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Warfarin syntheses
[rquote=682875&tid=159453&author=DocX]And then this thread, where ClearlyNotAtara outlines a ...
2-4-2023 at 12:47
by: Texium
Vacuum Desiccator vs Rotary Evaporator
You can certainly re-use the solvent recovered in a rotovap, so long as you clean the receiving flas ...
2-4-2023 at 12:33
by: Texium
Everyday Chemistry
Yeah for that reaction you shouldn’t have to worry about excess methanol being an issue. Nice.
2-4-2023 at 07:52
by: Texium
Preparation of isobutyrophenone by the addition of isopropyl Grignard reagent to benzonitrile (Photo-assay)
I wouldn’t recommend plastic syringes with rubber seals. The ones I use are all HDPE with no rubbe ...
2-4-2023 at 07:09
by: Texium
Does Mg react with carbonates?
[rquote=682840&tid=159432&author=blogfast25][rquote=682839&tid=159432&author=Texium] ...
31-3-2023 at 12:48
by: Texium
Does Mg react with carbonates?
And these are indeed thermite-style reactions being discussed, so the SERs are quite relevant in thi ...
31-3-2023 at 10:49
by: Texium
Preparation of isobutyrophenone by the addition of isopropyl Grignard reagent to benzonitrile (Photo-assay)
Thanks for the nice write-up! For addition of the reagents to the flask, I recommend you buy some ru ...
31-3-2023 at 07:49
by: Texium
Homemade and Repurposed Lab Gear
[rquote=643557&tid=61783&author=earpain]Now that DCM is gone, I've been plagued by the tedio ...
29-3-2023 at 07:06
by: Texium
Aluminum salts in baking powder - Why?
Yep. It’s used in what is referred to as double-acting baking powder. It partially reacts when wet ...
28-3-2023 at 07:13
by: Texium
Dissolving Ir and IrO2 to Hexachloroiridate
Fantasma, please stop posting vague and ridiculous ideas for problems that have already been answere ...
27-3-2023 at 05:44
by: Texium
Mystery oxidizer labeled as KNO3
That does look like a potassium flame.
25-3-2023 at 16:05
by: Texium
Mystery oxidizer labeled as KNO3
Barium salts also generally give a quite strong lime green flame test, so it’s unlikely to be the ...
25-3-2023 at 10:55
by: Texium
Photochemical oxidation of alcohols to aldehydes using uranyl nitrate
Probably just uranyl(IV), as opposed to the more commonplace uranyl(VI).

Regardless, the importan ...
24-3-2023 at 09:17
by: Texium
Knick ph-meter Type 35
The endpoint will not always be 7, it depends on what you are titrating. A strong acid/strong base t ...
24-3-2023 at 05:52
by: Texium
Photochemical oxidation of alcohols to aldehydes using uranyl nitrate
Uranyl nitrate is the oxidizing agent. Specifically, uranyl ions they have been excited by UV light. ...
23-3-2023 at 19:28
by: Texium
Failed distillation of HNO3 from KNO3 ??
I’m going to close this thread now to prevent cross-posting, being as the answer to why the distil ...
23-3-2023 at 13:55
by: Texium
Failed distillation of HNO3 from KNO3 ??
[rquote=682608&tid=159437&author=ave369]Not nitrate, maybe ammonium perchlorate?[/rquote]Pro ...
23-3-2023 at 10:57
by: Texium
Failed distillation of HNO3 from KNO3 ??
Yikes! I was wondering if that could have been what happened when I first read this. Fortunately you ...
22-3-2023 at 21:28
by: Texium
Brand new hotplate won't boil water?
[rquote=682530&tid=159426&author=BromicAcid]When I was doing chemistry in my back yard I had ...
22-3-2023 at 10:00
by: Texium
Chamazulene, natural blue dye extraction and purification
Apologies. I totally meant to move this thread to Organic Chemistry, but accidentally moved it to Be ...
20-3-2023 at 19:25
by: Texium
Ruby synthesis with the help of the Sun
If you can find an old projection TV, they had big Fresnel lenses like that right on the front! They ...
20-3-2023 at 17:54
by: Texium
Oxygen scavengers for working with Iron(II) and Manganese(II) salts?
Phenols aren’t a good option: they complex iron (I don’t know about manganese, but I wouldn’t ...
20-3-2023 at 17:21
by: Texium
Concentration of a solution based on molar mass
[rquote=682437&tid=159417&author=Sulaiman]eg If digital scales were previously easily availa ...
19-3-2023 at 15:02
by: Texium
Gas Stove
@Rainwater: You’re repeating several common misconceptions that may have been true 10 years ago or ...
19-3-2023 at 06:47
by: Texium
Glacial acetic acid and baking soda slow reaction
It's simple. Sodium bicarbonate is soluble in water but not in acetic acid. The ions that need to ex ...
18-3-2023 at 09:41
by: Texium
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