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from a secret admirer
I think it would form a mixture of azide from reacting with the NHNH<sub>2</sub> group a ...
2-3-2003 at 22:50
by: madscientist
Separatory funnel
I've had the valve of my separatory funnel get stuck before, and I found that I can free it by ...
28-2-2003 at 10:14
by: madscientist
Producing high % CO
PH Z, could you provide more details on that reaction you mentioned:

NaOH + CO ----> NaO2CH

...
25-2-2003 at 17:55
by: madscientist
Preparation of ionic nitrites
Here's an idea that occurred to me a while back for preparing nitrites (this should also work f ...
18-2-2003 at 17:45
by: madscientist
Stabilizing Nitrogen Tri-iodide
It's not safe when wet. Only less dangerous.

Be wary of iodine gas. Our biology doesn't ...
18-2-2003 at 17:29
by: madscientist
Aniline
Note: this has not been tested. What follows is only me speculating as to what I would do if I were ...
18-2-2003 at 17:26
by: madscientist
Phosphorus pentachloride
There is no common source of phosphorus pentachloride that I'm aware of.

It should be relati ...
18-2-2003 at 17:05
by: madscientist
Preparation of elemental phosphorus
Igniting a composition of aluminum powder and copper phosphate. If the stoichemitry is done right, t ...
2-2-2003 at 08:54
by: madscientist
Preparation of elemental phosphorus
Great idea! I think that at the very least the following will occur, considering that cupric chlorid ...
1-2-2003 at 21:45
by: madscientist
I use paper casings for detonators
They're superior in every way to plastic and metal casings, if made properly. I'll briefly go over h ...
29-1-2003 at 15:58
by: madscientist
AP Radical Changing
That compound you diagrammed would actually be an extremely powerful explosive. I doubt it would be ...
28-1-2003 at 22:21
by: madscientist
Nitrobenzene
Nitrating benzene at 60C in mixed acid (H2SO4/HNO3) yields mononitr ...
28-1-2003 at 15:39
by: madscientist
Trinitrotoluene preparation
No, PETN stands for pentaerythritol tetranitrate.
26-1-2003 at 22:33
by: madscientist
Trinitrophenol (TNP)
Aspirin is acetylsalicylic acid with small amounts of impurity (usually calcium phosphate and starch ...
24-1-2003 at 16:16
by: madscientist
Elemental bromine isolation
I think that passing dry chlorine over NaBr should yield dry bromine without the bromine chlorides - ...
22-1-2003 at 11:55
by: madscientist
Elemental bromine isolation
I was thinking of several methods of isolating elemental bromine without distillation. This is the i ...
21-1-2003 at 18:16
by: madscientist
Easy question
Pyrolysis is done by heating a sample to high temperatures. Electrolysis is done by having a sample ...
20-1-2003 at 14:29
by: madscientist
Blood as a Catlysor?!
What is it supposed to catalyze, though?
17-1-2003 at 16:49
by: madscientist
Sodium!
I prepared some sodium metal this last Saturday myself. I placed 20g of NaOH in a ceramic crucible, ...
13-1-2003 at 20:32
by: madscientist
Methyl Ethyl Ketone Peroxide
I would either dilute the sulfuric acid prior to adding it to the MEK/H2O2 sol ...
12-1-2003 at 17:52
by: madscientist
Hydriodic acid from iodides?
Oops, I should have clarified: the procedure I specified would yield some HI in solution at equilibr ...
12-1-2003 at 13:43
by: madscientist
Hydriodic acid from iodides?
You could use HCl to prepare HI from KI.

KI + HCl <----> KCl + HI

I don't think that HI can be ...
12-1-2003 at 13:03
by: madscientist
Dinitroacetone peroxide
I was thinking that nitrating acetone, and then preparing the cyclic peroxide of that, should yield ...
12-1-2003 at 13:00
by: madscientist
Hypobromite?
I recently tried to distill bromine out of a mix of Ca(OCl)2 and NaBr. I placed 64g of po ...
12-1-2003 at 11:59
by: madscientist
Lead/silver azide destruction?
I would place the lead/silver azide in hot water, add aluminum foil, and a touch of NaOH to help rem ...
6-1-2003 at 05:29
by: madscientist
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