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Preparation of Iodomethane
^Theory is worse than practice :D

But I think you'd have a better shot with TsOH. You can, for ex ...
11-5-2022 at 09:53
by: clearly_not_atara
Preparation of Iodomethane
[b]Keras[/b]: Crystals of H3PO4 can indeed be obtained by various means, as described e.g. by Ross a ...
11-5-2022 at 08:16
by: clearly_not_atara
Concentrated formic acid?
According to Schierz, anhydrous oxalic acid can be used to dehydrate formic acid:

https://pubs.ac ...
10-5-2022 at 09:22
by: clearly_not_atara
Preparation of Iodomethane
[rquote=673361&tid=12475&author=Keras]
I would have to read the article you provide a link ...
10-5-2022 at 08:12
by: clearly_not_atara
Concentrated formic acid?
Why not use a less acidic dehydrating agent? You could probably distill formic acid over MgSO4 or Ca ...
9-5-2022 at 17:05
by: clearly_not_atara
Preparation of Iodomethane
[rquote=673344&tid=12475&author=Keras]IINM, 100% H₃PO₄ is a solid with m.p. around 40 ° ...
8-5-2022 at 14:35
by: clearly_not_atara
Simple synthesis of NaOH from baking soda
I doubt you have to filter it that fast. Typical CO2 concentrations are about 400 ppm (300 ppm befor ...
8-5-2022 at 14:24
by: clearly_not_atara
obtaining isopropenyl acetate?
The action of excess anhydrous HBr in acetic acid on propylene glycol gives predominantly 2-acetoxy- ...
7-5-2022 at 05:02
by: clearly_not_atara
unconventional sodium
Sodium metal will probably corrode other metals by intercalation.
4-5-2022 at 11:03
by: clearly_not_atara
An Article for Thought and Discussion
Restrictions on weapons research are nothing new. It was applied to nuclear chain reaction research ...
2-5-2022 at 19:39
by: clearly_not_atara
Separating zinc and manganese sulfate
[rquote=673088&tid=158560&author=B(a)P]Thanks clearly_not_atara, this seems like the best ap ...
28-4-2022 at 07:25
by: clearly_not_atara
Acetic anhydride preparation
Lots of interesting transformations are possible with tBuOCl. It turns amines to N-chloroimines, ald ...
28-4-2022 at 06:49
by: clearly_not_atara
Separating zinc and manganese sulfate
I'm not sure how reliable the dissolution of zincates is. Plus, manganese could be oxidized and diss ...
27-4-2022 at 08:57
by: clearly_not_atara
Can Platinum be used as a hydrogenation catalyst?
Pd is just as rare as the others, but there was an oversupply following the collapse of the Soviet U ...
22-4-2022 at 19:07
by: clearly_not_atara
Hydrazine to Hydrazone question... please and thank you
I think you can do it actually, you have to acylate the far end of the hydrazine somehow and then ox ...
19-4-2022 at 20:01
by: clearly_not_atara
Zinc in organic chemistry -- why always the chloride salt?
Disinfectants and wood preserving are biological applications. We don't know anything about that kin ...
19-4-2022 at 18:16
by: clearly_not_atara
N-Dimethylation of aromatic nitro-amines
Nitration of aniline goes to para, then meta, due to electrostatic repulsion. Nitration of 4-bromodi ...
19-4-2022 at 16:17
by: clearly_not_atara
Small scale production of H2SO4 in the amateur lab
Oxalic acid is 80 times stronger than citric acid, so the product concentration will be 80 times bet ...
17-4-2022 at 08:18
by: clearly_not_atara
Acetic anhydride preparation
Well, for one thing, why would we choose a precursor (for Ac2O) which is a gas?

Acetaldehyde is ...
15-4-2022 at 06:41
by: clearly_not_atara
Acid neutralizing on industrial scale
[rquote=672775&tid=158528&author=Tsjerk]
He wants to neutralize inline with a mixing valve, ...
14-4-2022 at 19:01
by: clearly_not_atara
What's the easiest reaction to perform the produces elemental iron?
Anhydrous ferrous chloride can be obtained by drying the methanol solvate, FeCl2*4MeOH, with adequat ...
14-4-2022 at 07:51
by: clearly_not_atara
Acid neutralizing on industrial scale
Using NaHCO3 for neutralization will reduce the heat production significantly, but also releases ple ...
13-4-2022 at 07:58
by: clearly_not_atara
BnCl synthesis - Using anhy. CaCl2 as catalyst?
I think ZnCl2 is used as an example because it's undergraduate pedagogy, not practical engineering, ...
10-4-2022 at 09:03
by: clearly_not_atara
I grew crystals at home and got the structure published in the Cambridge Structural Database
That's amazing. Congratulations! ^,^
4-4-2022 at 06:53
by: clearly_not_atara
lithium citrate or lithium hydroxide?
You don't know where to get lithium this, but maybe you can make it from lithium that. But now you d ...
31-3-2022 at 11:48
by: clearly_not_atara
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