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Microwave-made Nitric Acid
Hello Ayush,

I'm not sure how electrochemistry is related to "Microwave-made Nitric Aci ...
23-7-2005 at 04:42
by: jpsmith123
A true “gel” silica gel binder for graphite (or PbO2?) electrodes.
Interesting.

One of my many ideas was to try to mix PbO2 with a castable ceramic like this stuff: ...
21-7-2005 at 19:35
by: jpsmith123
More on PbO2 electrodes
Well unfortunately I don't have what I would call "glassworking skill" (although I ha ...
21-7-2005 at 18:52
by: jpsmith123
More on PbO2 electrodes
Hello Garage_chemist,

I'm glad to to see you had success with your cell.

I debated using ...
21-7-2005 at 17:31
by: jpsmith123
Tantalum Rod Substrate
Well, I just ordered some tantalum rod.

I ordered 6" of 0.09 inch diameter tantalum...and it ...
21-7-2005 at 07:27
by: jpsmith123
More on PbO2 electrodes
I found another forum where people have been discussing making perchlorate by electrolysis:

http: ...
14-7-2005 at 05:35
by: jpsmith123
Any Successful PbO2 Anodes Here?
After reading everything related to PbO2 anodes I could find here, I get the impression that no one ...
12-7-2005 at 04:22
by: jpsmith123
What about silicon as an anode in a chlorate cell?
Unionised:

Sorry that the discussion has wandered.
It seems that there are already so many chlo ...
11-7-2005 at 05:44
by: jpsmith123
Another Idea
Taking the plastic substrate idea one step further, I wonder if the anode could be made of epoxy mix ...
10-7-2005 at 22:17
by: jpsmith123
What about silicon as an anode in a chlorate cell?
Strictly speaking, maybe it does actually plate lead first, and then the lead is immediately oxidize ...
8-7-2005 at 16:19
by: jpsmith123
What about silicon as an anode in a chlorate cell?
Hello 12AX7,

Being that I haven't had a chance to try making any anodes yet, I can't sa ...
8-7-2005 at 01:59
by: jpsmith123
Microwave-made Nitric Acid
Actually it may be the other way around.

In the patent and the paper I cited, the microwave disch ...
7-7-2005 at 17:36
by: jpsmith123
What about silicon as an anode in a chlorate cell?
Looks really messy. Rats.

I'm wondering, did you anodize the lead anode using the method I p ...
7-7-2005 at 16:47
by: jpsmith123
What about silicon as an anode in a chlorate cell?
Hmmm. I didn't know that several people had already unsuccessfully attempted to use plastic sub ...
6-7-2005 at 18:42
by: jpsmith123
What about silicon as an anode in a chlorate cell?
I believe that pure silicon has a high resistivity, so I was under the impression that you would nee ...
6-7-2005 at 07:07
by: jpsmith123
Method for anodic oxidation of lead.
Hello 12AX7,

I found the following by way of a Google search. I don't know if it works or no ...
6-7-2005 at 04:37
by: jpsmith123
What about Pb as a substrate for PbO2?
I wonder if a piece of pure lead could be somehow anodically oxidized and/or plated with PbO2 by the ...
6-7-2005 at 00:54
by: jpsmith123
What about silicon as an anode in a chlorate cell?
I have enough platinum that I could run at a few amps, conservatively, but the more I look into it, ...
5-7-2005 at 19:16
by: jpsmith123
6km/sec VOD From Cast NaCLO4 Composition
Thanks for that interesting patent regarding methylamine perchlorate.

BTW, it seems the commercia ...
2-7-2005 at 02:36
by: jpsmith123
Microwave-made Nitric Acid
It seems that using microwaves to make nitric oxide may be the easiest and best way to go.

At fir ...
2-7-2005 at 01:53
by: jpsmith123
Birkeland-Eyde reactor for making nitric acid.
Hello Marvin,

I'm not sure I understand exactly what you're saying. Are you saying tha ...
29-6-2005 at 23:21
by: jpsmith123
Birkeland-Eyde reactor for making nitric acid.
It's similar in the sense that you've got a high AC voltage and an insulator...I guess tha ...
29-6-2005 at 20:31
by: jpsmith123
Birkeland-Eyde reactor for making nitric acid.
Although I'm not planning on trying to make any HNO3 in the near future, it is something I look ...
29-6-2005 at 18:17
by: jpsmith123
What about silicon as an anode in a chlorate cell?
I was thinking that products like SiCl4 might not form in an aqueous environment.

In any case, I ...
29-6-2005 at 16:34
by: jpsmith123
What about silicon as an anode in a chlorate cell?
Hello Marvin,

Yes my first thought was that you'd get SiO2 and that would stop it, but, acco ...
28-6-2005 at 16:49
by: jpsmith123
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