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The short questions thread (2)
I have tryed Sn/HCl method- failure.
I also tryed the folowing method taken from ORganic Chemistry ... |
27-9-2009 at 01:04
by: Picric-A |
testing for organic peroxides
Probably because the peroxide formed from isopropanol is much less sensitive/powerfull ect?
[Edited ... |
24-9-2009 at 00:39
by: Picric-A |
diethyl phthalate synthesis
hmm if the phthalic anhydride acts like normal anhydrides meerly boiling 2 moles of ethanol with 1 m ... |
23-9-2009 at 12:18
by: Picric-A |
NOCl as chlorinating/nitrating agent?
I think the result of a nitration runaway is the oxidation of the alcohol to CO2 and water, i am not ... |
22-9-2009 at 01:50
by: Picric-A |
NOCl as chlorinating/nitrating agent?
[rquote=162687&tid=12839&author=ketel-one]__________________________________
______________ ... |
20-9-2009 at 23:00
by: Picric-A |
NOCl as chlorinating/nitrating agent?
NH4NO3 + HCl forms nitric acid which is corrosive to copper forming blue Cu(NO3)2 and nitrogen dioxi ... |
20-9-2009 at 22:58
by: Picric-A |
NOCl as chlorinating/nitrating agent?
I cannot find any refs to the cleavage of ethers using Nitrosyl chloride. do you have any?
I though ... |
20-9-2009 at 12:49
by: Picric-A |
The short questions thread (2)
[rquote=162507&tid=12054&author=entropy51][rquote=162493&tid=12054&author=Picric-A]
... |
18-9-2009 at 07:24
by: Picric-A |
The short questions thread (2)
[rquote=162480&tid=12054&author=entropy51]There is an OTC product which consists mainly of s ... |
17-9-2009 at 22:31
by: Picric-A |
Storing Diethylamine?
[rquote=162476&tid=12822&author=Agent MadHatter]
But whats the best way to get the DEA HC ... |
17-9-2009 at 12:54
by: Picric-A |
SnI4: A nice covalent compound of tin
Nice work Woelen!
what possible uses does organotin compounds have? maybe a possible less toxic sub ... |
17-9-2009 at 12:23
by: Picric-A |
The short questions thread (2)
[rquote=162473&tid=12054&author=Paddywhacker][rquote=162467&tid=12054&author=Jor]I a ... |
17-9-2009 at 12:16
by: Picric-A |
The short questions thread (2)
Sodium bromide melts at 747 deg C, its dihydrate dehydrates at 34deg C so if you wanted the anhydrou ... |
17-9-2009 at 10:23
by: Picric-A |
Iron Ethanedioate (oxalate) stains
Yes i hope so, it did take a while though (2 hours) for the stain to be fully removed though and how ... |
16-9-2009 at 09:07
by: Picric-A |
Storing Diethylamine?
quantities used, reaction time, problems encountered, colour changes ect! |
16-9-2009 at 02:09
by: Picric-A |
Iron Ethanedioate (oxalate) stains
When i used the filter flask to generate chlorine that removed the stain after about 2 hours contact ... |
15-9-2009 at 23:13
by: Picric-A |
Storing Diethylamine?
[rquote=162342&tid=12822&author=DJF90][rquote=162334&tid=12822&author=Picric-A]
If ... |
15-9-2009 at 12:49
by: Picric-A |
Storing Diethylamine?
I think he distilled the amine out into HCl(aq) then boiled down forming the salt!
but indeed this ... |
15-9-2009 at 11:16
by: Picric-A |
Storing Diethylamine?
Just a quick note, 100% deet can be had for half the rrp off ebay UK
If this guy thinks hes distill ... |
15-9-2009 at 10:14
by: Picric-A |
Diethylamine Synthesis
[rquote=162284&tid=11081&author=crazyboy][rquote=160949&tid=11081&author=entropy51] ... |
15-9-2009 at 07:13
by: Picric-A |
Benzene synthesis
Yes, heating 2-methyl-benzoic acid with NaOH will produce toluene |
14-9-2009 at 09:02
by: Picric-A |
Alternative Oxidisers in Skraup reaction
Yep unfortunatly i did use most (about a gram left) of the V2O5 on a catalyst but i am at school now ... |
10-9-2009 at 13:45
by: Picric-A |
Alternative Oxidisers in Skraup reaction
I am trying to synthesise some Quinoline from Phenylamine and glycerol however we dont have any Nitr ... |
9-9-2009 at 11:14
by: Picric-A |
Nitric Acid Synthesis
Roaring bunsen on test tube scale and nichrome on copper tube scale. If you had read what i wrote ca ... |
8-9-2009 at 01:13
by: Picric-A |
Nitric Acid Synthesis
[rquote=161768&tid=2176&author=entropy51]Is it just me, or are all these esoteric methods of ... |
7-9-2009 at 16:27
by: Picric-A |
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