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What to do with 6% hydrogen peroxide
I find the urea adduct is the most convenient for concentration of weak H2O2
18-12-2020 at 06:26
by: njl
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Melatonin is one of those things I thought was OTC everywhere since you can get it so easily and che ...
17-12-2020 at 11:43
by: njl
Formaldehyde bisulfite adduct preparation
Maybe an isopropanol/water solvent system would be better for recrystallization. Whenever I can't fi ...
17-12-2020 at 09:35
by: njl
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
FYI, the listed prices on alibaba/aliexpress are more often than not either misleading or downright ...
17-12-2020 at 06:17
by: njl
allyl phenoxyacetate - pineapple scent
THIS is the kind of content I love from the forum. Good shit my man. Obscure ester synthesis is some ...
17-12-2020 at 06:02
by: njl
Sodium Triacetoxyborhydrid from NaBH4 in Benzene **HELP**
Alcohols will react with STAB, but apparently isopropanol reacts slow enough to be a viable reaction ...
15-12-2020 at 10:59
by: njl
Sodium Triacetoxyborhydrid from NaBH4 in Benzene **HELP**
That suggestion was based on the assumption that AcOH is immiscible with benzene, which is incorrect ...
15-12-2020 at 10:04
by: njl
Sodium Triacetoxyborhydrid from NaBH4 in Benzene **HELP**
You need to share more about your preparation and intentions. If you were hoping to use benzene as a ...
15-12-2020 at 09:41
by: njl
Advice on safety for aldol products
Isn't iodoacetone a lachrymator? Or is it too low-boiling?
10-12-2020 at 19:11
by: njl
Everyday Chemistry
Can anyone shed some light on what "FG" means in the linked paper? Also, no developments on my previ ...
10-12-2020 at 09:45
by: njl
Reaction between ethylenediamine and nitrite?
Was there any bubbling during the reaction? That could indicate the loss of N2 via diazotization, gi ...
8-12-2020 at 09:50
by: njl
Reaction between ethylenediamine and nitrite?
Can you provide a reference for this procedure?
8-12-2020 at 07:55
by: njl
CuCl2 workup
Thank you for the replies. I think the sulfate will be the way to go. I wouldn't say it's difficult, ...
4-12-2020 at 06:25
by: njl
CuCl2 workup
I recently made some calcium chloride via the following procedure (that I made up as I went along ba ...
3-12-2020 at 13:34
by: njl
Dxm chemistry
Could you be talking about the Hofmann *elimination*? Because dxm could work as a substrate here, bu ...
3-12-2020 at 09:43
by: njl
Amine alkylation catalysts
Just kidding around :) I don't really understand how ceramics (like Al2O3, SiO2, CuO, TiO2, etc.) wh ...
3-12-2020 at 07:28
by: njl
Dxm chemistry
I'm not personally familiar with the Hofmann degradation but I don't see how that reaction would app ...
3-12-2020 at 07:05
by: njl
Amine alkylation catalysts
I think we're witnessing the birth of an account that will either be very helpful or very annoying. ...
3-12-2020 at 06:56
by: njl
Dxm chemistry
Honestly, I think the ether is the only good starting point since there isn't really any other area ...
2-12-2020 at 06:53
by: njl
Dxm chemistry
I have recently come into possession of a few grams of dextromethorphan freebase for reasons irrelev ...
1-12-2020 at 11:56
by: njl
TFA via oxidation of R-1234yf?
you could add an inert solvent to form a eutectic
1-12-2020 at 06:59
by: njl
Experimental: Alternative to Al/Hg - the Al/Cu
Can anyone provide more references for the activation of aluminum with copper ions? This thread had ...
30-11-2020 at 10:34
by: njl
2020 Secret Santa [tell everyone how it went]
Out of curiosity what is everyones first favorite DEA list 1 item?
30-11-2020 at 07:58
by: njl
Everyday Chemistry
Has anybody heard of urea being converted to ammonium formate? I'm trying to find a renewable source ...
23-11-2020 at 07:20
by: njl
Nitric acid synthesis with bisulfate weirdness.
Distilling under vacuum can reduce NOx formation
23-11-2020 at 05:52
by: njl
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