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Picric acid: different instructions
This scheme is something that may fit my idea about synthesis of azide in decent yield being possibl ... |
31-3-2015 at 10:54
by: Rosco Bodine |
picric acid from aspirin
For the nitration of phenolsulfonic acid the sulfonic group is easily replaced by a nitro, and simi ... |
31-3-2015 at 08:42
by: Rosco Bodine |
picric acid from aspirin
The nitroso group should have been included but was not provided in the sequence which Davis describ ... |
31-3-2015 at 06:58
by: Rosco Bodine |
picric acid from aspirin
[rquote=399152&tid=22241&author=PHILOU Zrealone][rquote=399062&tid=22241&author=Rosc ... |
31-3-2015 at 06:48
by: Rosco Bodine |
additonal references
Attached are some additional references related to sulfonation and nitration of salicylic acid. I th ... |
30-3-2015 at 21:56
by: Rosco Bodine |
picric acid from aspirin
Yes the facile thermal decomposition of trinitrobenzoic acid to trinitro benzene was something being ... |
30-3-2015 at 07:57
by: Rosco Bodine |
Picric acid: different instructions
[rquote=399014&tid=389&author=Hennig Brand]
I think you must be forgetting, or just rec ... |
29-3-2015 at 20:41
by: Rosco Bodine |
Picric acid: different instructions
It isn't really a substantive issue what is the mechanism, or if different paths are occurring simul ... |
29-3-2015 at 19:36
by: Rosco Bodine |
Picric acid: different instructions
The sulfonate group is more stable than the carboxyl so the "steering effect" on substitution by the ... |
29-3-2015 at 17:47
by: Rosco Bodine |
picric acid from aspirin
Yes I have finished reviewing the other thread and replied there with what I think is a needed refer ... |
29-3-2015 at 16:32
by: Rosco Bodine |
Picric acid: different instructions
[rquote=328104&tid=389&author=Hennig Brand]For a long time I was off and on questioning the ... |
29-3-2015 at 16:26
by: Rosco Bodine |
picric acid from aspirin
The other thread I am reviewing again, but something I have seen already is a diagram regarding the ... |
29-3-2015 at 15:16
by: Rosco Bodine |
picric acid from aspirin
I saw more thickening of the stirred mixture late in the nitration made a yet smaller rate of foamin ... |
29-3-2015 at 11:26
by: Rosco Bodine |
picric acid from aspirin
[rquote=363309&tid=22241&author=Hennig Brand]If aspirin is used instead of salicylic acid hy ... |
29-3-2015 at 10:25
by: Rosco Bodine |
ETN synthesis problem
Here is a reference of interest describing a mixed acid nitration of ETN and testing of ETN usefulne ... |
27-3-2015 at 12:21
by: Rosco Bodine |
RDX synthesis
[rquote=326429&tid=250&author=roXefeller][rquote=326410&tid=250&author=Dornier 335A] ... |
27-3-2015 at 11:14
by: Rosco Bodine |
Magnesium Nitrate Mg(NO3)2 dehydration related
More information provided here concerning dehydration properties of Magnesium Nitrate which is usefu ... |
25-3-2015 at 16:26
by: Rosco Bodine |
Is old picric acid gauze found in first aid kits really that dangerous?
In an industrial, weapons manufacturing, or bulk transportation quantity, there are several catastro ... |
22-3-2015 at 13:40
by: Rosco Bodine |
Is old picric acid gauze found in first aid kits really that dangerous?
[rquote=397916&tid=61870&author=kekule]I have read several internet reports of the bomb squa ... |
22-3-2015 at 09:52
by: Rosco Bodine |
Cyklonan
[rquote=393552&tid=33246&author=Laboratory of Liptakov]With the wax into it Berta system is ... |
20-2-2015 at 22:30
by: Rosco Bodine |
Cyklonan
I think the wax flows during pressing and fills small air spaces which are needed for DDT so for the ... |
20-2-2015 at 10:34
by: Rosco Bodine |
Cyklonan
I think the double or multiple salt may be anhydrous, based on no moisture loss observed at approxim ... |
19-2-2015 at 16:46
by: Rosco Bodine |
Cyklonan
@ LL I agree about the possibility of a mixed salt of TACN and TACP being the product. A synthesi ... |
19-2-2015 at 10:54
by: Rosco Bodine |
NPED detonator
For 1.5 grams TACP with no paraffin a 1/4" column diameter loaded at 8,000 psi, 300mg LA produced co ... |
18-2-2015 at 17:04
by: Rosco Bodine |
NPED detonator
Perhaps the detonation of AP is catalyzed by the Cu ion from the TACP.
Have you tried paraffin as a ... |
18-2-2015 at 11:50
by: Rosco Bodine |
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