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5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
God that is a lot of nitrogens. I like it. Any practical information on the synth or explosive prope ...
16-7-2008 at 01:22
by: 497
Ethyl/Isopropyl Bromide preparation
Maybe freeze with LN2...

EtBr freezes at -119*C while DCM at -97*C... might not work out.

EtBr ...
16-7-2008 at 01:15
by: 497
Cleaning crude DCM (from distillation)
Wow you are lucky to have paint stripper with such high DCM content, I have only managed to find it ...
14-7-2008 at 22:59
by: 497
Evil's not-so-amazing $20 OTC vacuum aspirator and recirculating station...
How about a low melting metal alloy like Woods metal?? :P Just kidding. That would get destroyed by ...
14-7-2008 at 16:11
by: 497
Preparation of elemental phosphorus
The red is just dye :P

IIRC they're mostly KClO3, glue, and ground glass for sensitizing. I'm pro ...
8-7-2008 at 19:02
by: 497
PLX type explosives
I was afraid of that. And I suppose something neutral and stable like ammonium picrate would be inso ...
3-7-2008 at 17:59
by: 497
H2SO4 by the Lead Chamber Process - success
I was just revisiting the old oleum/SO3 thread and found the discovery by garage chemist that HPO3 w ...
2-7-2008 at 18:36
by: 497
Ethyl/Isopropyl Bromide preparation
Do you think this would work with methyl instead of ethyl? I don't see why not. The condenser would ...
2-7-2008 at 15:59
by: 497
PLX type explosives
Another possible high powered explosive solvent for picric acid is methyl nitrate. I don't know anyt ...
2-7-2008 at 01:09
by: 497
Methyl Ethyl Ketone Peroxide
No it is not already oxygen deficient if i calculated right.

15.5g AN produces 3g oxygen

6.6g ...
30-6-2008 at 12:50
by: 497
Methyl Ethyl Ketone Peroxide
Aluminum is passivated with an oxide layer that renders it quite innert to attack by such weak thing ...
30-6-2008 at 12:06
by: 497
Methyl Ethyl Ketone Peroxide
There are no AP crystals involved. Personally I would never touch AP crystals, I like my fingers. AP ...
30-6-2008 at 04:18
by: 497
Methyl Ethyl Ketone Peroxide
Yesterday (in a dream of course) I mixed roughly equal volumes of Hodgdon Longshot shotgun powder wi ...
28-6-2008 at 16:28
by: 497
Chem Run, AN questions
I got 22,000 grams of ammonium nitrate, potassium nitrate, and calcium nitrate for $20 each...

I ...
27-6-2008 at 18:21
by: 497
Methyl Ethyl Ketone Peroxide
I wouldn't count on MEKP being a good solvent. I tossed some MEK on a styrofoam packing peanut and i ...
22-6-2008 at 23:02
by: 497
Aqua Regia equation
I just found a reference that looks fairly reliable that says 4-5 ml of AR is required per gram of s ...
21-6-2008 at 16:27
by: 497
Nitric Acid Synthesis
nodrog, a while ago I tried exactly what you said with the Ca(NO3)2 and believe me, it is extremely ...
21-6-2008 at 16:06
by: 497
Acetaldehyde and Silver, Experimental Results
I don't know what your mystery crystals are but I'm pretty sure they're not paraldehyde as it is a s ...
21-6-2008 at 15:58
by: 497
Destroying carbon monoxide in a gas stream
Hmm sorry about that, I did read the thread, I don't know how I missed yours.
21-6-2008 at 15:43
by: 497
Destroying carbon monoxide in a gas stream
I just found a simple OTC mixture that will destroy CO at room temperature. I found it in "The War G ...
21-6-2008 at 15:05
by: 497
Aqua Regia equation
From wikipedia:

Au (s) + 3 NO3 - (aq) + 6 H + (aq) ---> Au 3+ (aq) + 3 NO2 (g) + 3 H2O (l)

...
20-6-2008 at 20:16
by: 497
Exotic thermites & analogs
You are right, the high powered hygroscopicity(?) of B2O3 would pose a major problem for the practic ...
20-6-2008 at 15:27
by: 497
making dichloromethane
It actually makes perfect sense because while chloroform may be hard to buy, it is not hard to synth ...
20-6-2008 at 15:21
by: 497
H2SO4 by the Lead Chamber Process - success
I think iron is the way to go. If you didn't see in the patent, the whole purpose of decomposing the ...
19-6-2008 at 23:33
by: 497
Exotic thermites & analogs
That is a great reference chemoleo!

The only thing i think it is lacking is information on the sp ...
19-6-2008 at 00:14
by: 497
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