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methanesulfonic acid
Could it possibly be synthesized from methylsulfonylmethane (MSM)? It is available as a joint supple ...
26-8-2008 at 19:45
by: 497
From where are you?
Alaska, USA. Its nice for reactions that require cooling :P
25-8-2008 at 11:02
by: 497
Allstar Lab?
This is very strange, a supplier that sells only the following chemicals: 1,4 butanediol, toluene, a ...
24-8-2008 at 21:11
by: 497
Methyl Ethyl Ketone Peroxide
In the conditions you just gave there would still be plenty of water present. Maybe less than normal ...
24-8-2008 at 17:00
by: 497
Methyl Ethyl Ketone Peroxide
As far as I know the reaction requires acidic conditions to proceed. Then again I've never heard of ...
24-8-2008 at 12:02
by: 497
Methyl Ethyl Ketone Peroxide
I don't see why that wouldn't work as long as you neutralized all the acid. That would take quite a ...
21-8-2008 at 17:40
by: 497
Propylene (oxide) synthesis
Its fine if you want to derail it. The thread was intended for anything involving propylene and/or p ...
20-8-2008 at 01:33
by: 497
Propylene (oxide) synthesis
Until I knew it would work, I would not attempt a charge quite that big. If it failed to detonate it ...
19-8-2008 at 20:41
by: 497
Propylene (oxide) synthesis
I wasn't involved in that, and I agree it is not really mad science. One of them (there were actuall ...
19-8-2008 at 11:02
by: 497
Propylene (oxide) synthesis
@ Squirrel
What are you talking about? Toxic compared to what? All the MSDS reccomends is safety g ...
18-8-2008 at 23:12
by: 497
Regarding the use of home glassware as lab glassware
I've boiled down battery acid in a 1 L bomex flask at least 10 times with no problems. At first I tr ...
18-8-2008 at 11:40
by: 497
Propylene (oxide) synthesis
Yes I know its nasty stuff... 200 ppm for 8 hours begins to be toxic IIRC. I'm also considering 1,2 ...
18-8-2008 at 10:51
by: 497
Propylene (oxide) synthesis
@ MJP Yes someone already said propylene was available at welding stores. I have taken that into c ...
18-8-2008 at 09:49
by: 497
Propylene (oxide) synthesis
I read a paper about the decomposition products of PP a while ago. It resulted a soup of maybe 30 di ...
17-8-2008 at 13:41
by: 497
Propylene (oxide) synthesis
I wonder if it would be possible to produce the HCl in situ with NaHSO4 and NaCl(or any other suitab ...
16-8-2008 at 09:45
by: 497
Propylene (oxide) synthesis
Thank you, I looked for the procedure on google books and was unable to find any that were viewable. ...
4-8-2008 at 14:17
by: 497
Propylene (oxide) synthesis
Thanks Polverone, I will do that.
A good patent on continuous vapor phase alchohol dehydration is U ...
2-8-2008 at 18:03
by: 497
Propylene (oxide) synthesis
I like that idea Polverone, it just requires bubbling HCl through hot propylene glycol? Do you know ...
2-8-2008 at 13:08
by: 497
Propylene (oxide) synthesis
Hmm yes that may be the best option. Yeild will probably be worse with low pressure but that doesn't ...
2-8-2008 at 04:29
by: 497
Propylene (oxide) synthesis
What is a practical OTC source of propylene? There are many options that I see, few look usable thou ...
2-8-2008 at 04:06
by: 497
What reagent would you like to see an illustrated guide for?
Aww come on! Just plain old potassium??? :P

Really that would be quite interesting. What do you p ...
1-8-2008 at 11:00
by: 497
What reagent would you like to see an illustrated guide for?
Personally I would most like to see 1,2 Butylene Oxide. Another big one is DCM. While you're at it T ...
1-8-2008 at 02:53
by: 497
Methyl Ethyl Ketone Peroxide
;) I figured you'd like that. Lets see, I'll have to dig up the notepad file I wrote up to keep thin ...
19-7-2008 at 01:26
by: 497
Preparation of elemental phosphorus
So today I went to the store in search of some NaPO3. The only Calgon they had was non phosphate cra ...
19-7-2008 at 01:14
by: 497
Methyl Ethyl Ketone Peroxide
Well I'll let you try the DBSP in blender idea for yourself, considering the fairly high percent NG ...
19-7-2008 at 00:08
by: 497
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