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DDNP & related compounds: The über thread! Quite possibly the product consists mostly of pDDNP instead of the DDNR, although I wonder why in th ... |
23-7-2015 at 05:18 by: nitro-genes |
Perchloric acid and bismuth It may be that only a certain strenght of perchloric acid is needed to act as an oxidizer instead of ... |
23-7-2015 at 01:33 by: nitro-genes |
Perchloric acid and bismuth Chlorate and acid to generare chloric acid is a good idea. Its extremely
unstable at higher conce ... |
22-7-2015 at 18:33 by: nitro-genes |
DDNP & related compounds: The über thread! Regarding the synthesis of DDNR:
In a recent experiment I heated 3 grams of isopicramic acid with ... |
22-7-2015 at 17:51 by: nitro-genes |
DDNP & related compounds: The über thread! First of all, thanks to Boffis and Philou for the requested hydroxylamine synthesis from nitrite. I ... |
18-7-2015 at 13:47 by: nitro-genes |
High speed cameras In case of a nuclear event, at least you don't need external lighting.
Speaking of light...so ... |
17-7-2015 at 15:56 by: nitro-genes |
Perchloric acid and bismuth The superoxide crust forms very slowly under mineral oil, in which case only very small amounts of o ... |
17-7-2015 at 02:20 by: nitro-genes |
Unconventional Shaped Charges Like this (forgive my terrible drawing skills):
So the red colour representing some 3 mm piece o ... |
16-7-2015 at 08:56 by: nitro-genes |
Perchloric acid and bismuth Interesting, maybe bismuth is unique in being able to reduce perchloric acid to lower oxychlorites s ... |
16-7-2015 at 08:10 by: nitro-genes |
Unconventional Shaped Charges With these charge sizes, it might also help to give the detonator a thick bottom of foam or plastic ... |
16-7-2015 at 07:48 by: nitro-genes |
DDNP & related compounds: The über thread! Something completely different:
Would something along these lines possibly work? |
10-7-2015 at 13:59 by: nitro-genes |
Possible route to resorcinol from Tylenol / Paracetamol? @ Boffis and Rosco:
The paper regarding nitrite mediated nitration of acetaminophen to the suppos ... |
9-7-2015 at 01:31 by: nitro-genes |
Unconventional Shaped Charges A very interesting way of possibly making spherical ETN (PERFORM REMOTE though!!!) that I thought of ... |
7-7-2015 at 12:02 by: nitro-genes |
DDNP & related compounds: The über thread! Great finds Rosco! Initiating power equal to lead azide for the potassium salt of DDNR sounds great, ... |
26-6-2015 at 14:23 by: nitro-genes |
DDNP & related compounds: The über thread! 1 gram of the purified isopicramic acid (IPA) was diazotized using three different methods, stirring ... |
25-6-2015 at 03:42 by: nitro-genes |
easy way to synthesis nitroglycrine Should work, but finely powder the KNO£ before dissolving it in the sulfuric acid and make sure all ... |
24-6-2015 at 09:56 by: nitro-genes |
DDNP & related compounds: The über thread! One curious thing I want to look into is whether an insoluble carbonate salt/adduct can be formed fr ... |
22-6-2015 at 16:52 by: nitro-genes |
DDNP & related compounds: The über thread! Thanks, also would be interesting to see what the product will be after diazotization. Hopefully, th ... |
22-6-2015 at 13:51 by: nitro-genes |
DDNP & related compounds: The über thread! I was thinking, maybe it doesn't need complete neutralization at all. Maybe
adding ice and a very ... |
22-6-2015 at 07:57 by: nitro-genes |
DDNP & related compounds: The über thread! Thanks for your ideas about performing the reactions. The more I think about it, using AN for the ni ... |
20-6-2015 at 15:10 by: nitro-genes |
DDNP & related compounds: The über thread! Yeah, sorry...you were talking about crystallizing ammonium DNAc directly from the neutralized nitra ... |
19-6-2015 at 17:16 by: nitro-genes |
DDNP & related compounds: The über thread! Thanks for the info, the 250 ml and 2 grams isopicramic was based on this, but it certainly didn't d ... |
19-6-2015 at 12:37 by: nitro-genes |
DDNP & related compounds: The über thread! Sounds familiar
For the solubilty test in diluted SA, it seemed a good idea to start with very ... |
19-6-2015 at 12:16 by: nitro-genes |
DDNP & related compounds: The über thread! Yeah your right, was the colour recrystallized this way a sort of bright yellow, orange/brown or dar ... |
19-6-2015 at 06:10 by: nitro-genes |
DDNP & related compounds: The über thread! Here a picture of 5 grams of DNAc reacting O/N at room temperature in 20 ml 68% nitric acid (left) a ... |
19-6-2015 at 04:01 by: nitro-genes |
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