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Red phosphorus to Phosphorus trichloride?
[rquote=683973&tid=12582&author=clearly_not_atara][quote]This mixture is heated to 500-600 C ...
11-5-2023 at 14:59
by: ErgoloidMesylate
Notes on p-Toluenesulphonic acid → p-Cresol
[rquote=683951&tid=158976&author=Keras][rquote=683926&tid=158976&author=ErgoloidMesy ...
11-5-2023 at 11:44
by: ErgoloidMesylate
Red phosphorus to Phosphorus trichloride?
[rquote=683952&tid=12582&author=Tsjerk] If that patent would be interesting that might be fi ...
11-5-2023 at 11:42
by: ErgoloidMesylate
Red phosphorus to Phosphorus trichloride?
[rquote=220836&tid=12582&author=slyder]can someone confirm if this reaction works for synthe ...
10-5-2023 at 14:32
by: ErgoloidMesylate
Notes on p-Toluenesulphonic acid → p-Cresol
[rquote=683923&tid=158976&author=Keras]

Lol, right. But p-toluidine to anisaldehyde???

...
10-5-2023 at 08:42
by: ErgoloidMesylate
Woes with reduced pressure distillation
[rquote=683917&tid=159553&author=ErgoloidMesylate][rquote=683909&tid=159553&author=K ...
10-5-2023 at 06:25
by: ErgoloidMesylate
Notes on p-Toluenesulphonic acid → p-Cresol
[rquote=683910&tid=158976&author=Keras][rquote=683898&tid=158976&author=ErgoloidMesy ...
10-5-2023 at 05:53
by: ErgoloidMesylate
Woes with reduced pressure distillation
[rquote=683909&tid=159553&author=Keras]Thanks a bunch to all for your respective input, very ...
10-5-2023 at 05:49
by: ErgoloidMesylate
Elemental Scientific Liquidating Chemicals, glassware, and used equipment
[rquote=683496&tid=156073&author=tomholm]Elemental Scientific Auction


Hi All,

The BM ...
9-5-2023 at 18:21
by: ErgoloidMesylate
Woes with reduced pressure distillation
[rquote=683886&tid=159553&author=Keras]Folks,

that looks like a newbie (tyro, if you like ...
9-5-2023 at 17:43
by: ErgoloidMesylate
Notes on p-Toluenesulphonic acid → p-Cresol
[rquote=683898&tid=158976&author=ErgoloidMesylate][rquote=683869&tid=158976&author=K ...
9-5-2023 at 16:28
by: ErgoloidMesylate
Notes on p-Toluenesulphonic acid → p-Cresol
[rquote=683869&tid=158976&author=Keras][rquote=683853&tid=158976&author=ErgoloidMesy ...
9-5-2023 at 15:32
by: ErgoloidMesylate
Notes on p-Toluenesulphonic acid → p-Cresol
[rquote=683013&tid=158976&author=Texium]Nice. Minor critique though: you should write TsONa ...
8-5-2023 at 09:19
by: ErgoloidMesylate
Notes on p-Toluenesulphonic acid → p-Cresol
[rquote=683445&tid=158976&author=Keras]So, third time is a charm, so they say.

When KOH h ...
8-5-2023 at 09:05
by: ErgoloidMesylate
Ethylamine Synthesis
[rquote=675986&tid=18598&author=ErgoloidMesylate]
... having looked up an old method of con ...
7-5-2023 at 13:39
by: ErgoloidMesylate
Tartaric acid prep - OTC
[rquote=266191&tid=21987&author=CHRIS25]Well, success! Spoke too early. I have a nice col ...
7-5-2023 at 13:16
by: ErgoloidMesylate
How to dry tartaric acid to make it anhydrous?
[rquote=554993&tid=106069&author=beerwiz]How to dry tartaric acid to make it anhydrous?

I ...
7-5-2023 at 13:00
by: ErgoloidMesylate
13X molecular sieve
It appears to remove co2 and dries gases.

https://link.springer.com/article/10.1007/s43979-022-00 ...
6-5-2023 at 16:15
by: ErgoloidMesylate
Preparation of dimethylamine
[rquote=683825&tid=156408&author=SplendidAcylation]

@clearly_not_atara, I have done this ...
6-5-2023 at 13:37
by: ErgoloidMesylate
Sourcing Non-denatured Anhydrous Ethanol in the US?
Except you may not understand how insane big brother has become in the US.

Would you believe the ...
5-5-2023 at 11:28
by: ErgoloidMesylate
Diethyl ether from chloroethane and sodium ethoxide
[rquote=683769&tid=150639&author=Keras][rquote=683766&tid=150639&author=ErgoloidMesy ...
5-5-2023 at 11:10
by: ErgoloidMesylate
Diethyl ether from chloroethane and sodium ethoxide
[rquote=614022&tid=150639&author=Keras]Apparently,
C[sub]2[/sub]H[sub]5[/sub]ONa + C[sub]2[ ...
4-5-2023 at 21:31
by: ErgoloidMesylate
Sourcing Non-denatured Anhydrous Ethanol in the US?
[rquote=683135&tid=159466&author=Sulaiman]

My ethanol source was fractionally distilled f ...
4-5-2023 at 16:25
by: ErgoloidMesylate
Ethylamine Synthesis
[rquote=683722&tid=18598&author=clearly_not_atara]http://archives.njit.edu/vol01/etd/1960s/1 ...
4-5-2023 at 15:53
by: ErgoloidMesylate
Ethylamine Synthesis
[rquote=675986&tid=18598&author=ErgoloidMesylate]
I think a better idea is just to reduce n ...
3-5-2023 at 11:45
by: ErgoloidMesylate
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