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Sodium methoxide from methanol, NaOH and Aluminium
I think the reaction forming sodium aluminate would be much faster than the reaction forming sodium ...
19-10-2020 at 14:09
by: njl
Ferric chloride and HCl halogenation of hydroxyl groups
The conditions might be too harsh, but I would even try NaCl and H2SO4 to avoid as much water in the ...
19-10-2020 at 14:00
by: njl
Ferric chloride and HCl halogenation of hydroxyl groups
I didn't even realize that was your post, my bad.
19-10-2020 at 10:36
by: njl
Ferric chloride and HCl halogenation of hydroxyl groups
I am a bit confused because while the primary alcohol shouldn't be chlorinated that much just by aqu ...
19-10-2020 at 09:35
by: njl
Ferric chloride and HCl halogenation of hydroxyl groups
The reaction you're working is documented, there will be product with or without ferric chloride (un ...
19-10-2020 at 08:34
by: njl
EMP device for pesky drones
I wonder if those deauthors that are so common now could interfere with a wifi controlled drone? I t ...
19-10-2020 at 06:05
by: njl
Ferric chloride and HCl halogenation of hydroxyl groups
To be honest, your experiment would be more valuable than my input. Given the availability of the re ...
19-10-2020 at 06:03
by: njl
lead azide trouble
You say you used lab grade NaN3. What about dextrin? Being a natural product it might have some impa ...
19-10-2020 at 05:55
by: njl
Hexane from Adipic Acid?
What I was getting at is that you would need far more exotic reagents to go through with this proced ...
19-10-2020 at 05:51
by: njl
Hexane from Adipic Acid?
How were you planning on reducing the acid to the alcohol?
18-10-2020 at 15:34
by: njl
Ferric chloride and HCl halogenation of hydroxyl groups
I don't think its ability to dissolve gold is a good indicator of chlorinating strength for organic ...
18-10-2020 at 10:19
by: njl
How to seal a threaded stainless steel retort ?
Why not seal with teflon tape?
16-10-2020 at 08:55
by: njl
Ballistic gel
How do you know NaClO doesn't work?
16-10-2020 at 08:51
by: njl
Aluminum oxide (sapphire) glassware?
[rquote=646592&tid=156330&author=Fyndium]Oh well.. So why are there no ALON glassware yet? : ...
16-10-2020 at 08:48
by: njl
Knock out hazards 2.0
An organic nitrite, vitamin b, and sodium thiosulfate if I recall correctly. All of which are OTC.
13-10-2020 at 09:40
by: njl
m-Tolunitrile
I suppose so, what I had in mind was oxidation to the acid and then amide formation with diethylamin ...
13-10-2020 at 06:05
by: njl
m-Tolunitrile
I guess you could make DEET? If you for some reason felt so inclined.
13-10-2020 at 05:24
by: njl
Preparation of cyanides
Double displacement in aqueous solution with silver nitrate.
8-10-2020 at 14:28
by: njl
Azobisisobutyronitrile (AIBN) Synthesis Options
IDK if you're still planning on doing this but the cyanohydrin is far more dangerous than freebase h ...
8-10-2020 at 06:26
by: njl
T-Shirt Size (for secret santa)
Large
8-10-2020 at 06:22
by: njl
Questions about the Hofmann Rearrangement.
It shouldn't really matter. It's generally good practice to deal with solutions but in this case it ...
5-10-2020 at 17:27
by: njl
Drying Aldehydes properly - How to do it?
Yes that would probably work. Why not dissolve in a dry solvent and add a drying agent? That would b ...
5-10-2020 at 05:32
by: njl
Acetone reaction with chlorides?
I have never heard of the reaction between Chlorides and acetone but Calcium Chloride is known to fo ...
5-10-2020 at 04:58
by: njl
Concise, Step by step Reaction Scheme for Dimethyltryptamine
I have had success with tryptamine/formaldehyde/formic acid as determined by melting point and activ ...
2-10-2020 at 07:44
by: njl
Aluminium metal + base as a dehydrating agent?
Lots of things CAN be used as dehydrating agents, but its just not worth it most of the time. You ca ...
2-10-2020 at 06:09
by: njl
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