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Reaction mechanism? Anodic oxidation of chloride
If you want elemental electrode reactions, you'll have to look a lot closer than the overall result. ...
25-9-2010 at 08:23
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
[url=http://search.digikey.com/scripts/DkSearch/dksus.dll?Detail&name=HFA3101BZ-ND]These[/url] t ...
24-9-2010 at 23:51
by: 12AX7
Alternative way to make sodium first try
Sodium hydride is a large product of the hydroxide reduction, unfortunately.

Supposedly, doing it ...
24-9-2010 at 23:32
by: 12AX7
Ammonia from H2 and KNO3
H2 should reduce KNO3 at high temperature, possibly while molten.
KNO3 + 4 H2 = KOH + 2 H2O + NH3
...
24-9-2010 at 23:30
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
The noise of a 50 turn #32 coil at 30MHz will be very low indeed. Why? Because the parasitic capac ...
24-9-2010 at 15:21
by: 12AX7
Periodic Table Poster
I had one from Flinn Scientific that had a reasonable bit of data on it.

I've never seen one that ...
23-9-2010 at 20:31
by: 12AX7
Write-up on making pure BaCl2.2H2O
I imagine distillation is necessary. *cough* eww.
23-9-2010 at 20:19
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
[rquote=188111&tid=14365&author=arsphenamine]
At this point, the prospect of running a puls ...
23-9-2010 at 12:13
by: 12AX7
Suggestion please on which fluid to use?
Saltwater solution. Pick salts based on density and toxicity (e.g., Ca is denser than Mg, but Sr is ...
23-9-2010 at 10:44
by: 12AX7
Write-up on making pure BaCl2.2H2O
I had fine results (excepting the turbidity, which settles out) with plain old recrystallization. D ...
23-9-2010 at 10:41
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
My guess is somewhere between 1 and 50W for drive. Maybe more for big samples? The actual absorbed ...
22-9-2010 at 21:51
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
[rquote=188002&tid=14365&author=not_important]
Simple programmable oscillators, even at the ...
21-9-2010 at 20:41
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
Uh, did you notice my scheme? Downconvert the signal to a ~1kHz carrier. Tons of bandwidth. 44kHz ...
21-9-2010 at 20:29
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
Hmm, that diagram shows a lot of leakage. Looks like it would work even better locked inside a few ...
21-9-2010 at 17:39
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
[rquote=187919&tid=14365&author=un0me2]Yes, but I want to be able to hook this up to other m ...
20-9-2010 at 20:10
by: 12AX7
Potassium sulphate insoluble residue...
CaSO4, especially if you are using hard tapwater (but not to the tune of 8%!).

Tim
20-9-2010 at 11:23
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
Why the hell do you need a whole frickin DDS to generate exactly one frequency? Use an LC oscillato ...
20-9-2010 at 07:58
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
[rquote=187796&tid=14365&author=aonomus]I'm not sure if any of you guys have the equipment t ...
19-9-2010 at 10:36
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
Traditionally a simple pulse is applied (rectangular, or maybe rectangular windowed RF), during whic ...
18-9-2010 at 08:25
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
Shielding 35MHz is no big deal, the skin depth (and therefore penetration into shielding) is quite s ...
17-9-2010 at 07:14
by: 12AX7
Capsaicin extraction and isolation
Peruvian? That's a Simpsons reference...
17-9-2010 at 07:10
by: 12AX7
Starting a Science Club at University
Amazingly, at one meeting of Chemistry Club, at my last school, one of the faculty demonstrated nitr ...
15-9-2010 at 15:26
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
Yes, pole pieces.

Yes

YES

YES!!!

Anything else is pure retardery!

Looking for fairly ...
15-9-2010 at 15:24
by: 12AX7
do-it-yourself nuclear magnetic resonance spectroscopy
Plastics are unsuitable as they contain nuclei. Carbon obviously for one, and almost all contain hy ...
13-9-2010 at 11:45
by: 12AX7
Anode for chloride electrolysis ?
Said reactive metals oxidize and passivate under those conditions. A coating is required.

Has an ...
13-9-2010 at 11:38
by: 12AX7
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