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Nitromethane from Nitromethane/Oil
If you could get more information on the type of oil that would make separation easier. If the oil i ...
15-1-2021 at 09:33
by: njl
1,3,5-trichlorohexahydrotriazine
As mentioned above, the electrophilic Cl+ is needed for this reaction. I'm guessing NaDCC is less la ...
15-1-2021 at 08:10
by: njl
Carbonate ester synthesis from urea?
As discussed in other threads, simple carbonate esters can be made simply from the alcohol and urea ...
15-1-2021 at 07:16
by: njl
How to calcine aluminum but not copper.
I have never seen "calcine" refer to that process, nor can I find any info on anything under that na ...
14-1-2021 at 16:22
by: njl
How to calcine aluminum but not copper.
Could you by any chance mean chlorinate and not calcine?
14-1-2021 at 07:16
by: njl
Rice husk ash, an amazing material and its uses!
If rice husks are 20 percent silica by dry mass, how can they be turned into effective charcoal? Isn ...
12-1-2021 at 07:14
by: njl
Peracetic acid
Yes and yes. Peracids can be used as selective oxidizing agents for the formation of epoxides, ester ...
12-1-2021 at 06:59
by: njl
Synthesis of N,N'-dialkyloxamides
Relevant paper: https://doi.org/10.1016/j.cclet.2018.01.003
And abstract: https://www.sciencedirect ...
11-1-2021 at 09:40
by: njl
Friedel-Crafts acylation of anilides
Note 1 in the following:


http://www.orgsyn.org/demo.aspx?prep=cv3p0191
11-1-2021 at 09:26
by: njl
Trying to get rid of chemicals. Nearish Philadelphia
Missed the deal of a lifetime :(
9-1-2021 at 16:13
by: njl
Friedel-Crafts acylation of anilides
Amines are lewis bases while AlCl3 is a lewis acid. So there will probably be some reaction there, m ...
9-1-2021 at 10:21
by: njl
Chlorination
In Shulgin's report on the chlorination of 2C-H to 2C-C, he uses liquid chlorine as a reagent. Why c ...
8-1-2021 at 15:29
by: njl
Successful Synthesis of 1-Amino-3-nitroguanidine Nitrate
Impressive stuff! Will you be posting a write up on this synth?
8-1-2021 at 07:07
by: njl
hydrobenzamide from benzaldehyde and ammonia
Excellent write up!
7-1-2021 at 06:10
by: njl
ETN question
I believe phosphoric acid also works as an acid catalyst. As far as I know, an acid is needed to pro ...
5-1-2021 at 11:02
by: njl
ETN question
Using HNO3/H2SO4 is generally preferable to (X)NO3/H2SO4, but in both cases sulfuric acid is needed. ...
5-1-2021 at 10:33
by: njl
ETN question
At least using acetone you can leave behind most of the solids. I don't think the idea was to pull o ...
5-1-2021 at 10:10
by: njl
Freestyle chem
I very much enjoy "freestyle" chemistry, just winging a procedure based on background knowledge. For ...
5-1-2021 at 07:22
by: njl
ETN question
How dry is your reaction mixture? Even though part of the reaction is dehydration, I believe you do ...
5-1-2021 at 07:01
by: njl
Urea
Yes, boiling water can dissolve ~5 Kg/L while only ~.5 Kg/L will dissolve at 0 C.

edit: Urea is a ...
4-1-2021 at 05:52
by: njl
Domestic (USA) sodium borohydride or lithium aluminum hydride?
[rquote=651788&tid=156778&author=thors.lab]On an unrelated note, Onyxmet says an F2 "gas sph ...
22-12-2020 at 10:55
by: njl
Nickel benzoate
Source?
21-12-2020 at 12:23
by: njl
Member questions
Hey. This isn't a post I would normally make, but I'm in a good mood since I got a bunch of equipmen ...
19-12-2020 at 07:27
by: njl
Sodium Triacetoxyborhydrid from NaBH4 in Benzene **HELP**
Well for all we know benzene is dirt cheap for OP, point is you need to either extract or dilute the ...
19-12-2020 at 07:18
by: njl
Sample analysis in Europe
No advise, but could you post some pictures?
18-12-2020 at 13:07
by: njl
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