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thionyl chloride synthesis
I have decided that I am going to make one large batch of thionyl via Kyrides, when I have the money ... |
3-2-2009 at 16:16
by: Jor |
Carbon monoxide preparation?
I do really think people overrate CO.
Although it is colorless and odourless, you have to inhale qu ... |
2-2-2009 at 06:56
by: Jor |
thionyl chloride synthesis
I don't think phthalic acid should be used! Phthalic anhydride!
First I think it is less reactive ... |
1-2-2009 at 15:22
by: Jor |
thionyl chloride synthesis
[quote][i]Originally posted by panziandi[/i]
Yes, PCl5 will chlorinate phthalic acid and you would ... |
1-2-2009 at 14:57
by: Jor |
The short questions thread (1)
Are you sure it did not 'supercool'. My GAA was still liquid at 5C, but when I shaked the bottle, it ... |
1-2-2009 at 14:35
by: Jor |
thionyl chloride synthesis
Yes Kyrides.
You need phthaloyl chloride, wich is expensive, but can be made from phthalic anhydr ... |
1-2-2009 at 14:04
by: Jor |
thionyl chloride synthesis
Panziandi, as a answer to your first post in this topic:
-sulfur chlorides just stink very bad, muc ... |
1-2-2009 at 11:59
by: Jor |
thionyl chloride synthesis
I do not wish to work with SO3. It is extraordinary hazardous ,if I was told right.
First my fume h ... |
31-1-2009 at 15:10
by: Jor |
thionyl chloride synthesis
Well, Wilco, I have not asked Labstuff yet, but he gave me a lot of restricted chemicals as you hav ... |
31-1-2009 at 12:50
by: Jor |
thionyl chloride synthesis
Sorry.
I did not have PMs at hand when typing this message. I was not sure if you said that you re ... |
31-1-2009 at 12:32
by: Jor |
thionyl chloride synthesis
I really want some SOCl2, for making anhydrous metal salts (like CrCl3) from hydrated metal salts.
... |
31-1-2009 at 12:01
by: Jor |
anhydrous CrCl3
IrC, that looks like a not too hard to perform method, however....
I would want to build a tube f ... |
29-1-2009 at 03:23
by: Jor |
The short questions thread (1)
[quote][i]Originally posted by Aubrey[/i]
i've just been making phthalimide from phthalic anhydride ... |
28-1-2009 at 13:57
by: Jor |
anhydrous CrCl3
Yes, ofcourse. |
28-1-2009 at 10:41
by: Jor |
anhydrous CrCl3
Since I have seen some is this stuff in large crystal form, I really want to have some too. The comp ... |
28-1-2009 at 01:39
by: Jor |
Dutch hobby chemist forum
If you are Dutch or a Dutch speaking one from Belgium, and perform amateur chemistry, please take a ... |
28-1-2009 at 00:11
by: Jor |
ethylenediamine HCl
I wanted to prepare some ethylenediamine hydrochloride.
First attempt was to add a mL of ethylene ... |
26-1-2009 at 14:23
by: Jor |
At what point does Sulfuric Acid reach its lowest Ph?
If I remember right, even HCl does not fully dissociate at a concentration of 0,1M. And HCl is a str ... |
23-1-2009 at 15:05
by: Jor |
Uses of Chlorine
Another VERY nice experiment is burning sodium metal in chlorine gas.
Use a spoon-like spatula, a ... |
22-1-2009 at 12:39
by: Jor |
A nice peroxo complex of vanadium
Toxic is not a good description. I would rather call it very toxic.
http://msds.chem.ox.ac.uk/VA/ ... |
21-1-2009 at 00:39
by: Jor |
question an N-acetylation of aniline, using aspirin
Sorry for the late reply.
I have only a small amount of salicylic acid (5g) left, and i'd like to ... |
20-1-2009 at 14:36
by: Jor |
A nice peroxo complex of vanadium
Sorry, stupid mistake. I was calculating from the KVO4, and made a thinking mistake by thinking that ... |
18-1-2009 at 13:49
by: Jor |
question an N-acetylation of aniline, using aspirin
Are you sure heating GAA with aniline will give acetanilide? I thought only formic acid would do tha ... |
18-1-2009 at 11:54
by: Jor |
A nice peroxo complex of vanadium
Yes, I also have that beige/yellow powder. When some is added to dilute sulfuric acid, a red solutio ... |
18-1-2009 at 11:39
by: Jor |
question an N-acetylation of aniline, using aspirin
Last 2 days, I have tried this reaction again, using a readily available, potential N-acetylating ag ... |
18-1-2009 at 08:13
by: Jor |
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