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POCL3-Phosphorus Oxychloride Synthesis Dry HCl may be less active against stainless at rt, but at 450C HCl will wreck just about any metal ... |
4-12-2014 at 17:32 by: mnick12 |
POCL3-Phosphorus Oxychloride Synthesis Table salt is probably fine, but if you want kosher salt does not have any additives.
Also I wou ... |
4-12-2014 at 12:03 by: mnick12 |
Maltotriose or amylose? Thanks Ozone,
My intetion for maltotriose is to develop a medium for the isolation of attenuative ... |
26-11-2014 at 23:23 by: mnick12 |
Maltotriose or amylose? Does anyone know where to buy Maltotriose or amylose? Sigma is waaaay to expensive.
Apparently th ... |
9-11-2014 at 11:15 by: mnick12 |
THIOUREA - odorless or fart-scented? DrMario,
I have had a similar experience with my bottle of thiourea, when I open the bottle it sm ... |
2-10-2014 at 10:14 by: mnick12 |
Hydrogen Bromide for Halogenation It could be related to other stuff besides meth, but looking at aYoungKing's post history you can se ... |
2-10-2014 at 10:10 by: mnick12 |
Handling Formic Acid? Strength compared to other acids? Well I don't think the pKa has a whole lot to do with how dangerous the acid is.
For example I ha ... |
27-9-2014 at 16:41 by: mnick12 |
Oxidation of ethanol by hypochlorite If you are going to synthesize ketones or aldehydes from alcohols from bleach you will need and acid ... |
10-8-2014 at 10:58 by: mnick12 |
Fiberglass Cloth - Available in the US Thanks! That is good to know.
Is it contaminated in any way with plastics or resins? Or is it pur ... |
10-8-2014 at 10:55 by: mnick12 |
Cutting sodium Well it doesn't sound like its and oxide/passivating layer problem. If it were it would be obvious f ... |
8-8-2014 at 15:50 by: mnick12 |
Bad days in the lab or with glassware? Today I pulled a kim wipe soaked with trimethylsilylmethyl lithium out of a glove box, as soon as I ... |
24-7-2014 at 21:30 by: mnick12 |
Oxone Aromatic Halogenation in Water - Is this write-up a lie? Well conversion is different than yield, as you seem to point out in your post. Again you cannot tal ... |
20-7-2014 at 19:47 by: mnick12 |
Oxone Aromatic Halogenation in Water - Is this write-up a lie? FireLion3, I understand your frustration with what appears to be a failed reaction. That being said ... |
20-7-2014 at 16:26 by: mnick12 |
Esterfication Question Probably, but you are going to need to reflux it for a while. I would suggest a dean-stark apparatus ... |
17-7-2014 at 13:55 by: mnick12 |
Adding Polypyridyl complexes to Fe Usually when we make complexes in the lab, we dissolve the ligand and metal salt in a solvent like T ... |
9-7-2014 at 23:19 by: mnick12 |
Report on Decarboxylation of Tryptophan in various solvents Okay this may be a silly question, but wouldn't the use of a pure ketone like acetophenone results i ... |
8-7-2014 at 09:28 by: mnick12 |
Using Calcium Hydroxide as a base in place of Sodium Hydroxide? Solubility might be an issue, a lot calcium compounds have terrible solubility. Also phenols are pre ... |
8-7-2014 at 09:26 by: mnick12 |
t-butyl benzene by Friedel-Crafts: some questions... My guess is the slow addition is to keep the concentration of t-butyl chloride low during the reacti ... |
5-7-2014 at 10:34 by: mnick12 |
Transfer hydrogenations with glycerol Thanks for the paper solo.
Anyway I still don't believe they reduced benzoic acid to benzyl alcoh ... |
3-7-2014 at 16:07 by: mnick12 |
TMS-azide explosion at University of Minnesota It looks like it was about 200g of the stuff that exploded, I think the bigger issue is someone work ... |
3-7-2014 at 15:59 by: mnick12 |
Transfer hydrogenations with glycerol It is a cool reaction if it actually works, they claim reduction of benzoic acid to benzyl alcohol, ... |
30-6-2014 at 23:21 by: mnick12 |
Best way to clean tar (chemically) Potassium hydroxide in ethanol is an excellent way to dissolve organic residue. Let it soak for one ... |
21-6-2014 at 10:14 by: mnick12 |
Vanadium: The metal that may soon be powering your neighbourhood Its interesting, but doesn't seem very practical. A giant vat full of sulfuric acid and vanadium sal ... |
14-6-2014 at 09:56 by: mnick12 |
Photoredox Catalysts, & My recent preparation of Tris(bipyridine)nickel(II) hydrochloride Coordination chemistry, yay!
Out of curiosity what does the complex look like? Also is refluxing ... |
20-5-2014 at 15:39 by: mnick12 |
How to do KMno4 oxidation workup? Depending on how pure you need your acid to be, I would distill the final product after acidificatio ... |
18-5-2014 at 08:23 by: mnick12 |
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