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Amateur route from R-OH to R-Cl
[rquote=647450&tid=156401&author=DraconicAcid]Depends on the R group. A tertiary alcohol ca ... |
27-10-2020 at 08:47
by: thors.lab |
Amateur route from R-OH to R-Cl
As far as I know this reaction can be done with thionyl chloride or phosphorous trichloride, both of ... |
27-10-2020 at 07:22
by: thors.lab |
TLC of amine hydrochloride salt
Hi, I've got a small sample of 2-FMA hydrochloride that I'm running TLC analysis on. The purpose of ... |
14-10-2020 at 14:41
by: thors.lab |
Size of chromatography column
Thank you friend! Great replies! That's basically all the information I needed haha.
You're right ... |
12-10-2020 at 11:36
by: thors.lab |
Size of chromatography column
I've been doing a little bit of analysis and small scale purification these days. Mostly recrystalli ... |
12-10-2020 at 01:38
by: thors.lab |
Need help interpreting 3-FEA H-NMR results
[rquote=646042&tid=156278&author=DraconicAcid]The broad peak is definitely the one on N, qui ... |
7-10-2020 at 17:43
by: thors.lab |
Need help interpreting 3-FEA H-NMR results
Oh, could the peak at 9.75 correspond to HCl from the HCl salt of 3-FEA? In which case, there's not ... |
7-10-2020 at 13:31
by: thors.lab |
Need help interpreting 3-FEA H-NMR results
Hi,
I have these H-NMR results for a 3-FEA batch (not my 3-FEA, not my NMR, I just have the scree ... |
7-10-2020 at 11:16
by: thors.lab |
H-NMR Multiplicity of aldehyde hydrogen on 3-fluorobenzaldehyde
[rquote=645818&tid=156260&author=DraconicAcid]Yes, you can sometimes get what is called "W-c ... |
5-10-2020 at 06:42
by: thors.lab |
H-NMR Multiplicity of aldehyde hydrogen on 3-fluorobenzaldehyde
So I would suspect the aldehyde hydrogen on 3-fluorobenzaldehyde to be a singlet right? The adjacent ... |
4-10-2020 at 21:26
by: thors.lab |
Recommended thermocouple and well adapter?
I'm looking to upgrade to a thermocouple since I don't really trust the cheapo rubber gasket thermom ... |
28-8-2020 at 07:01
by: thors.lab |
Reaction between oxalyl chloride and indole
So the carbonyl carbon in oxalyl chloride is electrophilic enough to attack the indole C3 without so ... |
24-8-2020 at 13:19
by: thors.lab |
Reaction between oxalyl chloride and indole
In TiHKAL, Sasha forms indol-3-ylglyoxyl chloride by reacting oxalyl chloride with indole directly, ... |
23-8-2020 at 23:29
by: thors.lab |
Beantown Chemical: ordering to house?
I have heard on this forum that Elemental is owned by somebody on this forum who regularly interacts ... |
21-8-2020 at 17:45
by: thors.lab |
Beantown Chemical: ordering to house?
Thanks everyone. I think I may do a trial run on Beantown then. Yes, they will probably check, but o ... |
21-8-2020 at 14:12
by: thors.lab |
Beantown Chemical: ordering to house?
Hi,
So I found [url=https://beantownchem.com/]"Beantown Chemical"[/url] which looks like they don ... |
20-8-2020 at 02:14
by: thors.lab |
Recommendations for synthesis of medicines and other medical organic molecules.
[rquote=643045&tid=155888&author=Herr Haber]Seing your earlier use of German I'll assume you ... |
19-8-2020 at 23:02
by: thors.lab |
Use of decyltriethylammonium iodide in ether synthesis in PiHKAL?
[rquote=643329&tid=156057&author=Metacelsus]Hmm, usually this is a phase transfer catalyst. ... |
18-8-2020 at 15:20
by: thors.lab |
Use of decyltriethylammonium iodide in ether synthesis in PiHKAL?
In PiHKAL #30 and #37 (and probably others, I was just flipping through randomly), Sasha uses what I ... |
18-8-2020 at 14:13
by: thors.lab |
What’s banned in CA?
[rquote=642818&tid=155994&author=OldNubbins]Cannot get denatured alcohol here.... yes, denat ... |
12-8-2020 at 00:37
by: thors.lab |
What’s banned in CA?
[rquote=642768&tid=155994&author=monolithic]DCM is impossible to find even outside of CA. If ... |
11-8-2020 at 11:03
by: thors.lab |
What’s banned in CA?
[rquote=642740&tid=155994&author=Yttrium2]I'm not recommending breaking the laws but that's ... |
11-8-2020 at 00:38
by: thors.lab |
What’s banned in CA?
Hey,
I’m from California. I’m on a trip right now in Utah right now and will later pass throu ... |
10-8-2020 at 11:47
by: thors.lab |
(safer) fluorination of benzaldehyde?
[rquote=642215&tid=155910&author=Tellurium]Well I would diazotize 2-Aminobenzyl alcohol with ... |
5-8-2020 at 08:33
by: thors.lab |
(safer) fluorination of benzaldehyde?
[rquote=642204&tid=155910&author=Syn the Sizer]@draculic acid69 Yes me too, I am interested ... |
5-8-2020 at 08:27
by: thors.lab |
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