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Polymethyl pentene synthesis?
I am not well versed at all in polymerization reactions, however I looked up the reaction used indus ... |
13-1-2021 at 13:14
by: EverythingAl2O3 |
An attempt at making Phorone
[quote]
Hi EverythingAl2O3, you did very nice experiment! I found this article about synthesis, I h ... |
13-1-2021 at 06:09
by: EverythingAl2O3 |
An attempt at making Phorone
[quote]
Very cool! This can be used as a precursor for TEMPO which is a very useful oxidizing catal ... |
12-1-2021 at 17:10
by: EverythingAl2O3 |
An attempt at making Phorone
My first attempt at making phorone. I plan on using it to try and synthesize y-halo ketones/aldehyde ... |
12-1-2021 at 14:48
by: EverythingAl2O3 |
Large alcohol recrystallization
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Do you have the glass to make the nurdrage version?
[/quote]
Yes. I'm gonna need to get ... |
30-12-2020 at 20:10
by: EverythingAl2O3 |
Large alcohol recrystallization
[quote]
Do you have a dean stark trap heavy return? then do a steam dist. Or set up the heavy ret ... |
29-12-2020 at 09:30
by: EverythingAl2O3 |
Large alcohol recrystallization
I'm planning on making these alcohols, but their boiling points are so high that my hot plate can't ... |
28-12-2020 at 18:43
by: EverythingAl2O3 |
Question about a particular rendition of an allylic reaction
So I'm trying to figure this synthesis problem for a chemical I want to make which is related to 1,4 ... |
22-12-2020 at 09:28
by: EverythingAl2O3 |
Questions about MPV reduction
[quote]
I understand that I can't MPV with allyl iodide. Which is why I'm no longer trying to do th ... |
15-12-2020 at 16:25
by: EverythingAl2O3 |
Questions about MPV reduction
[quote]
EverythingAl2O3: First of all, it does not matter, you cannot do the MPV reduction on an ... |
14-12-2020 at 07:57
by: EverythingAl2O3 |
Questions about MPV reduction
[quote]
Ummm. MPV. Might expect either reaction of that Iodide, or synthesis of an Ether.
I'm ... |
13-12-2020 at 19:11
by: EverythingAl2O3 |
Advice on safety for aldol products
[quote]
Isn't iodoacetone a lachrymator? Or is it too low-boiling?
[/quote]
I have not come acr ... |
11-12-2020 at 13:41
by: EverythingAl2O3 |
Advice on safety for aldol products
So I was planning on doing an aldol of acetone and iodo-acetone, however I cannot find any safety in ... |
10-12-2020 at 15:14
by: EverythingAl2O3 |
More thoughts (rants) on AlCl3 Chlorination of alcohols
[quote]
The first time I tried making it was inside via ZnCl2 reduction with aluminum and I thoug ... |
9-12-2020 at 06:49
by: EverythingAl2O3 |
More thoughts (rants) on AlCl3 Chlorination of alcohols
So I did more thinking since my previous post about why AlCl3 doesn't work for chlorinating aliphati ... |
8-12-2020 at 20:43
by: EverythingAl2O3 |
Questions about MPV reduction
I found this paper on an alternative catalyst for MPV reduction instead of using AliPr3 and had a fe ... |
6-12-2020 at 08:38
by: EverythingAl2O3 |
AlCl3 is an alternative to SOCl2
[quote]
AlCl3 will not chlorinate alcohols. However, solutions of AlCl3 in hydrochloric acid will ... |
5-12-2020 at 05:55
by: EverythingAl2O3 |
AlCl3 is an alternative to SOCl2
Interesting that it doesn't tend to yield well. If that is normally the case then this paper found a ... |
4-12-2020 at 04:42
by: EverythingAl2O3 |
AlCl3 is an alternative to SOCl2
Hey everyone. I was thinking about reactions for Al2O3 (Not kidding really do this every second I ha ... |
3-12-2020 at 18:12
by: EverythingAl2O3 |
Amine alkylation catalysts
Absolutely. They are mostly non-toxic. In the case of Al2O3 it is only really a respiratory hazard. ... |
3-12-2020 at 09:45
by: EverythingAl2O3 |
Amine alkylation catalysts
I promise I am not going to try to be annoying. I have spent countless days working on theoretical r ... |
3-12-2020 at 07:07
by: EverythingAl2O3 |
Methanol from Acteone
If you can somehow get a hold of paraformaldehyde and NaOH you could get methanol from doing a Canni ... |
2-12-2020 at 19:45
by: EverythingAl2O3 |
Amine alkylation catalysts
You can also use Al2O3. The example given in an old 1959 Orgo textbook is that 1eq of MeOH +NH3 over ... |
2-12-2020 at 16:04
by: EverythingAl2O3 |
Various routes to acetaldehyde
Why bother with stuff as annoying as Acetylene or dangerous as chromium and mercury? Isn't it right ... |
2-12-2020 at 15:54
by: EverythingAl2O3 |
Selective cross aldol condensation for enolizable reagents
I'm looking for a selective aldol/looking to develop one. The closest I've found is linked below. I ... |
2-12-2020 at 12:58
by: EverythingAl2O3 |
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