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Lactoferrin conversion Apolactoferrin
Getting the proper dialysis tubing on such a large scale might be an issue. Otherwise it seems OK. B ...
26-11-2018 at 15:06
by: Metacelsus
Making potassium cuprate(III)
I would be concerned about the potassium metal reducing the copper (II) oxide to metallic copper. It ...
25-11-2018 at 00:51
by: Metacelsus
I bought a Mass Spec!
Wow, this could potentially be a great resource for amateur chemists. I'm very impressed.

[rquote ...
20-11-2018 at 14:36
by: Metacelsus
Can you use Water as an eluent on an Alumina column?
It should be fine to elute. pH 10 isn't high enough to dissolve alumina.
20-11-2018 at 00:12
by: Metacelsus
Preparation of Al(HSO4)3
You could try mixing aluminum sulfate (Al2(SO4)3) with sulfuric acid.
16-11-2018 at 01:15
by: Metacelsus
How to push out (extrude) wet Silica in Column Chromatography in one piece like a sausage?
He probably just applied compressed air to the bottom of the column instead of the top.

However, ...
13-11-2018 at 23:45
by: Metacelsus
Air cusion micropipette - which solvents i can use
I've used a micropipettor with chloroform before. I expect that it could handle many solvents. I wou ...
13-11-2018 at 08:45
by: Metacelsus
How can I synthesise 2-methyl-4chlorophenol?
You can try chlorinating 2-methylphenol (aka o-cresol). This will produce a mixture of the 4-chloro ...
9-11-2018 at 10:46
by: Metacelsus
Tricyclopentyl alcohol treated with HCL
OP said tetrasubstituted alkene, that one is trisubstituted.

This would be the correct tetrasubs ...
7-11-2018 at 23:52
by: Metacelsus
Hazard Concerns: Melting FEP Fluropolymer?
Breathing ammonia isn't very good for you either.
1-11-2018 at 08:46
by: Metacelsus
Borosilicate under pressure?
Yes, a blast shield is highly advisable (and something which I forgot to mention in my post above!)
...
30-10-2018 at 10:09
by: Metacelsus
4-Benzylpiperidine
It's quite common to leave a reaction running overnight (say, 20:00 to 8:00 the next day).
29-10-2018 at 23:03
by: Metacelsus
Borosilicate under pressure?
I've used thick-walled borosilicate pressure vessels at 150 °C and 10 bar pressure. I'm talking abo ...
29-10-2018 at 23:02
by: Metacelsus
"Broken" thermometre
I think Phlostigon intends for centrifugation to move the separated part down towards the rest of th ...
26-10-2018 at 10:48
by: Metacelsus
Production of pharmaceutical grade (USP, EP, BP, JP) compounds
[rquote=545802&tid=98867&author=DavidJR]
[rquote=545798&tid=98867&author=Fulmen]
W ...
22-10-2018 at 11:05
by: Metacelsus
Reaction skill tree
[rquote=542932&tid=97160&author=Sulaiman]C + O[sub]2[/sub] = CO[sub]2[/sub] + heat and light ...
12-10-2018 at 14:14
by: Metacelsus
"Friendly" synthesis of Benzyl Dimethyl Carbinol
What about reacting phenyl-2-propanone with dimethylzinc?

:D

More seriously, the Barbier react ...
6-10-2018 at 23:20
by: Metacelsus
Assining IR spec peak values
[rquote=541190&tid=96106&author=tekkado]would any one be able to privide some info for the a ...
6-10-2018 at 23:14
by: Metacelsus
Why some languages write compounds' names with anions first?
[rquote=541122&tid=96037&author=DraconicAcid]In French as well- le chlorure de sodium, etc. ...
6-10-2018 at 09:32
by: Metacelsus
Getting a lot of "flooding" messages while trying to post
And even with the "flood prevention" the board is still flooded by spammers :mad:
4-10-2018 at 22:16
by: Metacelsus
Mescaline synthesis
I don't think that reaction will work. Glycerin doesn't add methoxy groups to benzene rings. What wo ...
1-10-2018 at 09:42
by: Metacelsus
NMP - Purification - Ideas?
If you don't have a good enough column, you might be able to selectively hydrolyze the GBL, distill ...
28-9-2018 at 04:55
by: Metacelsus
Dissolving molecular sieves!!??
If it does indeed dissolve sieves, why would it leave a few sieves behind? I would expect either:
1 ...
28-9-2018 at 04:48
by: Metacelsus
Does KClO3 oxidation ignition not work under vacuum ?
I know that the Rosetta/Philae spacecraft had an issue with harpoons not firing because the pyrotech ...
17-9-2018 at 12:53
by: Metacelsus
Preparation of Dimethyl Sulfate Discussion
For methylation of phenols, dimethyl sulfate gives quantitative yields. I don't know about other met ...
11-9-2018 at 20:11
by: Metacelsus
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