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First mononitrotoluene synthesis - Having some problems (I think?)
[rquote=655631&tid=157094&author=Benignium]I suggest getting some Bel-Art brand stir bars, t ... |
1-3-2021 at 08:03
by: SuperOxide |
First mononitrotoluene synthesis - Having some problems (I think?)
Ok, so it's all finished.
Basically it took forever because the container I used for the ice bat ... |
28-2-2021 at 07:36
by: SuperOxide |
First mononitrotoluene synthesis - Having some problems (I think?)
[b]Update 1[/b]: It's now turning a lighter orange (still orange though.. but less red, I guess). So ... |
27-2-2021 at 18:46
by: SuperOxide |
First mononitrotoluene synthesis - Having some problems (I think?)
I'm doing my first nitrotoluene synthesis, just a quick summary of how it's gone so far:
- The mix ... |
27-2-2021 at 18:24
by: SuperOxide |
Best/preferred method for cleaning up toluene paint thinner?
[rquote=655498&tid=157084&author=unionised]Do you have any quantitative idea how much thioph ... |
25-2-2021 at 16:22
by: SuperOxide |
Safe storage of DCM
[rquote=655469&tid=156955&author=Tellurium]Wow these are high prices, that you have in ameri ... |
25-2-2021 at 09:18
by: SuperOxide |
Best/preferred method for cleaning up toluene paint thinner?
[rquote=655490&tid=157084&author=Texium (zts16)]Try method 1 first. The toluene that I have ... |
25-2-2021 at 09:11
by: SuperOxide |
Best/preferred method for cleaning up toluene paint thinner?
I have some toluene that I want to clean up so I can use it as a solvent as well as in some reaction ... |
25-2-2021 at 08:25
by: SuperOxide |
Properties of diphenhydramine base?
[b]@OctanitroC[/b] - Did this ever work out? Curious what your results were, or if you chose a diffe ... |
24-2-2021 at 08:48
by: SuperOxide |
Polyphosphoric acid
@RustyShackleford - Very nice! Thanks for sharing your procedure and photos. |
22-2-2021 at 14:40
by: SuperOxide |
Separation of nitrotoluene isomers
[rquote=655251&tid=155891&author=Fery]For pure 2-nitrotoluene you need vacuum distillation o ... |
19-2-2021 at 09:31
by: SuperOxide |
Separation of nitrotoluene isomers
I plan on making some [i][b]mono[/b]nitrotoluene[/i] soon, and I'm particularly interested in the [i ... |
18-2-2021 at 20:23
by: SuperOxide |
Separation of nitrotoluene isomers
[rquote=655159&tid=155891&author=Fery]Hi SuperOxide, I did this recently, not yet fully fini ... |
17-2-2021 at 08:46
by: SuperOxide |
Safe storage of DCM
[rquote=655134&tid=156955&author=alive&kickin]I know that DCM is getting harder to find ... |
16-2-2021 at 18:01
by: SuperOxide |
Separation of nitrotoluene isomers
I plan on doing this in the very near future. I'm trying to see how low I can get with ice/salt, and ... |
16-2-2021 at 13:39
by: SuperOxide |
Removing acetone from chloroform
[rquote=655062&tid=157050&author=Fyndium]You know where that leads... Eventually you've got ... |
15-2-2021 at 08:11
by: SuperOxide |
Removing acetone from chloroform
[rquote=655033&tid=157050&author=Fyndium]
At the moment, I have acetone that reeks strongly ... |
15-2-2021 at 06:12
by: SuperOxide |
Removing acetone from chloroform
[rquote=654996&tid=157050&author=ChemichaelRXN]You can add water to separate the chloroform ... |
14-2-2021 at 15:26
by: SuperOxide |
Removing acetone from chloroform
I made some chloroform using the bleach/acetone method, and while I was pretty sure the bleach was i ... |
14-2-2021 at 11:14
by: SuperOxide |
successful method for purifying anthranilic acid(quick report)
I was doing another anthranilic acid synthesis today, getting enough so that I can get enough to put ... |
11-2-2021 at 17:44
by: SuperOxide |
successful method for purifying anthranilic acid(quick report)
[rquote=654646&tid=155744&author=Texium (zts16)]This is fantastic, B.D.E. That is the cleane ... |
8-2-2021 at 18:08
by: SuperOxide |
successful method for purifying anthranilic acid(quick report)
[rquote=640083&tid=155744&author=B.D.E][...]
If larger crystals are desired, you can add a ... |
8-2-2021 at 14:13
by: SuperOxide |
Safe storage of DCM
[rquote=654497&tid=156955&author=Chemorg42]I get my solvents from hardware stores, so they c ... |
6-2-2021 at 10:46
by: SuperOxide |
Safe storage of DCM
[rquote=654469&tid=156955&author=NaK]Some sellers - limac for example - ship DCM in HDPE bec ... |
6-2-2021 at 08:09
by: SuperOxide |
Methaqualone
@Benignium - in your initial post here, you said:
[rquote=651043&tid=156723&author=Benigniu ... |
4-2-2021 at 10:47
by: SuperOxide |
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