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Friedel-Crafts acylation of anilides Hi Pumukli, take a look at these two papers:
Chattaway, Proc. Chem. Soc. 1902, p173 and 1903, p12 ... |
9-1-2021 at 12:58 by: Boffis |
Fenton type oxidation Does anyone have any actual experience of the se of Fenton's reagent in oxidation in organic chemist ... |
9-1-2021 at 02:18 by: Boffis |
Successful Synthesis of 1-Amino-3-nitroguanidine Nitrate Did you check out this thread?:
http://www.sciencemadness.org/talk/viewthread.php?tid=83736 |
8-1-2021 at 14:46 by: Boffis |
Things to do with Ethyl Formate [rquote=652755&tid=156492&author=Pumukli]Why not combine the two? Alkaline sulfide precipita ... |
8-1-2021 at 09:04 by: Boffis |
Things to do with Ethyl Formate I have now isolated over 60g of copper triazole sulphate, its composition is as yet unknown but look ... |
8-1-2021 at 03:35 by: Boffis |
p-Nitroso-dimethylaniline Hi Pumukli, I had a go at recrystallising some of my least pure p-nitrosodimethylaniline from pet et ... |
7-1-2021 at 14:39 by: Boffis |
Group buy Duran Keck vacuum erlenmeyer adapters Thanks Bubbles. Glad to hear they arrived OK. |
7-1-2021 at 13:53 by: Boffis |
Preparation of furfural from cherry gum and other pentose sources Hi Fery. My understanding is that for steam distillation to work the compound should be essentially ... |
7-1-2021 at 13:50 by: Boffis |
hydrobenzamide from benzaldehyde and ammonia Nice work Fery and really well referenced. There are some interesting sounding derivatives too.
I ... |
7-1-2021 at 05:58 by: Boffis |
Preparation of furfural from cherry gum and other pentose sources I tried scaling up the preparation to 150g of xylose under the same conditions and obtained the same ... |
7-1-2021 at 05:16 by: Boffis |
Purple acid, N2O2HSO4 What an interesting find! Thank for the attached papers too, some light bedtime reading |
6-1-2021 at 04:11 by: Boffis |
furfural Hi Fery, Yes. In both cases with xylose I had to run the reaction for about 7 hours to get to a poin ... |
4-1-2021 at 10:41 by: Boffis |
Urea @Hey Buddy; urea is a very useful compound in terms of being a starting material. Apart from buiret, ... |
4-1-2021 at 03:35 by: Boffis |
furfural I have now repeated the larger scale preparation using 150g of D-ribose in stead of xylose. I used e ... |
4-1-2021 at 01:53 by: Boffis |
furfural OK I've posted my full write-up on the preparation of furfural from various source over in the "Prep ... |
2-1-2021 at 01:15 by: Boffis |
Preparation of furfural from cherry gum and other pentose sources A flowering cherry tree in our garden has over the past few years begun to weep a clear gelatinous g ... |
1-1-2021 at 14:41 by: Boffis |
Ethylamine Synthesis Feasible but your source of propionitrile is..? |
1-1-2021 at 12:45 by: Boffis |
furfural Hi Fery, I hope to get my prepub posting up today. But yes the price of D-ribose in the UK now is as ... |
1-1-2021 at 03:28 by: Boffis |
Nitroguanidine from guanidine nitrate dehydration @roXefeller; the key to this preparation is keeping the reaction temperature low <10 degrees. Abo ... |
1-1-2021 at 03:11 by: Boffis |
furfural Ethyl furoate, what does that smell like ? |
31-12-2020 at 12:31 by: Boffis |
Cleaning / Recycling HNO3 Solution If by -80% of ATM you mean 200 mBar then yes. I have found that water venturi pressures (typically a ... |
31-12-2020 at 10:35 by: Boffis |
furfural This is a long dormant thread but I think it is worth reviving. Over the last few years, each spring ... |
31-12-2020 at 05:42 by: Boffis |
Cleaning / Recycling HNO3 Solution Vacuum distillation? |
30-12-2020 at 15:51 by: Boffis |
Violuric acid salts (fantastic colors and variety) Alloxan reacts with 1 molar equivalence of hydroxylamine to give violuric acid. In practice a hydrox ... |
30-12-2020 at 13:39 by: Boffis |
p-Nitroso-dimethylaniline Many thanks AvBaeyer, this is an interesting since this is one of my intended uses of the freebase. ... |
30-12-2020 at 10:28 by: Boffis |
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