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Decarboxylation of Glycine to Methylamine?! In Scr0t's pirrolidine synthesis there is a lot of turpentine, a small ammount of spearmint oil and ... |
17-4-2018 at 10:32 by: Pumukli |
2-butanol azeotrope? Do anyone know if secbutanol forms any sort of azeotrope with ethanol?
I could not find it online. |
31-3-2018 at 01:27 by: Pumukli |
Pretty Pictures (2) Failed recrystallization attempt of MCPA.
The liquid separated into two layers upon cooling and aft ... |
30-3-2018 at 10:39 by: Pumukli |
Aluminum - sourcing purest alloys - Can's are actually a good option! Thanks for the article, RogueRose! I'm wondering if I could make a few hundred grams of Al melt, hea ... |
30-3-2018 at 04:16 by: Pumukli |
Synthesis of m-nitro ethylbenzoate I tried to save on methanol (which is a "non-renewable" for me) but in the end it might have been be ... |
29-3-2018 at 01:21 by: Pumukli |
Synthesis of m-nitro ethylbenzoate [align=center][size=2]Synthesis of m-nitro ethylbenzoate[/size][/align]
[b]Literature:[/b] Orgsyn ... |
28-3-2018 at 10:02 by: Pumukli |
Decarboxylation of Glycine to Methylamine?! Seems to be a good idea.
Also, the note about not being pure product but a mixture of MeNH2 and oth ... |
28-3-2018 at 08:41 by: Pumukli |
Synthesis of m-nitro-ethylbenzoate The ethylbenzoate saga continues.
I'm over two batches, same procedure. The second one went more ... |
20-3-2018 at 11:16 by: Pumukli |
Decarboxylation of Glycine to Methylamine?!
ChemiPharma:
I use this complicated setup because I learned (of course the hard way) that the t ... |
17-3-2018 at 23:47 by: Pumukli |
Decarboxylation of Glycine to Methylamine?! [align=center][size=2]Making methylamine from glycine[/size]
testing a hypothetical pathway[/align] ... |
17-3-2018 at 14:05 by: Pumukli |
Decarboxylation of Glycine to Methylamine?! Since then I tried carbylamine test on NH4Cl. I could only smell sharp ammonia stench, nothing rotti ... |
17-3-2018 at 04:16 by: Pumukli |
Decarboxylation of Glycine to Methylamine?! Preliminary result:
We all know that preliminaries could have big mistakes, but here it goes anyw ... |
17-3-2018 at 00:33 by: Pumukli |
Decarboxylation of Glycine to Methylamine?! That's it, the carbylamine reaction!
I'll go that way. It is quick and can be done theoretically ... |
16-3-2018 at 16:36 by: Pumukli |
Decarboxylation of Glycine to Methylamine?! I would give it a go.
My plan is roughly: put a few NaOH beads into a mortar, put some glycine po ... |
16-3-2018 at 11:41 by: Pumukli |
Decarboxylation of Glycine to Methylamine?! All right :-) Now I know that NH3 and MeNH2 smell the same. And I also know they are quite different ... |
16-3-2018 at 09:14 by: Pumukli |
Decarboxylation of Glycine to Methylamine?! "@Diball sniffed only ammonia smell instead methylamine"
Can anyone tell the difference by smell ... |
16-3-2018 at 07:43 by: Pumukli |
Borohydride Offer closed. |
13-3-2018 at 11:50 by: Pumukli |
Carbamazepine Synthesis You are probably over this but yes, try the original reaction at reflux temperature too! And don't f ... |
13-3-2018 at 09:28 by: Pumukli |
Ethyl benzoate synthesis [size=2][align=center][b]Synthesis of ethyl benzoate[/b][/align][/size]
[align=center][size=2]-two ... |
12-3-2018 at 10:22 by: Pumukli |
Pretty Pictures (2) Have you ever tried sublimating benzoic acid in a pickle's jar?
After two days 8 g benzoic acid fil ... |
10-3-2018 at 12:58 by: Pumukli |
Carbamazepine Synthesis I understand your problem. Unexpectedly unreactive acid chloride.
I would expect at least partial h ... |
10-3-2018 at 12:16 by: Pumukli |
Experiments with Vanillin and Ethyl Vanillin Ideas Forget DMS or any other alkylating agents under your circumstances! Do more basic stuff with less vo ... |
8-3-2018 at 13:17 by: Pumukli |
Experiments with Vanillin and Ethyl Vanillin Ideas Condensation reactions with ketones. With simple acetone it is good, but even better with acetylacet ... |
8-3-2018 at 12:22 by: Pumukli |
Synthesis of ethylbenzoate I finished my epic synthesis yesterday and now I'm compiling/translating the results into a Prepubli ... |
8-3-2018 at 12:01 by: Pumukli |
Borohydride No offence taken, at all! What if you U2Ud me the address of your source? I'd rather pay less if I c ... |
5-3-2018 at 02:28 by: Pumukli |
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