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2-chloroethanol
@GC- your method of refluxing disulphur dichloride and glycol looks extremly tempting!
should you b ...
31-7-2009 at 13:27
by: Picric-A
2-chloroethanol
Well if you are saying 1 works, two must work. 2 is simply forming the HOCl in situe by the reaction ...
30-7-2009 at 16:32
by: Picric-A
2-chloroethanol
I have read about many ways to produce this compound, some look more simple than others.
2-chloroe ...
30-7-2009 at 15:59
by: Picric-A
Ozonelabs- Synthesis of Methyl Orange
Nice clear write-up on a extremly usefull indicator!
well done!
28-7-2009 at 15:43
by: Picric-A
4-AminoBenzoic Acid from PET
[/rquote]

Ammonium Hydrogen Biterephthalate[/rquote]

No, the correct naming is ammonium hydrog ...
27-7-2009 at 12:17
by: Picric-A
4-AminoBenzoic Acid from PET
I will make a PDF when im next free.
Verification, purity analysis ect, was dont with m.p. test
26-7-2009 at 01:11
by: Picric-A
4-AminoBenzoic Acid from PET
Depolymerization of PET using the ethylene glycol/NaOH mixture documented in preppublication, produc ...
25-7-2009 at 09:40
by: Picric-A
ethanolamine
I thought that if there was a chance the alcohol group woiuld be attacked i could protect it with an ...
25-7-2009 at 01:43
by: Picric-A
ethanolamine
[rquote=158491&tid=12575&author=kclo4]It would be easy to determine if it formed, wouldn't i ...
24-7-2009 at 14:43
by: Picric-A
ethanolamine
Will 2-Chloroethanol react with aqeous ammonia to produce ethanolamine?
thanks,
24-7-2009 at 13:03
by: Picric-A
Synthesis of 3-Nitrophthalic Acid; Luminol Precursor
Can 3-nitrophthalhydrazide be reduced with anything other than Sodium dithionite?
Would NaOH/Al wor ...
21-7-2009 at 02:16
by: Picric-A
Propofol Synthesis
The only thing i can think of off the top of my head is dinitrate the phenol, mono-reduce the ortho ...
18-7-2009 at 15:46
by: Picric-A
Propofol Synthesis
Sorry yes i should of put this is begginings, however i thought this is a very organic syntheis.
I ...
18-7-2009 at 15:35
by: Picric-A
Propofol Synthesis
Starting from one mole of Phenol, could i react it with two moles of Isopropyl chloride to produce P ...
18-7-2009 at 15:10
by: Picric-A
Storage of Fuming Nitric acid
Relieveing pressure would release a cloud of toxic/corrosive fumes, along with weakening the acid, a ...
14-6-2009 at 07:38
by: Picric-A
Storage of Fuming Nitric acid
Why dont you just make it as and when needed?
that way you dont have to worry about overpressure/co ...
14-6-2009 at 07:28
by: Picric-A
Reducing and Diazotization problems
I am attempting to synthesis Resorcinol from Benzene.
To do this i dinitrate benzene with fuming ni ...
14-6-2009 at 07:25
by: Picric-A
Terephthalic acid from PET
@ DJF90 - I guessed one could substitute the conc NaOH soloution for the easier NaOH dissolved in et ...
27-4-2009 at 03:59
by: Picric-A
Nitric Acid Synthesis
Conc. HNO3 has been stored in aluminium containers as they are so strongly oxidising they are not at ...
21-4-2009 at 04:57
by: Picric-A
Terephthalic acid from PET
Has anybody got access to this article? http://pubs.acs.org/doi/abs/10.1021/ie010563z
Seems a good ...
20-4-2009 at 09:57
by: Picric-A
tin salts thread
Hydrolosis of Tin Chlorides only occurs in either hot water or an exess of water.
You can safly hyd ...
16-4-2009 at 15:32
by: Picric-A
tin salts thread
Tin compounds are very usefull indeed.
I have recently been using acidic stannous chloride to reduc ...
5-4-2009 at 06:24
by: Picric-A
The short questions thread (1)
@ Panache- Release HI from the KI using conc phosphoric acid, and run the vapours through a NaOH or ...
1-4-2009 at 12:03
by: Picric-A
The short questions thread (1)
Potassium hydroxide used to be manufactured industrially by boiling an aquous soloution of wood ash ...
9-3-2009 at 11:05
by: Picric-A
Acetone Uses
Im sure plenty of people have jobs in working out what fuels make cars more efficient,
If acetone ...
28-2-2009 at 10:20
by: Picric-A
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