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A new demethylation reagent pair: AlCl3/Thiourea
[quote]Tetrachloroethylene is not something I have though[/quote]

Tetrachloroethylene has to be o ...
28-12-2008 at 02:13
by: 497
Homemade Furnace
Try an oxy-acetylene torch...
25-12-2008 at 22:28
by: 497
Which oxidizers are explosives?
I'm pretty sure chlorate/perchlorate salts on their own are not explosives, with the exception of am ...
24-12-2008 at 02:44
by: 497
Rocket propelled E+W forum SC 'design'
What username did you have? I'm interested in what their justification is.

But I'm not too surpri ...
20-12-2008 at 15:05
by: 497
tert-Butyl Alcohol
I've looked around and have been unable to find any sort of OTC source or synthesis of tert-butyl al ...
12-12-2008 at 01:10
by: 497
Safety Reminder: home chemistry and kids
Damn, I'm glad I don't have any kids to worry about.
9-12-2008 at 19:00
by: 497
The POTENCY of carcinogens.
Interesting data. It leads me to wonder why people get so freaked out about stuff like benzene and C ...
9-12-2008 at 18:14
by: 497
The short questions thread (1)
Iron powder works for that purpose but I'm not sure if that's what they are.
6-12-2008 at 13:42
by: 497
The short questions thread (1)
[quote]
I don't understand are you trying to make phenylmethylamines? Maybe I am just missing somet ...
1-12-2008 at 01:08
by: 497
Alternatives to using a "pipe bomb" for a reaction?
I've seen "bomb" in some older literature, like on OrgSyn. Never "pipe bomb" though..
29-11-2008 at 20:29
by: 497
The short questions thread (1)
[quote]
What is the procedure benzyl bromide --> benzaldoxime? Do you have a ref? [/quote]

W ...
29-11-2008 at 12:17
by: 497
The short questions thread (1)
[quote]
LiAlH4 or diborane reductions (NaBH4/BF3.Et2O, NaBH4/I2, etc) will reduce acetamides to ami ...
23-11-2008 at 18:50
by: 497
The short questions thread (1)
[quote]
497, all you want is 2C-H? [/quote]

Why do you ask? I wouldn't want to do anything illeg ...
23-11-2008 at 12:54
by: 497
The short questions thread (1)
[quote]
Well, you can halomethylate withe acetaldehyde and HX IIRC[/quote]

Great idea! I hadn't ...
23-11-2008 at 05:36
by: 497
The separation of NaHSO4 from NaCl
[quote]
Then add the proper amount of Calcium Sulfate and allow it to react with the Potassium Chlo ...
22-11-2008 at 23:26
by: 497
The short questions thread (1)
[quote]
How would you react the two solids? As a solution/suspension in DMF or similar?[/quote]

...
22-11-2008 at 13:49
by: 497
The separation of NaHSO4 from NaCl
I was going to say something about NH4HSO4 being substantially more soluble than NH4Cl, making frac ...
21-11-2008 at 22:14
by: 497
The separation of NaHSO4 from NaCl
Wow, that's interesting. It makes sense I guess, but I'd never thought about it working that way. I ...
21-11-2008 at 15:41
by: 497
Create propane2ol from Glucose - How to??
[quote]
You can get chloroform from CCl4 by reducing with acid[/quote]

Could you then get CH2Cl2 ...
21-11-2008 at 11:31
by: 497
New Energetic Materials - Current Research
Hah! I know how you feel, one time I read almost the whole DPPP thread... Only to be disappointing i ...
21-11-2008 at 11:28
by: 497
The short questions thread (1)
[quote]
Trimethylglycine doesn't seem very appealling. I would rather go with trimethylphosphate or ...
21-11-2008 at 11:24
by: 497
The short questions thread (1)
Two questions:

Does anyone know a good way of separating 4-methoxyphenol and 1,4-dimethoxybenzene ...
21-11-2008 at 03:19
by: 497
New Energetic Materials - Current Research
It looks like a very interesting little compound.

Here it is:

[Edited on 25-12-08 by The_Davste ...
17-11-2008 at 20:41
by: 497
vacuum
[quote]
It cost nothing and works for years at 20 mmHg[/quote]

Wow do they really do that good? ...
15-11-2008 at 13:18
by: 497
Recirculating aspirator pump for solvent recovery
Yes you could.. But I'm not sure why you'd want to, I think it would start to get extremely viscous/ ...
13-11-2008 at 12:03
by: 497
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