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Trinitrophenol (TNP)
Check out the thread in this section "Picric Acid and the Mystery of the Red Goo".
5-1-2003 at 12:57
by: madscientist
Picric acid: different instructions
I would definitely go with the Powerlabs synthesis. Any procedure that measures phenol in milliliter ...
5-1-2003 at 10:26
by: madscientist
Note
This is somewhat out of place, but I wanted to post this in a place where everyone can see it.

Wh ...
4-1-2003 at 22:53
by: madscientist
Xenon Electronegativity
Electronegativity of Xe is just a figure found by comparing the strength of a Xe-Xe and a F-F single ...
4-1-2003 at 16:00
by: madscientist
Greetings.
Nice to see you here. :)
2-1-2003 at 16:38
by: madscientist
H2SO4 from CU2SO4 and HCl
That would work if one was willing to part with *lots* of anhydrous HCl.

pKa HCl = -7
...
1-1-2003 at 11:42
by: madscientist
Anhydrous metal chlorides with NH4Cl?
Ammonium chloride is slightly soluble in alcohol.
1-1-2003 at 11:40
by: madscientist
Drain Cleaner
I can find two brands of concentrated sulfuric acid at the local hardware store: "Liquid Fire", and ...
25-12-2002 at 22:53
by: madscientist
Hexamine Diperchlorate
Wouldn't it be possible to prepare purer hexamine perchlorate by reacting moist ammonium perchlorate ...
25-12-2002 at 22:36
by: madscientist
Can't make CuO
I've noticed that electrolyzing a solution of MgSO4 with a Cu anode, and then allowing it ...
25-12-2002 at 22:23
by: madscientist
monoalkanolamide ?
A few months back, ability to edit posts mysteriously ended - apparently something went screwy with ...
25-12-2002 at 22:14
by: madscientist
Diphoronepentaperoxide (DPPP)
The answers are in this thread... let's not have discussion going in circles.
21-12-2002 at 18:30
by: madscientist
KCLO3 by way of H2O + KCL
I forgot to mention: during electrolysis, the temperature of the solution was from 50C to 90C, usual ...
19-12-2002 at 21:38
by: madscientist
KCLO3 by way of H2O + KCL
I just electrolyzed 20g of KCl in distilled water for several hours using a graphite anode, a steel ...
19-12-2002 at 19:45
by: madscientist
monoalkanolamide ?
Kingspaz: that would be an oxime (if you're thinking of the --NHOH group).
19-12-2002 at 16:16
by: madscientist
H2SO4 from CU2SO4 and HCl
That won't work. H2SO4 is significantly less volatile than HCl, and H2
18-12-2002 at 17:22
by: madscientist
Hexanitrobenzene
Could you provide details on preparing pentanitroaniline from aniline?
17-12-2002 at 20:39
by: madscientist
Acetaldehyde synthesis
That procedure for preparing benzaldehyde from benzyl alcohol is actually of use. If an equamolar qu ...
17-12-2002 at 20:25
by: madscientist
Preparing solid iodine.
The iodine in the seaweed is probably in the form of sodium iodide. So, this is my suggestion: add t ...
17-12-2002 at 20:15
by: madscientist
Nylon synthesis, help please
HCl will add to H2C=CH2 to form CH3CH2Cl.
17-12-2002 at 16:27
by: madscientist
Hexanitrobenzene
I would think that it would be rather explosive, considering what the thermodynamics of decompositio ...
15-12-2002 at 18:39
by: madscientist
Chlorobutanol synthesis
Chlorobutanol: Cl3CC(CH3)2OH: Colorless to white crystals with c ...
15-12-2002 at 18:35
by: madscientist
Acetaldehyde synthesis
I recently attempted to dehydrogenate ethanol to yield acetaldehyde. I boiled 100mL of ethanol (dena ...
13-12-2002 at 17:12
by: madscientist
Lead Picrate
I do think that Ramiel may have had a valid point.

This energetic materials forum is more about t ...
13-12-2002 at 12:22
by: madscientist
Acidic water production...
What is the solution?
12-12-2002 at 11:36
by: madscientist
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