| Search |
| [Next Page] |
DDNP & related compounds: The über thread!
There is definitely enough ammonia value present for the Neutralization scheme "Plan A" to work if i ... |
20-6-2015 at 17:00
by: Rosco Bodine |
DDNP & related compounds: The über thread!
Yes I understand the scheme used and described for variations before, but this is simply an idea tha ... |
20-6-2015 at 12:07
by: Rosco Bodine |
DDNP & related compounds: The über thread!
[rquote=409785&tid=439&author=nitro-genes]Yeah, sorry...you were talking about crystallizing ... |
19-6-2015 at 20:53
by: Rosco Bodine |
DDNP & related compounds: The über thread!
Trust but verify on the reported data. It is odd how the ammonium salt for the acetylisopicramic ac ... |
19-6-2015 at 13:07
by: Rosco Bodine |
DDNP & related compounds: The über thread!
[rquote=409749&tid=439&author=nitro-genes]Sounds familiar
For the solubilty test in dilu ... |
19-6-2015 at 12:24
by: Rosco Bodine |
DDNP & related compounds: The über thread!
[rquote=409701&tid=439&author=nitro-genes]Sure, I'll give it a try, though it may not be as ... |
19-6-2015 at 06:43
by: Rosco Bodine |
DDNP & related compounds: The über thread!
Here is a solubility chart for sodium sulfate which is soluble to the extent of 4.7% (anhydrous basi ... |
18-6-2015 at 18:36
by: Rosco Bodine |
DDNP & related compounds: The über thread!
The presence of the accumulating soluble ammonium bisulfate byproduct and unreacted dissolved ammoni ... |
18-6-2015 at 17:34
by: Rosco Bodine |
DDNP & related compounds: The über thread!
I have a jug of 68% HNO3 on hand, so when I do this I'll probably just use the same method as the Le ... |
18-6-2015 at 16:46
by: Rosco Bodine |
DDNP & related compounds: The über thread!
I think you may have an impure sample because of the heavier residue. The oxygen balance is identic ... |
18-6-2015 at 14:43
by: Rosco Bodine |
DDNP & related compounds: The über thread!
Acetic acid may help with the solubility issues. The cycling of the materials through manipulations ... |
18-6-2015 at 13:38
by: Rosco Bodine |
DDNP & related compounds: The über thread!
When some good solubility data is available for all the materials being manipulated it will be helpf ... |
18-6-2015 at 11:29
by: Rosco Bodine |
DDNP & related compounds: The über thread!
[rquote=409586&tid=439&author=Hennig Brand]That data sheet doesn't inspire a lot of confiden ... |
18-6-2015 at 05:16
by: Rosco Bodine |
DDNP & related compounds: The über thread!
Here is the link from when nitro-genes was experimenting with this
http://www.sciencemadness.org/t ... |
17-6-2015 at 17:37
by: Rosco Bodine |
DDNP & related compounds: The über thread!
It is easy enough to test. Put a weighed amount of dry isopicramic acid into solution using the mi ... |
17-6-2015 at 16:43
by: Rosco Bodine |
DDNP & related compounds: The über thread!
Yeah I read that but it is not certain that is accurate. Check the spot test described in the Chemi ... |
17-6-2015 at 13:38
by: Rosco Bodine |
DDNP & related compounds: The über thread!
With all the excess nitrate you probably made the 2,3,5,6,-tetranitro derivative 
so this could ge ... |
17-6-2015 at 13:24
by: Rosco Bodine |
DDNP & related compounds: The über thread!
You need to follow nitro-genes on that one, and maybe say the Shepards prayer
(Alan Shepard)
... |
17-6-2015 at 13:08
by: Rosco Bodine |
DDNP & related compounds: The über thread!
Yeah I saw that one coming. Don't worry about solubility losses too much for isopicramic acid, as t ... |
17-6-2015 at 12:34
by: Rosco Bodine |
DDNP & related compounds: The über thread!
You and nitro-genes can see better what you have encountered while actually doing the reactions hand ... |
17-6-2015 at 12:13
by: Rosco Bodine |
DDNP & related compounds: The über thread!
I plotted all the reported nitration mixtures and water contents and solids content and sort of inte ... |
17-6-2015 at 11:19
by: Rosco Bodine |
DDNP & related compounds: The über thread!
Yippeeeeeeee! 
https://www.youtube.com/watch?v=Ah_a5-oU7gM
<iframe width="640" height= ... |
17-6-2015 at 09:11
by: Rosco Bodine |
DDNP & related compounds: The über thread!
The relatively mild conditions for synthesis under which the p-DDNP and its precursors dinitroparace ... |
17-6-2015 at 06:59
by: Rosco Bodine |
DDNP & related compounds: The über thread!
This thread has evolved into what is absolutely state of the art cutting edge Vanguard kind of beake ... |
16-6-2015 at 20:04
by: Rosco Bodine |
DDNP & related compounds: The über thread!
There shouldn't be any issue with disassociation of the isopicramic acid sulfate upon dilution, IIRC ... |
16-6-2015 at 17:29
by: Rosco Bodine |
| [Next Page] |
