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ketone-bisulfite product recrystallization
[quote][i]Originally posted by Baphomet[/i]
But if we're trying to avoid a cumbersome vac setup by ...
18-2-2007 at 19:15
by: pantone159
ketone-bisulfite product recrystallization
[quote][i]Originally posted by Sergei_Eisenstein[/i]
It's not a bad idea to wash the adduct with et ...
18-2-2007 at 15:47
by: pantone159
ketone-bisulfite product recrystallization
[quote][i]Originally posted by Magpie[/i]
It has always been my impression that sodium metabisulfit ...
18-2-2007 at 15:14
by: pantone159
1,3-propanediol, aka "Bio-PDO"
It occurs to me that 1,3-propanediol, HO-CH2-CH2-CH2-OH, aka "Trimethylene glycol" ought to be a ver ...
18-2-2007 at 11:13
by: pantone159
Heat and Cold of dissolution....
It takes energy to separate, e.g., the NH4+ and NO3- ions from each other in the lattice in the soli ...
18-2-2007 at 10:42
by: pantone159
No good recrystallization
I never posted this result (maybe should have), but I did try and recrystallize the acetone-bisulfit ...
17-2-2007 at 22:53
by: pantone159
Decarboxylation of oxaloacetic acid
Note: The decarboxylation of the beta-keto acid formed by oxidizing does NOT yield malonic acid, bu ...
15-2-2007 at 17:59
by: pantone159
Recovery of Cesium salts from Pollucite ore.
One link offering to sell pollucite samples, $25...
It doesn't say how much, though.

http://www. ...
10-2-2007 at 16:00
by: pantone159
A good digital scale
Also look at postal scales. I bought one at a local office supply store for around $US 30, it displ ...
9-2-2007 at 12:32
by: pantone159
Separation of Acetone and Nitroethane
[Edited on 8-2-2007 by pantone159]
7-2-2007 at 21:49
by: pantone159
I hope this isn't a stupid question.....
[quote][i]Originally posted by woelen[/i]
Then we enter the field of pure mathematics. [/quote]

...
7-2-2007 at 00:40
by: pantone159
its TEXAS law, partner
[quote][i]Originally posted by unionised[/i]
I note that the Texas Authorities consider you a meth ...
6-2-2007 at 11:45
by: pantone159
Methyl Vanillyl Ketone
MDP2P has the 3-4 positions connected by a R3-O-CH2-O-R4 ring, where R3 is the 3 position and R4 the ...
3-2-2007 at 22:32
by: pantone159
Methyl Vanillyl Ketone
Vanillin is 4-hydroxy-3-methoxy-benzaldehyde, i.e.,

3-OMe,4-OH-Ph-C(=O)-H

so I'd (now) guess ( ...
3-2-2007 at 18:35
by: pantone159
Making solutions from solutions
I second the suggestion of measuring things by weight, not volume.

Volumes don't always combine l ...
3-2-2007 at 00:29
by: pantone159
UK ARRESTS - kno3.com - user Kerry-Ann Shanks
A couple of other stories about this...

http://news.bbc.co.uk/2/hi/uk_news/scotland/tayside_and_c ...
31-1-2007 at 10:55
by: pantone159
Ceric(IV) sulfate vs ammonium nitrate
What are the advantages/disadvantages of ceric(IV) sulfate vs ceric(IV) ammonium nitrate for the BZ ...
30-1-2007 at 20:16
by: pantone159
Briggs-Rauscher Oscillating Reaction
Gas Evolution Oscillating Reactions:

Shakhashiri 7.13 also describes this:
A: Dissolve 26g ammon ...
30-1-2007 at 11:00
by: pantone159
Briggs-Rauscher Oscillating Reaction
I think the kit is a good deal. For around $10, you get 5g of both malonic acid and sodium iodate, ...
29-1-2007 at 19:40
by: pantone159
Briggs-Rauscher Oscillating Reaction
I picked up 'The Facinating Oscillating Reaction Kit', made by Universe of Science http://www.univer ...
29-1-2007 at 17:53
by: pantone159
methylamine
Has anybody tried using n-butanol for the separation? The OrgSyn synthesis mentions this as good, s ...
21-1-2007 at 10:37
by: pantone159
Epsom Salts
I make my drying agent from MgSO4-7H2O, I put it in the oven for 2 hours at (nominally) 525 F (275 C ...
20-1-2007 at 11:24
by: pantone159
Mad Science at the max, where do you draw the line?
Distilling Cs metal does sound facinating. I'd expect that you'll end up coating the inside of the ...
18-1-2007 at 18:31
by: pantone159
Distillation set questions
You can't put erlenmeyer flasks under vacuum.
16-1-2007 at 18:22
by: pantone159
methylamine
Could pH 8 not be high enough???

What else could the stuff be? - even if NH4Cl it should smell wh ...
15-1-2007 at 20:00
by: pantone159
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