| Search |
| [Next Page] |
Desperately seeking method for ethyl bromide.
I suggest to you to look in the Rhodium site under "Nitroalkane FAQ" or something like that.
Easy ... |
1-1-2011 at 21:23
by: xwinorb |
N-methyl isopropylamine synthesis
Both methyl isopropylamine and diisopropylamine are used in the synthesis of 4 and 5 substituted try ... |
28-12-2010 at 14:16
by: xwinorb |
N-methyl isopropylamine synthesis
I have just looked more carefully at the synthesis of this substance, and I have some concerns. The ... |
27-12-2010 at 15:55
by: xwinorb |
extraction an re-X without distillation suficcent?
I have tried the Ritter reaction for this particular synthesis, it does not work. If you look into s ... |
23-12-2010 at 15:50
by: xwinorb |
Hexamine from Esbit tablets
I have once looked at the tablets composition information from Esbit, I think they say it is only he ... |
19-11-2010 at 21:33
by: xwinorb |
Hexamine from Esbit tablets
I would like to know if hexamine from Esbit tablets would be OK to use in a sulfuric modified Duff f ... |
17-11-2010 at 18:23
by: xwinorb |
Titration Vs Density
My suggestion :
Try peroxide test strips. I am not an expert on the subject, I think titration is ... |
14-8-2010 at 05:48
by: xwinorb |
SpiceBoy method
I can't help you with the other method, IPA + I2 + H2O2. I never tried it. I have seen several posts ... |
30-7-2010 at 14:44
by: xwinorb |
p-benzoquinone HELP!!!
The SpiceBoy recipe is easy. It will not become yellow.
Yes, you can't dissolve the potassium dic ... |
28-7-2010 at 19:21
by: xwinorb |
Tryptamine refusing to crystallize
More exactly, the partial pressure of tetralin at 38 C is 1 mm Hg. |
19-7-2010 at 15:53
by: xwinorb |
Partial pressure of tetralin
I found a PDF document that lists the partial pressure of tetralin at 1 mm Hg as 38 C. So, turd, loo ... |
17-7-2010 at 17:29
by: xwinorb |
Tryptamine refusing to crystallize
I would suggest to do an A/B extraction instead of distilling out the tetralin.
Suggested proce ... |
13-7-2010 at 19:17
by: xwinorb |
Vacuum aspirator connection
Since you have mentioned the high powered aspirator setup :
Do you know how much the increase in ... |
9-5-2010 at 14:04
by: xwinorb |
Vacuum aspirator connection
I found a Web site that sells one interface from 3/4 in hose to 3/8 in, vacuum aspirator.
The nam ... |
9-5-2010 at 09:55
by: xwinorb |
Capsuline
I decided not to try to exchange it, I called my credit card company and asked them to cancel my pur ... |
6-4-2010 at 19:01
by: xwinorb |
Capsuline
Is this company a scam ?
I ordered online a small plastic "gadget" they sell, they asked me for a ... |
6-4-2010 at 13:51
by: xwinorb |
Zinc reduction for 2C-H from nitrostyrene
I have never tried it. The yield is quite high already anyway.
My best 75 %, my worse 55 %.
Th ... |
2-4-2010 at 14:18
by: xwinorb |
Pump not working correctly?
I don't think ballasts are an effective way of outgassing water, solvents and other impurities in yo ... |
29-3-2010 at 15:54
by: xwinorb |
Pump not working correctly?
Two links on vacuum gauges :
http://www.gaugestore.com/
http://www.tcvacuum.com/
I have the ... |
24-3-2010 at 11:40
by: xwinorb |
Pump not working correctly?
Forgot, also do not use BP of water to measure your vacuum pump vacuum. It is OK to use it for aspir ... |
23-3-2010 at 12:59
by: xwinorb |
Pump not working correctly?
I assume you have a rotary vane pump, looks like.
I strongly suggest to you to get a good electro ... |
23-3-2010 at 11:44
by: xwinorb |
toluquinone reduction
To Steve :
I think probably not worth doing it. Your benzoquinone is must probably OK to use. Unl ... |
17-3-2010 at 07:19
by: xwinorb |
hydroquinone and NaOH
I think I understand it better now.
Yes, the reference I have seen ( not read as carefully as I s ... |
16-3-2010 at 16:08
by: xwinorb |
hydroquinone and NaOH
I think I have found out. Looks like hydroquinone is oxidized by O2 and that happens faster under ba ... |
15-3-2010 at 20:57
by: xwinorb |
hydroquinone and NaOH
Does hydroquinone reacts directly with NaOH ? If so, what is the reaction product ?
I think it mi ... |
15-3-2010 at 20:28
by: xwinorb |
| [Next Page] |
