| Search |
| [Next Page] |
Isocyanate synthesis via halide displacement
I found another paper that claims the reaction of alkyl chlorides and isocyanate does yield organic ... |
20-11-2020 at 10:53
by: njl |
Otc oxalyl chloride success?
Good stuff. Maybe DMSO as a cosolvent? It's high boiling too so maybe you could squeeze out a bit mo ... |
20-11-2020 at 10:36
by: njl |
Crystallisation - truly a dark art
I suppose it isn't very special relative to the crystallization you mentioned, but I love seeing nit ... |
20-11-2020 at 07:17
by: njl |
2020 Secret Santa [tell everyone how it went]
Not sure if I'm supposed to talk about it, but I received my package! I got a new flask! FYI, it is ... |
20-11-2020 at 06:48
by: njl |
Isocyanate synthesis via halide displacement
Thanks atara for the insight. While isocyanates are dangerous, I would never isolate one. I think th ... |
19-11-2020 at 16:44
by: njl |
Isocyanate synthesis via halide displacement
@draconicacid that's what I am confused about. I have read in some papers that the isocyanate ion wi ... |
19-11-2020 at 09:48
by: njl |
Isocyanate synthesis via halide displacement
Other than the fact that expanding the communities arsenal is a good thing by itself:
The NaDFA r ... |
19-11-2020 at 09:43
by: njl |
Isocyanate synthesis via halide displacement
Thank you. For those wondering, the paper claims:
The reaction between organic halides or sulfate ... |
19-11-2020 at 07:57
by: njl |
Isocyanate synthesis via halide displacement
In the Kolbe nitrile synthesis, nitriles are formed from alkyl halides via reaction with an alkali c ... |
19-11-2020 at 07:37
by: njl |
Acid Chlorides
Alpha chloro ethers are byproducts of some reactions, chloromethyl-methyl ether being a notable one. ... |
16-11-2020 at 06:23
by: njl |
Conversion of Red Phosphorus to Tetraphosphorus by the Action of Heat
Have you had any luck creating a reusable apparatus? |
15-11-2020 at 10:53
by: njl |
2-butanol from Butanone (MEK)
I think Thiourea dioxide can reduce carbonyls to alcohols. |
14-11-2020 at 10:32
by: njl |
Decarboxylation of L-tryptophan in DMSO
You should try to concentrate the solution first to see if you can get a crop without anymore workup ... |
13-11-2020 at 19:13
by: njl |
reduction with zinc or iron
If you insist on using a dissolving metal reduction then that's ok, but I second thiourea dioxide. V ... |
13-11-2020 at 09:33
by: njl |
Candle Wax Water Explosion Experiment Explantion required
Maybe it's the leidenfrost effect between the hot wax and butane. |
12-11-2020 at 11:00
by: njl |
Convert Sodium Iodide to sodium Iodate? ( Iodi'IDE' -> Iod'ATE')
If you don't want iodate then the SM thread that you linked has an OTC procedure for both NaI and IO ... |
12-11-2020 at 10:36
by: njl |
How to Reduce Trichloromethane to Dichloromethane?
It works (and has been discussed here before) but the yield is awful. You really are better off buyi ... |
12-11-2020 at 07:18
by: njl |
diethyl carbonate (NO PHOSGENE)
I think urea and ethanol can react to ethyl carbamate, so maybe you could go one step further and ge ... |
11-11-2020 at 10:47
by: njl |
Nitromethane synthesis from methylamine
@Opylation I have also done some reading about amine --> nitro and I think going from amine to ox ... |
9-11-2020 at 05:12
by: njl |
Creating a noopept suspension?
Are you using the solution you made as a nasal spray? |
8-11-2020 at 08:12
by: njl |
Hi. Im new here.
Would adding Calcium nitrate to the solution lower the hydroxide concentration via precipitation or ... |
8-11-2020 at 08:05
by: njl |
Acetic anhydride preparation
Could there conceivably be a route to 2-butyne from 2-butanone? In the interest of OTCness. |
5-11-2020 at 11:06
by: njl |
Hydrogenation of Eugenol
I have no idea what you are saying above the words "Regarding raney nickel" so I can't add on to tha ... |
5-11-2020 at 10:41
by: njl |
90 - 99% nitric acid using dichloromethane
What about it... |
5-11-2020 at 10:13
by: njl |
Acetic anhydride preparation
That or the similar synthesis of phenylacetylene via 1,2 dibromoethylbenzene. UC235 has a youtube vi ... |
5-11-2020 at 04:36
by: njl |
| [Next Page] |
