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NIHT/NHHT Synth Suxess!
I gave NIHT a shot recently:

Hexamine (3.5 g, 25 mmol) was added to hydrochloric acid (37%, 10 ml ...
21-1-2024 at 06:44
by: Microtek
Nitration of Tetramethylene dinitroethane tetranitrate
I think the main reason that P2O5 is not used more than it is, is that it is difficult to work with. ...
16-1-2024 at 00:40
by: Microtek
How to plasticize ETN with SBR (styrene-butadiene rubber)?
Denny, when you say:

[quote]
There are also many silicone-based adhesives, but as far as I know, ...
12-1-2024 at 00:55
by: Microtek
My problem with pure fuming hno3
If you add the urea in small portions and wait until the exotherm has subsided before adding more, r ...
11-1-2024 at 01:34
by: Microtek
Azides
I would suggest doing microscale experiments to see what works best. Consider using a mix of solvent ...
9-1-2024 at 23:10
by: Microtek
question about primaries
It is well known that many primaries can detonate from the breaking of large crystals. It is possibl ...
8-1-2024 at 23:27
by: Microtek
Azides
HN3 is a weak acid so when NaN3 is dissolved in water, some of the azide ions will be protonated as ...
6-1-2024 at 14:55
by: Microtek
What's inside the dry fuel tablets
I would recommend purifying the hexamine (if that is what it is) before using it in a synthesis. You ...
28-12-2023 at 03:30
by: Microtek
Exotic Primaries - Complex Salts
I have tried tackling the problem of reliable sensitivity tests myself. I experimented with vertical ...
23-12-2023 at 02:39
by: Microtek
Exotic Primaries - Complex Salts

[quote]
A matchhead quantity placed on concrete floor hit with the top of a pliers set it off (no ...
22-12-2023 at 08:41
by: Microtek
New Energetic Materials - Current Research

[quote]
There are no closed systems in the universe or we would be unable to study them experimen ...
20-12-2023 at 00:54
by: Microtek
New Energetic Materials - Current Research
I completely disagree. Both on the implied existence of a conspiracy in the energetics community, an ...
19-12-2023 at 01:58
by: Microtek
New Energetic Materials - Current Research
Well, Klapƶtke et al (among others) have done quite a lot of work on high nitrogen compounds. This ...
18-12-2023 at 02:04
by: Microtek
New Energetic Materials - Current Research
What I meant was, is there any data that suggest it may have been synthesized at some point? All I s ...
17-12-2023 at 03:15
by: Microtek
New Energetic Materials - Current Research
Is there reason to think that this is anything other than a purely theoretical molecular structure? ...
13-12-2023 at 00:29
by: Microtek
Exotic Primaries - Complex Salts
I wouldn't say that the synthesis is particularly complex; you are simply adding silver nitrate soln ...
4-12-2023 at 04:27
by: Microtek
Exotic Primaries - Complex Salts
Hmm, I only experimented with the perchlorate variant but those numbers look enticing. Maybe I will ...
30-11-2023 at 00:07
by: Microtek
Nickel aminoguanidine diperchlorate
I think the water sensitivity is caused by aminoguanidine being a quite labile ligand in this comple ...
23-11-2023 at 03:27
by: Microtek
Nickel aminoguanidine diperchlorate
Yes, NAP is very hard to beat. However, have you tried putting the finished NAP in water? I did that ...
22-11-2023 at 13:02
by: Microtek
Nickel aminoguanidine diperchlorate
I agree that it is almost inconceivable that Co(AGu)2(ClO4)2 should be non-energetic. One thing to t ...
22-11-2023 at 03:58
by: Microtek
Exotic Primaries - Complex Salts
I didn't mean to imply that there isn't a use case for silver 5-ATz perchlorate, just that when I ex ...
22-11-2023 at 02:56
by: Microtek
Exotic Primaries - Complex Salts
I have experimented with the silver 5-ATz perchlorate some years ago. IIRC, it worked fine, and was ...
21-11-2023 at 04:33
by: Microtek
Short question / quick answer - Thread
I would think that the vapor pressure of NG at least is too low to support combustion, though I have ...
6-11-2023 at 13:41
by: Microtek
"DINA", the nitration product of diethanolamine
But they are much more difficult to prepare than DINA (at least the ones in that paper)...

I did ...
6-11-2023 at 13:38
by: Microtek
Wrappolite from Dr. Liptakov
What is your EG diluted with? If it's water, it should be easy to just heat it to maybe 150C to driv ...
6-11-2023 at 02:20
by: Microtek
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