of Diethyl Sulfate
Its a good job I won't be wasting my time then...
3-4-2013 at 10:27
by: DJF90
Lab Prep of Diethyl Sulfate
I'm not too suprised this doesn't work as advertised, but I'm amazed by what little product you did ...
1-4-2013 at 01:36
by: DJF90
Building a polarimeter
Any idea about the electronics as I mentioned above? Thats the only thing that stopped me from gathe ...
10-3-2013 at 13:30
by: DJF90
Synthesis of Vanillyl Acetamide, a capsaicin derivative
Don't worry about the oversight, like I said I've fallen ill of this before myself. Additionally, th ...
24-2-2013 at 07:50
by: DJF90
Synthesis of Vanillyl Acetamide, a capsaicin derivative
In the reduction of the oxime, you filter off the excess zinc but don't seem to afford any separatio ...
24-2-2013 at 05:59
by: DJF90
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