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proposed final revision I resequenced a couple of sections to align with the reaction sequence and have reduced the file siz ...	11-9-2015 at 09:02 by: Rosco Bodine
Methylamine hydrochloride reacting with copper Actually it was trimethylamine that I was thinking of does not form a complex with copper. So it co ...	10-9-2015 at 14:46 by: Rosco Bodine
Methylamine hydrochloride reacting with copper IIRC Methylamine does not complex copper	9-9-2015 at 23:28 by: Rosco Bodine
Restoring Forum Images [rquote=406123&tid=62440&author=gdflp]Does anyone happen to still be in contact with [b]Enga ...	6-9-2015 at 10:56 by: Rosco Bodine
DBX-1 One of the inventors passed this along to me. Sharing is caring. I get a real chuckle knowi ...	4-9-2015 at 15:34 by: Rosco Bodine
DDNP & related compounds: The über thread! [rquote=418035&tid=439&author=nitro-genes] @ At Rosco, haha amazing, had the same idea and ...	3-9-2015 at 07:11 by: Rosco Bodine
possible alternative synthesis for o-DDNP I have an idea for a possible alternative method of synthesis for o-DDNP based upon nitration of sal ...	31-8-2015 at 21:49 by: Rosco Bodine
DDNP & related compounds: The über thread! Regarding US8748639 (attached) It looks like what they are doing is forming the soluble diazonium ...	27-8-2015 at 08:08 by: Rosco Bodine
3-diazo-picric acid (exist?) possible? precursor for iso-DDNR (exist?) If they don't exist yet, then let us invent them here In a couple of posts last month by nitro ...	26-8-2015 at 20:32 by: Rosco Bodine
DDNP & related compounds: The über thread! You are onto something good there with the use of copper in wire form. The fine copper wire could ...	25-8-2015 at 10:33 by: Rosco Bodine
DDNP & related compounds: The über thread! That is a clever variation for the diazotization scheme using copper to generate the NO2. Was that ...	25-8-2015 at 06:15 by: Rosco Bodine
Synthesis of 4-amino-2,6-dinitrophenol (isopicramic acid) and p-DDNP from acetaminophen Also see the dedicated DDNP and related compounds sticky thread in Energetic Materials which contain ...	24-8-2015 at 23:55 by: Rosco Bodine
Synthesis of 4-amino-2,6-dinitrophenol (isopicramic acid) and p-DDNP from acetaminophen That reference about p-DDNP for which you were asking is I think Meldola and Stephens, JCS, Volume 8 ...	24-8-2015 at 09:51 by: Rosco Bodine
DDNP & related compounds: The über thread! Usually the boiling of a diazo compound with alcohol will eliminate the diazo and leave the unsubsti ...	16-8-2015 at 16:15 by: Rosco Bodine
DDNP & related compounds: The über thread! What you could be observing with the color shift is a dye indicator pH effect similar as occurs with ...	12-8-2015 at 11:26 by: Rosco Bodine
DDNP & related compounds: The über thread! Great minds think alike. The possibility of improving the yield by reducing any nitrous acid pres ...	11-8-2015 at 08:15 by: Rosco Bodine
DDNP & related compounds: The über thread! Thank you for the detailed report. This is one for the books, and provides valuable information not ...	9-8-2015 at 12:16 by: Rosco Bodine
possible catalyst for 3-nitro acetaminophen and DDNR There has been some progress to report a possible usefulness of molybdenum as a nitration catalyst p ...	5-8-2015 at 21:45 by: Rosco Bodine
"nitrous gases" useful for nitrations In a previous post the subject of nitrosylsulfuric acid was brought up as being an observed componen ...	1-8-2015 at 08:19 by: Rosco Bodine
DDNP & related compounds: The über thread! Many diazo compounds are sensitive to decomposition by bases, so it may be better when making the so ...	27-7-2015 at 05:55 by: Rosco Bodine
DDNP & related compounds: The über thread! Should be light yellow for the color for DDNR and for the K salt There is a different brown color ...	25-7-2015 at 04:19 by: Rosco Bodine
DDNP & related compounds: The über thread! Ha! It would be fortuitous if another error has been found in the literature with the ancient repor ...	24-7-2015 at 07:48 by: Rosco Bodine
Low melting salt mixtures Here's a useful table for mixed nitrates eutectics made anhydrous by heating http://www.sciencem ...	23-7-2015 at 18:58 by: Rosco Bodine
DDNP & related compounds: The über thread! There are some additional attachments to the earlier post where I found the third reference for whic ...	23-7-2015 at 16:23 by: Rosco Bodine
DDNP & related compounds: The über thread! [rquote=413309&tid=439&author=nitro-genes]Quite possibly the product consists mostly of pDDN ...	23-7-2015 at 09:05 by: Rosco Bodine
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