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thermoelectric cooling bath
I have some of those blue ice things, they melt too quick and recently the ambient temp in my lab ha ... |
5-7-2021 at 00:29
by: mr_bovinejony |
thermoelectric cooling bath
Clamping with what? Maybe some cheap wood clamps on all 4 corners? |
4-7-2021 at 19:16
by: mr_bovinejony |
thermoelectric cooling bath
Oh hell yeah those would be perfect! In the video he used silicon around the TECs which seems like a ... |
4-7-2021 at 17:57
by: mr_bovinejony |
thermoelectric cooling bath
Very interesting! I was thinking to use a small tupperware that holds the water for the heat sinks, ... |
4-7-2021 at 16:57
by: mr_bovinejony |
thermoelectric cooling bath
https://youtu.be/0xY06PT5JDE
This video shows some peltier device that cools on one side and heat ... |
4-7-2021 at 11:05
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
This method also works no problem with 1,4 dimethoxybenzene. And the product is even more pure based ... |
19-6-2021 at 16:22
by: mr_bovinejony |
16 oz of nitroethane. Buy or nah?
Where are you buying these bottles from where a middleman gets ahold of them? Seems like from Amazon ... |
15-6-2021 at 16:09
by: mr_bovinejony |
16 oz of nitroethane. Buy or nah?
Do they not update the sds on their website? That's kinda shitty, although I bought some small bottl ... |
12-6-2021 at 20:53
by: mr_bovinejony |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Oh I have that thread bookmarked, still have to try that synthesis out. I didn't read through the wh ... |
11-6-2021 at 21:28
by: mr_bovinejony |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Do you have the link for that thread? |
11-6-2021 at 09:41
by: mr_bovinejony |
16 oz of nitroethane. Buy or nah?
Ohh I recognize that brand. I'm curious to know how much of a yield you get if you distill it |
7-6-2021 at 09:05
by: mr_bovinejony |
Indole-3-Carbinol Oxidation
Sure haven't! I'm going to run a tlc on these indoles I have now for practice |
5-6-2021 at 07:47
by: mr_bovinejony |
Indole-3-Carbinol Oxidation
I had some succes recrystallizing indole 3 aldehyde with dmf and water, maybe it'll work for indole ... |
5-6-2021 at 06:43
by: mr_bovinejony |
Indole-3-Carbinol Oxidation
Yeah I still have them, but the color is stupid and two recrystalizations later helped none. It's a ... |
5-6-2021 at 06:23
by: mr_bovinejony |
Indole-3-Carbinol Oxidation
I have already tried this with PCC twice with no success, but I haven't seen any other trials so don ... |
5-6-2021 at 03:58
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
Not sure why I can't edit the posts, but I have the images saved for if they do disappear. I don't t ... |
28-5-2021 at 17:41
by: mr_bovinejony |
LabDIRECT is now an Official US TCI Distributer!
Is there any kind of markup for these products? I imagine a very good percentage of my chemicals wil ... |
27-5-2021 at 14:56
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
The end of the vilsmeier saga: part one
5 grams of pcl5 is added to 5 ml of dmf. This heats up a ... |
26-5-2021 at 16:12
by: mr_bovinejony |
Elemental Scientific Liquidating Chemicals, glassware, and used equipment
Is this something you have to pick up in person? Or can they be shipped? |
25-5-2021 at 19:28
by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind
Very!! Bromo saccharin is incredibly easy to make. And it's much less irritating than nbs, although ... |
24-5-2021 at 20:23
by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind
Yes it did work, in fact it was as easy as replacing nbs with it in this bromination of 2ch. But fo ... |
24-5-2021 at 17:28
by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind
Dissolve 2ch in a minimum amount of gaa and add an equal weight of nbs! The product will precipitate ... |
24-5-2021 at 15:11
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
Of course not, I'm looking for some indole identification right now
The stuff decomposed once it ... |
24-5-2021 at 08:38
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
One last update until I get some real results, this first picture here is what I'm thinking is the f ... |
24-5-2021 at 07:52
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
Some interesting thing happens now, 5 grams of pcl5 are added to 5 ml of ice cold dmf. After this is ... |
24-5-2021 at 00:22
by: mr_bovinejony |
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