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The Short Questions Thread (4) I have stupid question as I am not very deeply into practise because im a beginner. If i have to ste ...	24-5-2018 at 11:17 by: mackolol
triphenylphosphine oxide preparation I want to make green triboluminescent compound which is Mn(Ph3PO)2Br2 complex	21-5-2018 at 08:02 by: mackolol
triphenylphosphine oxide preparation Hi, I want to make triphenylphosphine oxide from TPP. I know that TPP gets easily oxidized even by a ...	20-5-2018 at 00:29 by: mackolol
Whats the most dangerous chemical you've ever synthesized? Yesterday i tried to remove my pbr5 from pcl3, pbr3 mixture so i heated it up but nothing happened. ...	15-5-2018 at 01:30 by: mackolol
Oxalyl Chloride Challenge Hi, today i tried synthesis of oxalyl chloride by chlorination of ethylene glycol. I have read an ar ...	14-5-2018 at 10:01 by: mackolol
Modified Patent Route to Oxalyl Chloride What about making it by Example III described in this patent. Firstly esterification of ethylene gly ...	9-4-2018 at 03:15 by: mackolol
nitration of xylene using HNO3/DCM mixture Yup i'm trying to make lidocaine and it would be great if it was pure enough to test it safely on my ...	10-3-2018 at 10:15 by: mackolol
Triethyl borate and triisopropyl borate I want to play with boric acid esters but since trimethyl borate forms an azeotrope with methanol, w ...	8-3-2018 at 14:44 by: mackolol
nitration of xylene using HNO3/DCM mixture Hi, I want to make 2,6 xylidine and i dont have better idea than to make it from mixed xylenes. Howe ...	28-2-2018 at 08:35 by: mackolol
Destroying THF peroxide with ascorbic acid The yield is gammabutyrolactone in 60% yield. Doesnt the feso4 destroy peroxides? Or i will must che ...	25-1-2018 at 12:38 by: mackolol
Destroying THF peroxide with ascorbic acid So do FeSO4 destroys preoxide? Because i want to oxidise THF with FeSO4 and H2O2 and I'm wonder if i ...	25-1-2018 at 08:23 by: mackolol
Easy Isopropyl Nitrate Let me bring this thread to live. Yesterday i tried to make IPN because it interested me. I did this ...	7-1-2018 at 10:37 by: mackolol
Separating phthalic acid isomers @Aga; I am attempting this experiment as i said my last attempt was hydrolysing m xylene sulphonic a ...	31-12-2017 at 00:39 by: mackolol
useful compounds You can try benzocaine synthesis as it is easily made anaesthetic.	30-12-2017 at 13:50 by: mackolol
Separating phthalic acid isomers @Boffis; Yes i got same black product in all my reactions (w using 98 and 85% h2so4) and it smells l ...	30-12-2017 at 13:46 by: mackolol
Separating phthalic acid isomers Today i did this reaction one more time and took 40ml of mixed xylenes and 20ml of 98% h2so4 run in ...	26-12-2017 at 13:31 by: mackolol
Separating phthalic acid isomers I have done a little research and I found this https://www.google.com/patents/US2348329. According t ...	21-12-2017 at 12:34 by: mackolol
Separating phthalic acid isomers Youre right i took somewhere around 5ml of watet and about 20ml sulphuric acid (i dont really rememb ...	15-12-2017 at 06:58 by: mackolol
Separating phthalic acid isomers Today i did the reaction and used as I said 36ml of mixed xylenes and 27ml h2so4 diluted to 80%. Aft ...	9-12-2017 at 12:30 by: mackolol
Separating phthalic acid isomers Ok now i see i used 60ml of conc h2so4 what makes 80 ml of 80% sulph acid and only 36ml of xylene ac ...	8-12-2017 at 13:06 by: mackolol
Separating phthalic acid isomers I have done this reaction yesterday but i used 80% sulphuric acid. While dilution of h2so4 i didnt w ...	7-12-2017 at 05:30 by: mackolol
Purifying luminol Will it be OK if i use spirit vinegar (food acetic acid)? Because i dont want to use solid acid beca ...	4-12-2017 at 09:36 by: mackolol
Purifying luminol Thanks a lot	2-12-2017 at 08:12 by: mackolol
Purifying luminol I have water/acetone luminol solution and im wondering if it wont decompose when i distill it off to ...	2-12-2017 at 07:04 by: mackolol
Armstrong mix that does not explode on impact. why? Making armstrong's mix isnt good idea. If reagents are pure and dry if explodes after mixing. Its ex ...	20-11-2017 at 10:47 by: mackolol
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