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Isopropylamine via sulfuric acid, propylene (MAPP PRO gas), and sulfamic acid?
Check page 2 of this thread for posts by Scr0t and Magpie - http://www.sciencemadness.org/talk/viewt ...
4-7-2017 at 10:02
by: Corrosive Joeseph
Street drug analysis / harm reduction
d-Methamphetamine hydrochloride - Melting Point = 172 - 174c

N-Isopropylbenzylamine hydrochlorid ...
4-7-2017 at 09:29
by: Corrosive Joeseph
Isopropylamine via sulfuric acid, propylene (MAPP PRO gas), and sulfamic acid?
A popular glyphosate herbicide in my area has this printed on the front label -

"This product is ...
3-7-2017 at 15:35
by: Corrosive Joeseph
OTC source of sodium dithionite and synthesis
[rquote=486821&tid=75133&author=symboom]
Carbona color run remover ingredients
In the laun ...
2-7-2017 at 17:47
by: Corrosive Joeseph
Isopropylamine via sulfuric acid, propylene (MAPP PRO gas), and sulfamic acid?
[rquote=486679&tid=75081&author=Melgar] and MAPP PRO gas is just propylene and propane mixed ...
1-7-2017 at 22:50
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
[rquote=486102&tid=74672&author=alking]What is cyclohexamine sold as in autoparts stores? [/ ...
27-6-2017 at 11:00
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
Thanks Melgar, that was all I had dug up so far....... Most of it posted for the OP and the benefit ...
21-6-2017 at 01:19
by: Corrosive Joeseph
Drizzle - kitchen soxhlet appliance
Wow, that's VERY cool. Impressive stuff.

I have built a few extraction vessels in my day but non ...
21-6-2017 at 00:25
by: Corrosive Joeseph
Drizzle - kitchen soxhlet appliance
Very cool dude. Plant extractions and tinctures are 'my thing' right now.
Can't wait to see the "up ...
20-6-2017 at 21:30
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
Please excuse the double post...........

For the OP - Taken from the attachment above -

"The ...
20-6-2017 at 20:49
by: Corrosive Joeseph
Does this seem a safe and effective way to alkylate ammonia?
Here is the citation for the n-Butylamine prep - Ref 84

Frank C. Whitmore, D. P. Langlois. J. Am. ...
20-6-2017 at 20:23
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
Oh-kay............. The whole reaction is very complex actually.......... I'm still trying to get my ...
19-6-2017 at 12:18
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
@ Meglar - Could you elaborate on that, I always thought it was aluminium hydroxide that was one of ...
15-6-2017 at 07:24
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
[rquote=485445&tid=74672&author=Melgar]Imine formation is reversible. Typically, the reacti ...
13-6-2017 at 15:33
by: Corrosive Joeseph
Alternative to DCM?
Ethyl acetate is available as 'acetone-free nail varnish remover'...........

Dichloroethane from ...
13-6-2017 at 14:51
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
I have been interested in low MW amines for a while now. I really wish I knew more. But what I do kn ...
12-6-2017 at 14:47
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
Quote from a post by Nicodem in this thread - 'Isopropylamine and Diisopropylamine from Acetone'
ht ...
12-6-2017 at 07:43
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
Freebase IPA boils at 31-35 degrees C and is miscible with water - https://en.wikipedia.org/wiki/Iso ...
10-6-2017 at 13:37
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
[rquote=485295&tid=74672&author=unionised]IIRC the reaction of ammonia solution with acetone ...
10-6-2017 at 12:58
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
Did you basify like regular Al-Hg.............? Although it's probably pretty basic already. Taken f ...
10-6-2017 at 12:27
by: Corrosive Joeseph
Acetate salts (Ca/Na preferrb) products - what is it used in and where to get it (5-25kg)
"Calcium acetate is used as a food additive, as a stabilizer, buffer and sequestrant, mainly in cand ...
10-6-2017 at 01:51
by: Corrosive Joeseph
Hg/Al Reductive Amination w/Ammonia - Not Viable?
Can you post your experimental please..............?


/CJ
9-6-2017 at 14:51
by: Corrosive Joeseph
Hypothetically drinkable ethanol from methylated spirits
Many of those compounds have a lower BP than EtOH, but there shouldn't be more than trace amounts
A ...
9-6-2017 at 02:55
by: Corrosive Joeseph
Hypothetically drinkable ethanol from methylated spirits
[rquote=485178&tid=74507&author=Assured Fish]
If you ferment your own the only component th ...
8-6-2017 at 22:42
by: Corrosive Joeseph
Hypothetically drinkable ethanol from methylated spirits
The ethanol-ethyl acetate azeotrope boils at 71.8c and is 69.2% by weight with a specific gravity of ...
5-6-2017 at 02:21
by: Corrosive Joeseph
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