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First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=657349&tid=157162&author=Fery]I found helpful video here:
https://www.youtube.com/w ... |
1-4-2021 at 10:19
by: SuperOxide |
Methaqualone
[rquote=651155&tid=156723&author=karlos³][...]
Also, a personal opinion, I consider the pr ... |
28-3-2021 at 17:00
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=657197&tid=157162&author=Benignium]Awesome! There is indeed going to be some DCM as ... |
28-3-2021 at 15:37
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=657073&tid=157068&author=mr_bovinejony]I recently did a run of 150 grams of the grap ... |
26-3-2021 at 10:04
by: SuperOxide |
Large scale anthranilic acid prep
Very interesting... I have 500g of phthalimide that I will probably never use, which I could make th ... |
26-3-2021 at 08:43
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
FYI - finally got this synth/workup finished (mostly).
Here's the result:
[file]87604[/file]
... |
24-3-2021 at 18:44
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656481&tid=157162&author=Benignium]Somewhat unrelated, but I was left with a few gra ... |
16-3-2021 at 08:13
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656474&tid=157162&author=S.C. Wack]PS the pH and amount of NaOH to add does not need ... |
15-3-2021 at 16:16
by: SuperOxide |
Anyone else in the US having issues finding OTC sodium bromide?
[rquote=656404&tid=157140&author=zed][...]
Funny World. My Pyrotechnics guy say yer lim ... |
15-3-2021 at 11:30
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656423&tid=157162&author=Fery]This advice is too late, but why did you use Sn instea ... |
15-3-2021 at 08:08
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656400&tid=157162&author=zed]Um. You are going to steam distill it. Most of the br ... |
14-3-2021 at 15:41
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656387&tid=157162&author=Benignium]Seems reasonable on paper. Add all of the NaOH so ... |
14-3-2021 at 13:38
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
I'm in the middle of my first o-toluidine synthesis at the moment, using the protocol on the [url=ht ... |
14-3-2021 at 09:57
by: SuperOxide |
Anyone else in the US having issues finding OTC sodium bromide?
[rquote=656107&tid=157140&author=Texium (zts16)]Maybe you were remembering the brominating t ... |
9-3-2021 at 12:06
by: SuperOxide |
Anyone else in the US having issues finding OTC sodium bromide?
[rquote=656097&tid=157140&author=Texium (zts16)]Try a pool supply store. In TX I never saw N ... |
9-3-2021 at 10:45
by: SuperOxide |
Anyone else in the US having issues finding OTC sodium bromide?
Before I was really into chemistry, I remember seeing sodium bromide being sold at Home Depot, Walma ... |
9-3-2021 at 09:42
by: SuperOxide |
successful method for purifying anthranilic acid(quick report)
[rquote=656027&tid=155744&author=Texium (zts16)]What was your percent recovery?[/rquote]Unfo ... |
8-3-2021 at 07:33
by: SuperOxide |
successful method for purifying anthranilic acid(quick report)
@B.D.E - Can you tell me how much crude anthranilic acid you processed and for how long you refluxed ... |
7-3-2021 at 18:58
by: SuperOxide |
First mononitrotoluene synthesis - Having some problems (I think?)
So I just re-did the synthesis keeping everything the same except for the scale (just 25% larger sca ... |
6-3-2021 at 16:13
by: SuperOxide |
First mononitrotoluene synthesis - Having some problems (I think?)
[rquote=655861&tid=157094&author=Benignium]very nice!!![/rquote]Benignium - nice to hear fro ... |
5-3-2021 at 09:59
by: SuperOxide |
First mononitrotoluene synthesis - Having some problems (I think?)
[rquote=655845&tid=157094&author=Fery]very nice!!![/rquote] Thank you. It was a lot of work, ... |
4-3-2021 at 12:25
by: SuperOxide |
First mononitrotoluene synthesis - Having some problems (I think?)
For anyone wondering, I got the two isomers separated (kinda). The liquid (before separation) was [b ... |
4-3-2021 at 09:09
by: SuperOxide |
First mononitrotoluene synthesis - Having some problems (I think?)
[rquote=655681&tid=157094&author=mr_bovinejony]Does the quality of water really matter so mu ... |
1-3-2021 at 21:24
by: SuperOxide |
First mononitrotoluene synthesis - Having some problems (I think?)
[rquote=655676&tid=157094&author=Benignium]Great time to start keeping complete notes! It wa ... |
1-3-2021 at 17:11
by: SuperOxide |
Safe storage of DCM
[rquote=655672&tid=156955&author=Mateo_swe]DCM doesnt do well in HDPE?
Hmm, i got two 5L ... |
1-3-2021 at 14:24
by: SuperOxide |
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