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Acquire trimesic acid.
I had to Google that one, but how much do you need? And do you have a reference to the synth from to ...
22-3-2022 at 10:54
by: Tsjerk
Bromo-DDT, p,p-dibromo-diphenyl-1,1,1-trichloro-ethane
F-DDT was made.

85% yield, not distilled, but it did crystallize.

20 grams of chloral distill ...
21-3-2022 at 13:35
by: Tsjerk
Sodium Hypochlorite "bleach" reagent OTC
Calcium hypochlorite with sodium sulfate results in clean sodium hypochlorite.
21-3-2022 at 04:33
by: Tsjerk
Sodium Hypochlorite "bleach" reagent OTC
[rquote=672148&tid=158479&author=cycloknight19]
I know I could have bubbled it to make my o ...
21-3-2022 at 01:23
by: Tsjerk
Is trichloroisocyanuric acid actually an acid?
draculic acid, did you try adding a solution of cyanuric acid to a solution of NaOH?
21-3-2022 at 00:12
by: Tsjerk
Sticky Situation
The Wiki is not a place where everyone can contribute and discuss. The Wiki is a nice to have, but t ...
20-3-2022 at 12:27
by: Tsjerk
Sticky Situation
Sounds good to me. Especially with j_sums1's idea of having multiple people writing on the summary, ...
18-3-2022 at 00:19
by: Tsjerk
NaCl Crystals
When you have glycine you can try to grow triglycine sulfate. The crystals are nice and show birefri ...
17-3-2022 at 07:49
by: Tsjerk
Best way to extract sodium hypochlorite?
Enthalpy of sublimation is a bit higher than enthalpy of evaporation (50 kJ/mol against 40 kJ/mol). ...
16-3-2022 at 00:20
by: Tsjerk
Glassware cleaning routine
Depends on what you use the glassware for. Mercury? Probably better not. Kitchen salt? Shouldn't be ...
15-3-2022 at 07:40
by: Tsjerk
Nitric Acid From Oxalic Acid
Melting or even heating oxalic acid with a nitrate will oxidize the oxalic acid, but you could very ...
14-3-2022 at 12:01
by: Tsjerk
Everyday Chemistry
Recrystallizing some vanillyl oxime now to reduce with U-Ni-NH3 made in situ with zinc. I didn't loo ...
14-3-2022 at 03:48
by: Tsjerk
Is trichloroisocyanuric acid actually an acid?
No TCCA is not an acid, it is just in the name as you say.
14-3-2022 at 01:54
by: Tsjerk
Best way to extract sodium hypochlorite?
[rquote=671934&tid=158455&author=S.C. Wack]

On topic, I suspect that distillation with a ...
13-3-2022 at 01:53
by: Tsjerk
Best way to extract sodium hypochlorite?
Sodium hypochlorite pentahydrate is stable at refrigerator temperatures according to wiki.
11-3-2022 at 06:28
by: Tsjerk
Corrosion Chemistry of CaCl2 and MgCl2 Fully Explained?
[quote] But is this explanation for the highly corrosive nature for these particular select salts po ...
10-3-2022 at 23:29
by: Tsjerk
Synthesis of thioacetone?
No, because it is already evaporated when diluted. Also vapour pressure only starts playing a role i ...
10-3-2022 at 04:50
by: Tsjerk
Best way to extract sodium hypochlorite?
You made a mixture of sodium chloride and sodium chlorate. Upon heating hypochlorite decomposes into ...
9-3-2022 at 22:54
by: Tsjerk
Need help interpreting this TLC plate
You should downsize the images, I can't even zoom out far enough to get everything into one screen.
8-3-2022 at 22:58
by: Tsjerk
Labotoriumdiscounter NL
I ordered from them many times, but sometimes they try to cut corners here and there. I once ordered ...
8-3-2022 at 14:22
by: Tsjerk
Pretty Pictures (2)
That blue is intense! I read about it, is the color in the picture representative for the color in r ...
8-3-2022 at 02:42
by: Tsjerk
Pretty Pictures (2)
[file]92691[/file]

Hydroxylamine HCl from approximately 80% methanol.
6-3-2022 at 02:38
by: Tsjerk
Hydroxylamine via HCL, Nitromethane, and H2O?
I just ran this reaction and got a 87% yield, I used 1.2x excess azeotropic HCl.

After 24 hours I ...
6-3-2022 at 01:01
by: Tsjerk
Condition of a used hotplate
You shouldn't be doing what Antiswat is proposing to a functional IKA. They are designed to work wit ...
5-3-2022 at 06:37
by: Tsjerk
Is it now illegal to buy from chemcraft?
Although Chemcraft is not directly targeted by the sanctions, I would expect a severe delay in shipp ...
5-3-2022 at 04:00
by: Tsjerk
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