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Nitromethane from Nitromethane/Oil If you could get more information on the type of oil that would make separation easier. If the oil i ... |
15-1-2021 at 09:33 by: njl |
1,3,5-trichlorohexahydrotriazine As mentioned above, the electrophilic Cl+ is needed for this reaction. I'm guessing NaDCC is less la ... |
15-1-2021 at 08:10 by: njl |
Carbonate ester synthesis from urea? As discussed in other threads, simple carbonate esters can be made simply from the alcohol and urea ... |
15-1-2021 at 07:16 by: njl |
How to calcine aluminum but not copper. I have never seen "calcine" refer to that process, nor can I find any info on anything under that na ... |
14-1-2021 at 16:22 by: njl |
How to calcine aluminum but not copper. Could you by any chance mean chlorinate and not calcine? |
14-1-2021 at 07:16 by: njl |
Rice husk ash, an amazing material and its uses! If rice husks are 20 percent silica by dry mass, how can they be turned into effective charcoal? Isn ... |
12-1-2021 at 07:14 by: njl |
Peracetic acid Yes and yes. Peracids can be used as selective oxidizing agents for the formation of epoxides, ester ... |
12-1-2021 at 06:59 by: njl |
Synthesis of N,N'-dialkyloxamides Relevant paper: https://doi.org/10.1016/j.cclet.2018.01.003
And abstract: https://www.sciencedirect ... |
11-1-2021 at 09:40 by: njl |
Friedel-Crafts acylation of anilides Note 1 in the following:
http://www.orgsyn.org/demo.aspx?prep=cv3p0191 |
11-1-2021 at 09:26 by: njl |
Trying to get rid of chemicals. Nearish Philadelphia Missed the deal of a lifetime |
9-1-2021 at 16:13 by: njl |
Friedel-Crafts acylation of anilides Amines are lewis bases while AlCl3 is a lewis acid. So there will probably be some reaction there, m ... |
9-1-2021 at 10:21 by: njl |
Chlorination In Shulgin's report on the chlorination of 2C-H to 2C-C, he uses liquid chlorine as a reagent. Why c ... |
8-1-2021 at 15:29 by: njl |
Successful Synthesis of 1-Amino-3-nitroguanidine Nitrate Impressive stuff! Will you be posting a write up on this synth? |
8-1-2021 at 07:07 by: njl |
hydrobenzamide from benzaldehyde and ammonia Excellent write up! |
7-1-2021 at 06:10 by: njl |
ETN question I believe phosphoric acid also works as an acid catalyst. As far as I know, an acid is needed to pro ... |
5-1-2021 at 11:02 by: njl |
ETN question Using HNO3/H2SO4 is generally preferable to (X)NO3/H2SO4, but in both cases sulfuric acid is needed. ... |
5-1-2021 at 10:33 by: njl |
ETN question At least using acetone you can leave behind most of the solids. I don't think the idea was to pull o ... |
5-1-2021 at 10:10 by: njl |
Freestyle chem I very much enjoy "freestyle" chemistry, just winging a procedure based on background knowledge. For ... |
5-1-2021 at 07:22 by: njl |
ETN question How dry is your reaction mixture? Even though part of the reaction is dehydration, I believe you do ... |
5-1-2021 at 07:01 by: njl |
Urea Yes, boiling water can dissolve ~5 Kg/L while only ~.5 Kg/L will dissolve at 0 C.
edit: Urea is a ... |
4-1-2021 at 05:52 by: njl |
Domestic (USA) sodium borohydride or lithium aluminum hydride? [rquote=651788&tid=156778&author=thors.lab]On an unrelated note, Onyxmet says an F2 "gas sph ... |
22-12-2020 at 10:55 by: njl |
Nickel benzoate Source? |
21-12-2020 at 12:23 by: njl |
Member questions Hey. This isn't a post I would normally make, but I'm in a good mood since I got a bunch of equipmen ... |
19-12-2020 at 07:27 by: njl |
Sodium Triacetoxyborhydrid from NaBH4 in Benzene **HELP** Well for all we know benzene is dirt cheap for OP, point is you need to either extract or dilute the ... |
19-12-2020 at 07:18 by: njl |
Sample analysis in Europe No advise, but could you post some pictures? |
18-12-2020 at 13:07 by: njl |
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